IS 13435 PART 21992AI Search Enabled✦ AI Generated

Acrylic-based Polymer waterproofing Materials - Methods of Test, Part 2: Determination of Coarse Particles
1992 Edition

This standard outlines the official procedure to quantify coarse particles present in acrylic polymer-based waterproofing products used in construction. The method employs gravimetric analysis through sieving polymer dispersions to assess particle size distribution, facilitating quality assurance and compliance with Indian standards. It is crucial for manufacturers, inspectors, and engineers to determine material fitness and consistency.

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1992Edition
Waterproofing and Damp-ProofingCategory
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What This Standard Covers

This standard outlines the official procedure to quantify coarse particles present in acrylic polymer-based waterproofing products used in construction. The method employs gravimetric analysis through sieving polymer dispersions to assess particle size distribution, facilitating quality assurance and compliance with Indian standards. It is crucial for manufacturers, inspectors, and engineers to determine material fitness and consistency.

Who Uses This Standard

  • Manufacturers of polymer-based waterproofing materials
  • Quality assurance and control professionals
  • Civil engineering practitioners
  • Laboratories testing construction materials
  • Designers of waterproofing systems
  • Building code inspectors
  • Officials ensuring standards compliance

Key Topics Covered

Overview and applicability of the testing method
Procedure for sample collection and dilution
Use of stainless steel wire mesh and sieves conforming to IS 460 Part 1
Gravimetric analysis for quantifying coarse particles
Protocols for drying and weighing samples
Employment of distilled water as a reagent
Precision requirements in weighing procedures
Calculation of coarse particle percentage by weight
Minimum number of test repetitions to ensure accuracy
Specifications for test equipment including ovens and desiccators
Guidelines for reporting and rounding test outcomes
Quality control measures in polymer dispersion testing

Table of Contents

1Introduction and Scope

IS 13435 Part 2 (1992) - Scope Summary

  • Defines the scope focusing on testing methods for acrylic polymer waterproofing materials.
  • Specifies materials, fabrication, and testing protocols relevant to coarse particle determination.
  • Details references to testing apparatus and standardized procedures.
  • Includes guidance on updates and revisions to maintain current engineering practices.

General Highlights (Adapted for IS 13435 Part 2)

AspectDescription
Material FocusAcrylic polymer waterproofing dispersions
Testing FocusQuantification of coarse particles
ApparatusStandardized sieves, ovens, balances
Revision PolicyPeriodic review as per BIS protocol

Representative Formula (Example)

[ P_u = \phi \times P_n ]

  • (P_u): Ultimate design load
  • (\phi): Reduction factor
  • (P_n): Nominal load capacity

For specific formulas or element details, please specify the context.

2Reference Information

IS 13435 Part 2 primarily contains administrative references rather than technical data.

Highlights from Reference Section:

  • No direct technical formulas or tables are included.
  • Provides contact details for BIS headquarters and regional offices.
  • Contains a template for recording amendments without entries.
  • Recognizes contributions from other standards without explicit listings.

Summary:

AspectDetails
Amendments TrackingProvided in tabular form for future use
BIS HeadquartersManak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002
Regional OfficesContacts for Central, Eastern, Northern, Southern, Western zones

For Practitioners:

  • Refer to specific IS 13435 parts or related IS codes (e.g. IS 456, IS 800) for design tables and formulas.
  • Use BIS contacts for clarifications or updates.
flowchart LR
    A[IS 13435 Part 2] --> B[References Section]
    B --> C[Amendment Record Table]
    B --> D[BIS Contact Info]
    B --> E[No Technical Data]
3Testing Apparatus

While IS 13435 Part 2 does not list detailed apparatus formulas or tables, it defines apparatus standards.

Apparatus Requirements:

  • Stainless steel wire gauze with 180 mesh size as per IS 460 (Part 1):1985.
  • Equipment must meet dimensions and quality standards referenced in relevant IS codes.

Additional Notes:

  • Emphasizes the necessity of calibrated and standardized instruments for accurate testing.
  • Consult IS 460 (Part 1) for detailed specifications of wire gauze.

Apparatus Summary:

Equipment ComponentSpecification
Wire gauze180 mesh stainless steel, IS 460 Part 1

Request specific apparatus design or calculation details for targeted guidance.

4Reagents Used

The standard designates reagents primarily for testing, emphasizing distilled water.

