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Specifications for Dense Graded Bituminous Mixes
2009 Edition

IRC 111:2009 outlines the standards and criteria for dense graded bituminous mixtures utilized in Indian road building projects. It details the specifications for materials, mix design, execution methods, and quality assurance procedures applicable to Dense Bituminous Macadam (DBM), Semi-Dense Bituminous Concrete (SDBC), and Bituminous Concrete (BC) mixes. This code is indispensable for professionals engaged in the design, supply, and implementation of robust bituminous pavement layers.

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What This Standard Covers

IRC 111:2009 outlines the standards and criteria for dense graded bituminous mixtures utilized in Indian road building projects. It details the specifications for materials, mix design, execution methods, and quality assurance procedures applicable to Dense Bituminous Macadam (DBM), Semi-Dense Bituminous Concrete (SDBC), and Bituminous Concrete (BC) mixes. This code is indispensable for professionals engaged in the design, supply, and implementation of robust bituminous pavement layers.

Who Uses This Standard

  • Highway pavement design engineers
  • Specialists in pavement materials
  • Road construction contractors
  • Quality assurance inspectors
  • Road maintenance professionals
  • Suppliers of bitumen and aggregates
  • Laboratory testing technicians

Key Topics Covered

Classification and use of dense graded bituminous mixtures
Material specifications for aggregates, bitumen, and mineral fillers
Procedures for mix design including the Marshall method
Aggregate gradation and bitumen proportion requirements
Application of viscosity-graded and modified bitumen types
Techniques for preparing and laying bituminous pavement layers
Compaction and rolling standards
Criteria for surface finish and texture
Quality control testing such as tensile strength ratio and density verification
Laboratory and field testing methodologies and apparatus
Moisture susceptibility assessment and anti-stripping measures
Trial laying and acceptance standards
Layer thickness and joint offsetting for multi-layer pavement construction

Table of Contents

1Overview

Introduction to IRC 111 - Essential Formulas, Tables & Guidelines


1. Calculation of Maximum Theoretical Specific Gravity (Gmm) - ASTM D2041

Used for determining air voids and compaction objectives:

Formula (Vacuum Bowl Method)Explanation
Gmm = A / (D + A - E)A = dry mass of sample (g) <br> D = combined mass of lid, bowl, and water (g) <br> E = combined mass of lid, bowl, sample, and water (g)

2. Marshall Compaction Procedure

  • Target Air Voids: 7.0 ± 0.5%
  • Compaction: Adjust number of blows per side (initial ~10 blows)
  • Specimens: Six total, divided into two groups for dry and conditioned testing

3. Indirect Tensile Strength (ITS) Calculation

Tensile strength (St) in kPa is computed as:

[ St = \frac{2000 \times P}{t \times d} ]

  • P: Maximum load applied (N)
  • t: Thickness of specimen (mm)
  • d: Diameter of specimen (mm)

4. Tensile Strength Ratio (TSR) Formula

[ TSR = \frac{S_2}{S_1} ]

  • (S_1): Average tensile strength of dry specimens (kPa)
  • (S_2): Average tensile strength of conditioned specimens (kPa)

5. Summary of Mix Requirements (Table 8)

PropertyViscosity-Grade BitumenModified Bitumen (Hot Climate)Test Standard
Compaction Blows75 blows per face75 blows per faceMS-2, ASTM D2041
Air Voids (%)3-5-MS-2
Bitumen Filled Voids (%)-65-75MS-2
Marshall Quotient2-52.5-
2Scope and Application

Scope of IRC 111 for Dense Graded Bituminous Mixtures

Important Highlights from Clause 2.2:

  • Dense graded bituminous mixes comprise mineral aggregates blended with bituminous binders.
  • These mixes are produced in hot mix plants and laid using mechanical pavers.
  • Primarily used for binder and wearing courses on highway pavements.
  • The binder course is the intermediate layer between base and wearing courses.

Types of Dense Graded Bituminous Mixes (Based on Table 1):

Mix TypeIntended UseNumber of LayersThickness per Layer (mm)
Dense Bituminous Macadam (DBM)Base/Binder course or overlay for strengtheningSingle or multiple50 - 100
Semi-Dense Bituminous Concrete (SDBC)Wearing courseSingle25 - 40
Bituminous Concrete (BC)Wearing courseSingle25, 40 or 50

Aggregate Gradation and Bitumen Content (Excerpt from Table 7):

  • Nominal maximum aggregate sizes differ per mix: DBM (37.5 mm), SDBC (13.2 mm), BC (19 mm).
  • Bitumen content typically ranges between 4% and 5.4% depending on the mix.

Summary Diagram (Mermaid.js):

graph TD
    A[Dense Graded Bituminous Mixes] --> B(DBM)
    A --> C(SDBC)
    A --> D(BC)
    B --> E[Base/Binder Course]
    C --> F[Wearing Course]
    D --> G[Wearing Course]
    E --> H[Layer Thickness: 50-100 mm]
    F --> I[Layer Thickness: 25-40 mm]
    G --> J[Layer Thickness: 25/40/50 mm]

This section assists in selecting appropriate mix types, layer thicknesses, and layers count in highway pavement design as per IRC 111.

3Material Specifications

Material Requirements as per IRC 111

1. Fine Aggregates (Clause 3.3.1)

  • Must pass through 2.36 mm sieve and be retained on 0.075 mm sieve.
  • Natural sand is prohibited in binder and wearing courses; permitted up to 50% in base courses.
  • Aggregates should be clean, hard, durable, dry, and free from dust or harmful substances.
  • Sand Equivalent value should be minimum 50 (IS: 2720 Part 37).
  • Plasticity Index must not exceed 4 for particles passing 0.425 mm sieve (IS: 2720 Part 5).

2. Coarse Aggregate Characteristics (Refer Table 5)

PropertyMaximum/Minimum LimitTesting Standard
Cleanliness (passing 0.075 mm)Maximum 5%IS: 2386 Part I
Flakiness and Elongation IndexMax 35% combinedIS: 2386 Part I
Los Angeles Abrasion ValueBC: Max 30%, Others: 35%IS: 2386 Part IV
Aggregate Impact ValueBC: Max 24%, Others: 27%IS: 2386 Part IV
Polished Stone ValueMinimum 55IS: 2386 Part IV
Soundness (5 cycles)Sodium Sulfate: Max 12%IS: 2386 Part V
Magnesium Sulfate: Max 18%
Water AbsorptionMaximum 2%IS: 2386 Part III
Bitumen CoatingMinimum 95% coating retainedIS: 6241
Retained Tensile StrengthMinimum 80% (use anti-stripping agents if below)AASHTO 283

3. Maximum Specific Gravity (Gmm) Calculation (Clause 24.2.2010)

  • Bowl Method Formula:

[ G_{mm} = \frac{A}{D + A - E} ]

  • Flask Method Formula:

[ G_{mm} = \frac{A}{D + A - E} ]

Where:

  • (A) = Dry mass of sample (g)
  • (D) = Mass of lid and container with water (g)
  • (E) = Mass of lid, container, sample with water (g)
4Mix Design

Key Points in Mix Design According to IRC 111

1. Fines to Bitumen Ratio (Clause 3.5.4)

  • Ratio of fines to bitumen by weight of total mix should be between 0.6 and 1.2 for all mixes listed in Table 7.

2. Job Mix Formula (JMF) Details (Clauses 4.3 & 4.3.1)

The JMF should specify:

  • Material Information:
    • Source and origin of all constituent materials.
    • Proportions of each material.
  • Binder Details:
    • Type and percentage of binder by total mix weight.
  • Aggregates:
    • Percentages of coarse aggregate, fine aggregate, and mineral filler (including filler).
    • Precise percentage passing each sieve size for the combined gradation.
    • Individual grading curves and proportions for each aggregate size fraction.
  • Batching Information:
    • Weights of each aggregate type and bitumen per batch (for batch plants).
  • Test Data:
    • Aggregate physical properties results.
  • Mixing and Compaction Temperatures:
    • Specified temperatures for mixing and compacting.