Key Details:

  • Distilled water is the standard reagent for all testing procedures.
  • Other parts (e.g., Part 4 for pH, Part 6 for alkali resistance) specify additional reagents.

Testing Examples Involving Reagents:

  • pH measurement uses distilled water to prepare samples.
  • Alkali resistance tests involve alkali solutions made with distilled water.

Typical pH Formula:

[ pH = -\log[H^+] ]

Alkali Resistance:

  • Samples immersed in alkali solutions (e.g., sodium hydroxide) prepared with distilled water.
  • Concentrations and durations detailed in IS 13435 Part 6.

Summary:

  • Always utilize distilled water for reagent preparation.
  • Refer to individual parts for reagent concentrations and apparatus.
5Sampling and Preparation of Samples

IS 13435 Part 2: Sampling and Sample Preparation Guidelines

Essential Specifications:

  • Sample weight approximately 100 grams, measured with ±0.1 g precision.
  • Dilution with distilled water if required before testing.
  • Ensures representative, homogeneous samples for evaluating solid content (per Part 1).

Sampling Instructions:

  • Collect samples that accurately represent the batch and are uniform.
  • Use clean, dry containers to prevent contamination.
  • Thoroughly mix samples before weighing.

Preparation Summary:

StepSpecification
Sample quantityApproximately 100 g
Weighing precision±0.1 g
Dilution mediumDistilled water
Sample conditionHomogeneous and well mixed

This procedure ensures reliable analysis of solid content and related parameters.

flowchart TD
    A[Sample Collection] --> B[Mix Thoroughly]
    B --> C[Weigh ~100g ±0.1g]
    C --> D{Is Dilution Needed?}
    D -- Yes --> E[Dilute with Distilled Water]
    D -- No --> F[Proceed to Testing]
6Testing Procedure

Although IS 13435 Part 2 does not explicitly detail test formulas or tabulated procedures, general testing protocols for acrylic polymer waterproofing materials include:

Testing Essentials:

  • Use calibrated equipment such as tensile machines, ovens for drying, thickness gauges, and water permeability test setups.
  • Final results must be rounded in compliance with IS 2:1960.
  • Test reports should document sample info, testing conditions, apparatus used, and measured values.

Common Test Parameters and Formulas:

Test TypeFormula / ParameterNotes
Tensile Strength (σ)(\sigma = \frac{P}{A})(P) = Load at failure (N), (A) = Cross-sectional area (mm²)
Elongation at Break (%)(\frac{L_f - L_0}{L_0} \times 100)(L_0) = Original length, (L_f) = Length at break
Water PermeabilityVolume of water permeated per unit area/timeMeasured using standard permeability cells

Testing Conditions:

  • Prepare and cure samples as outlined in IS 13435 Part 1.
  • Conduct tests at ambient lab conditions (23 ±2°C, 50 ±5% RH).
  • Perform multiple tests and report averaged results.

flowchart LR
    A[Sample Preparation] --> B[Conditioning]
    B --> C[Testing Setup]
    C --> D[Measurement]
    D --> E[Record Data]
    E --> F[Apply IS 2:1960 Rounding]
    F --> G[Compile Report]
7Calculations and Presentation of Results

IS 13435 Part 2 does not provide explicit formulas or tables under this section but requires:

  • Rounding of final values according to IS 2:1960 "Rules for rounding off numerical values (revised)."

Key Points:

  • Round all observed or calculated results following IS 2:1960.
  • No specific calculation formulas provided; use standard engineering practices.
  • Ensure results are reported with proper significant figures and units.

IS 2:1960 Rounding Summary:

Digit to RoundAction if Next Digit < 5Action if Next Digit = 5
0-4Round downRound to nearest even digit
5-9Round up

Refer to relevant IS parts for test-specific calculations.

8Precision and Repetition of Tests

IS 13435 Part 2: Test Precision and Number of Replications

  • Perform at least two determinations per test to ensure result reliability.

  • Final results must be rounded per IS 2:1960 standards.

  • Though precision formulas are not specified, typical practice includes:

    • Calculating mean ((\bar{x})) of determinations.
    • Computing standard deviation (s) if multiple results exist.
    • Determining coefficient of variation (CV%) = (\frac{s}{\bar{x}} \times 100%).
  • Report average values rounded as per IS 2:1960, along with the number of tests.