3. Aggregates Blending (Clause 4.3.1)

  • Blending of multiple aggregate sizes is carried out by weight to meet the target gradation.
  • Laboratory mix design defines gradation percentages per sieve size.
  • These blending proportions are critical for field production.

Summary Table for Fines to Bitumen Ratio

ParameterAcceptable Range
Fines to Bitumen Ratio0.6 to 1.2

flowchart TD
    A[Lab Mix Design] --> B[Determine Sieve-Wise Proportions]
    B --> C[Calculate Weight-Based Blending Ratios]
    C --> D[Prepare Job Mix Formula]
    D --> E[Field Implementation]
    E --> F[Batch Mixing and Compaction]

This sequence ensures compliance with gradation and binder content for optimal durability and performance.

5Construction Practices

IRC 111 Guidance on Construction Procedures and Quality Assurance

Overview of Construction Operations (Clause 5)

  • Emphasizes proper placement of dense graded bituminous layers in base, binder, and wearing courses.
  • Critical to maintain temperature control, proper mixing, placing, and compaction techniques.

Quality Control Tests and Their Frequency (Table 13, Clause 6.4.1)

Test ParameterFrequencyReference Standard
Binder QualityPer lot batchIS:73 / IRC:SP:53
Aggregate Impact Value / LA AbrasionOnce per 350 m³ per source-
Flakiness IndexOnce per 350 m³ per source-
Soundness Test (Na₂SO₄ & MgSO₄)Once per source-
Water AbsorptionOnce per source-
Sand Equivalent TestOnce per source-
Plasticity IndexOnce per source-
Polished Stone ValueOnce per source-
Percentage of Fractured FacesOnce per 350 m³ (for crushed gravel)-
Mix GradationOne set per 400 tons (minimum 2/day)-
Stability and Voids AnalysisThree tests per 400 tons (minimum 2/day)-
Temperature (Binder, Aggregate, Mix)At regular intervals-
Binder ContentOne set per 400 tons (minimum 2/day)-
Rate of SpreadAfter every 5 truck loads-
Density of Compacted LayerOne test per 700 m²-

Important Notes:

  • Temperature control during mixing and paving is essential for workability.
  • Stability and voids tests confirm durability.
  • Frequent sampling guarantees consistent quality and compaction.

flowchart TD
    A[Material Acquisition] --> B[Quality Testing]
    B --> C[Mix Design]
    C --> D[Mixing and Heating]
    D --> E[Placement and Spreading]
    E --> F[Compaction]
    F --> G[Quality Control Testing]
    G --> H[Final Approval]

This systematic approach aligns construction with IRC 111 requirements.

6Quality Control and Limits

Control Measures for Dense Graded Bituminous Mixes as per IRC 111

Key Tests and Their Frequencies (Clause 6 & Table 13)

ParameterFrequency / Limits
Binder QualityTested per lot according to IS:73 / IRC:SP:53
Aggregate Impact / LA AbrasionOne test per 350 m³ per source and after quality changes
Flakiness IndexOne test per 350 m³ per source and after changes
Soundness (Sodium & Magnesium Sulfate)One test per source and after changes
Water AbsorptionOne test per source and on quality change
Sand EquivalentOne test per source and on quality change
Plasticity IndexOne test per source and on quality change
Polished Stone ValueOne test per source and on quality change
Percentage of Fractured FacesOne test per 350 m³ for crushed gravel
Mix GradationOne set per 400 tons, minimum 2 daily tests per plant
Stability & Voids AnalysisThree tests per 400 tons, minimum 2 daily tests per plant
Temperature (Binder, Aggregate, Mix)Regular intervals, ±10°C tolerance
Binder ContentOne set per 400 tons, minimum 2 daily tests, ±0.3% tolerance
Rate of SpreadAfter every 5 truckloads
Density of Compacted LayerOne test per 700 m²

Allowable Deviations from Job Mix Formula (Table 9)

Material Size (mm)DBM Allowable DeviationSDBC / BC Allowable Deviation
≥19±8%±7%
13.2 / 9.5±7%±6%
4.75±6%±5%
2.36, 1.18, 0.6±5%±4%
0.3, 0.15±4%±3%
0.075±2%±1.5%
Binder Content (%)±0.3%-
Annex AMoisture Susceptibility Testing Procedure

Moisture Susceptibility Test Method as per IRC 111

Specimen Preparation and Conditioning

  • Compact six specimens using Marshall compactor targeting air voids of 7.0 ± 0.5% (adjust number of blows starting near 10 per side).
  • Split specimens into two groups with approximately equal air void content:
    • Dry Group: Store at room temperature, then soak in water at 25°C for 2 hours before testing.
    • Conditioned Group: Vacuum saturate specimens, wrap in plastic with 10 ml water in sealed bags, freeze at -18 ± 3°C for at least 16 hours, thaw in 60 ± 1°C water bath for 24 hours, then soak at 25°C for 2 hours prior to testing.

Indirect Tensile Strength (ITS) Test

  • Measure specimen thickness (t, mm).
  • Apply diametral load at 50 mm/min using Marshall testing equipment.
  • Calculate tensile strength (St) using:

[ St = \frac{2000 \times P}{t \times d} ]

Where:

  • (P) = Maximum load (N)
  • (t) = Specimen thickness (mm)
  • (d) = Specimen diameter (mm)

Tensile Strength Ratio (TSR)

[ TSR = \frac{S_2}{S_1} ]

  • (S_1): Mean ITS of dry specimens (kPa)
  • (S_2): Mean ITS of conditioned specimens (kPa)
  • A higher TSR indicates superior resistance to moisture damage.

ASTM D2041: Determination of Maximum Theoretical Specific Gravity (Gmm)

  • Used to determine air void content and compaction targets.
  • Involves vacuum saturation of loose mix submerged in water at 25°C.
  • Calculation formula (vacuum bowl under water method):

[ G_{mm} = \frac{A}{A - (C - B)} ]

Where:

  • (A) = Dry sample mass in air (g)
  • (B) = Mass of bowl under water (g)
  • (C) = Mass of bowl plus sample under water (g)

Equipment Summary

  • Marshall compactor for specimen preparation.
Annex BOutline of ASTM D2041 for Specific Gravity Determination

Summary of ASTM D2041 Procedure as per IRC 111 Annex B


Objective:

  • To determine the Theoretical Maximum Specific Gravity (Gmm) of loose bituminous mixtures at 25°C.
  • This value is essential for calculating air voids, binder absorption, and compaction targets.

Required Equipment:

  • Vacuum container (bowl or flask) with ~4000 ml capacity.
  • Vacuum pump capable of achieving residual pressure ≤ 4.0 kPa.
  • Precision balance with 0.1 g accuracy.
  • Water bath maintained at 25 ± 1°C.
  • Manometer or pressure gauge for monitoring vacuum.

Key Equations:

MethodFormulaVariables
Vacuum Bowl Under WaterGmm = A / (A - (C - B))A = dry sample mass (g) <br> B = bowl mass under water (g) <br> C = bowl + sample mass under water (g)
Bowl in Air MethodGmm = A / (D + A - E)A = dry sample mass (g) <br> D = lid & bowl + water mass (g) <br> E = lid, bowl, sample + water mass (g)
Flask MethodGmm = A / (D + A - E)A = dry sample mass (g) <br> D = flask & cover + water mass (g) <br> E = flask, cover, sample + water mass (g)

Procedure Summary:

  • Weigh representative sample (1500-2500 g) and place in vacuum container.
  • Add water at 25°C to cover sample completely.
  • Apply vacuum to remove air bubbles (residual pressure ~3.7 kPa).
  • Maintain vacuum with agitation for 15 ± 2 minutes.
  • Weigh container plus sample submerged or in air as per selected method.
  • Calculate Gmm using corresponding formula.

Application:

  • Gmm values are used to evaluate volumetric properties and compaction requirements for bituminous mixes.

Popular Questions About IRC 111

?What are the specified aggregate grading limits for Dense Bituminous Macadam (DBM), Semi-Dense Bituminous Concrete (SDBC), and Bituminous Concrete (BC)?