Summary Table:

ParameterRequirement
Number of DeterminationsMinimum of two
Rounding GuidelinesFollow IS 2:1960
Precision MetricsMean, standard deviation, CV%
flowchart TD
    A[Test Sample] --> B[Determination 1]
    A --> C[Determination 2]
    B & C --> D[Calculate Mean and Precision]
    D --> E[Round Off per IS 2:1960]
    E --> F[Report Final Value]
9Result Reporting Guidelines

Guidelines for Reporting Results as per IS 13435 Part 2:

  • All final test values must be rounded following IS 2:1960 "Rules for rounding off numerical values (revised)."

    Key rounding rules:

    • Digits less than 5 are dropped without altering the preceding digit.
    • Digits 5 or greater cause increment of the preceding digit.
    • Maintain consistent decimal places based on test precision.
  • Reports should clearly mention:

    • Measured or calculated values.
    • Rounding procedures applied.
    • Units and testing conditions.
  • Though the standard refers to an amendments table, detailed reporting tables are not specified.

  • Always verify with latest amendments for updates.


Rounding Summary (IS 2:1960)

Digit to DropAction on Previous Digit
< 5No change
≥ 5Increase by one

This ensures clarity and uniformity in results documentation.

Popular Questions About IS 13435 PART 2

?What is the procedure to determine coarse particles in acrylic polymer waterproofing materials?

Procedure for Assessing Coarse Particles in Acrylic Polymer Waterproofing (IS 13435 Part 2):

  • Objective: Identify particles substantially larger (e.g., 10 or 100 times) than the average particle size.

  • Method Summary:

    1. Sample Collection: Obtain a representative sample of the acrylic polymer waterproofing material.
    2. Particle Size Measurement: Analyze particle sizes via sieving or microscopic examination.
    3. Separation: Pass the sample through a sieve with openings matching the defined threshold to isolate coarse particles.
    4. Quantification: Weigh or count the coarse particles retained on the sieve to determine their proportion.
  • Importance: This test ensures material uniformity by detecting oversized particles that could compromise performance.

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?Which type and size of wire gauze is specified for the test?

Per IS 13435 Part 2, the wire gauze required for testing is:

  • Material: Stainless steel
  • Mesh Size: 180 mesh, conforming to IS 460 Part 1:1985

Additional points:

  • The gauze must be cleaned and degreased prior to use.
  • It is folded into a four-layer cone shape for the test.
  • IS 460 Part 1 details the specifications for wire cloth sieves.

Specification Summary:

ParameterDetails
Wire gauze materialStainless steel
Mesh size180 mesh
Reference standardIS 460 (Part 1): 1985

This ensures consistency and precision in performing residue tests.

?How is the sample prepared and diluted before testing?

As per IS 13435 Part 2, sample preparation involves:

  • Weighing approximately 100 grams of the sample with an accuracy of ±0.1 grams.
  • Diluting the sample with distilled water if necessary to meet concentration requirements.
  • Utilizing distilled water as the reagent to prevent contamination.
  • Following procedures outlined in Part 1 of IS 13435 for solid content determination.

This approach guarantees consistent sample concentration for accurate testing.

?What equipment and accuracy standards are required for weighing?

According to IS 13435 Part 2, weighing equipment and precision criteria include:

  • Employing a laboratory balance with a precision of 0.01 grams for accurate measurement.
  • Weighing around 100 grams of the sample with ±0.1 grams accuracy.
  • Using distilled water for any necessary dilutions.

Summary:

EquipmentAccuracy Requirement
Laboratory balance0.01 g
Sample weighing±0.1 g

These standards minimize measurement errors and enhance test reliability.

?How are the test results calculated and reported according to IS 13435 Part 2?

Under IS 13435 Part 2 (1992), calculation and reporting of test results require:

  • Rounding the final measured or computed values according to IS 2:1960 - Rules for rounding numerical values.
  • Ensuring consistency and accuracy in reporting coarse particle content.
  • Rounding is based on the digit immediately following the last significant figure:
    • If the digit is 5 or higher, round up.
    • If less than 5, round down.

Reporting Process:

StepDescription
1. Obtain raw valuePerform test and record measurements
2. Apply rounding rulesUse IS 2:1960 for final value rounding
3. Present final valueInclude rounded value in the report

This method standardizes results presentation and comparability.

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