Aggregate Gradation Limits for DBM, SDBC & BC (per IRC 111: Clause 3.5, Table 7)

IS Sieve Size (mm)DBM Passing (%)SDBC Passing (%)BC Passing (%)
45100--
37.595-100100-
26.563-9390-100100
19-71-9590-100
13.255-7556-8059-79
9.5-70-9052-72
4.7538-5435-5135-55
2.3628-4224-3928-44
1.18-15-3020-34
0.6--15-27
0.37-219-1910-20
0.15--5-13
0.0752-83-82-8

Key Points:

  • Nominal maximum aggregate sizes vary: DBM (37.5/26.5 mm), SDBC (13.2/9.5 mm), BC (19/13.2 mm).
  • Bitumen content ranges approximately from 4% to 5.4% depending on mix type.
  • Gap grading is avoided; combined gradation should not jump abruptly between sieve sizes.

This ensures a well-graded aggregate framework for strength and longevity in bituminous pavement layers.

?Which types of bitumen are recommended and how is the viscosity grade selected for different climatic conditions?

Recommended Bitumen Types and Selection of Viscosity Grades (IRC 111)

  • Bitumen must conform to IS:73 (viscosity-graded paving bitumen) or modified bitumen standards as per IS:15462.
  • Selection of Viscosity-Graded (VG) Bitumen depends on climate and traffic loading:
Viscosity GradePenetration RangeTypical Application Area
VG-40 (40-60)High stress zones (e.g., intersections, toll plazas)
VG-30 (50-70)Predominant regions with normal climate
VG-20 (60-80)Cold climates and high altitude areas (Northern India)
VG-10 (80-100)Very cold regions and for spraying applications
  • Selection Chart (based on climatic temperatures):
Lowest Daily Mean Temp (°C)Highest Daily Mean Temp (°C)Recommended VG Grade
> -10< 20VG-10
> -1020 to 30VG-20
> -10> 30VG-30
≤ -10< 20VG-10
≤ -1020 to 30VG-10
≤ -10> 30VG-20
  • For modified bitumen, consult Table 4 for Polymer Modified Bitumen (PMB), Natural Rubber Modified Bitumen (NRMB), and Crumb Rubber Modified Bitumen (CRMB) grades suited to temperature ranges.
  • In areas with more than 2000 commercial vehicles per lane per day and temperatures over 40°C, VG-40 or equivalent modified bitumen is advised.

Summary:

  • Gather local climatic data (highest and lowest daily mean temperatures).
  • Choose VG grade accordingly.
  • Use modified bitumen grades where specified.
  • Ensure bitumen complies with IS standards and contract requirements.
?What laboratory procedures are prescribed for designing the bituminous mix using the Marshall Method?

Laboratory Procedures for Bituminous Mix Design Using the Marshall Method (IRC 111)

  1. Specimen Preparation:

    • Use 100 mm diameter specimens for maximum aggregate sizes ≤ 26.5 mm.
    • For aggregate sizes > 26.5 mm, employ 150 mm diameter specimens (Modified Marshall Method per Asphalt Institute MS-2 and ASTM D5581).
    • Compact specimens with 75 blows on each face.
  2. Testing:

    • Conduct Marshall Stability test at 60°C with a loading rate of 50 mm/min.
    • Measure:
      • Stability (in kN)
      • Flow (in mm)
      • Compute Marshall Quotient = Stability / Flow.
    • Determine:
      • Air voids percentage (target 3-5%)
      • Voids Filled with Bitumen (VFB), typically 65-75% for modified bitumen mixes.
      • Voids in Mineral Aggregate (VMA) based on nominal maximum aggregate size (see Table 8).
  3. Adjustments for Modified Marshall Method (for large aggregates):

    • Multiply minimum stability value by 2.25.
    • Multiply flow values by 1.5.
  4. Additional Tests:

    • Indirect Tensile Strength tests before and after vacuum saturation and freeze-thaw cycles to assess stripping potential (see Annex A).
    • Ensure at least 95% of aggregate particles are coated with bitumen (IS:6241).

Extract from Table 8

PropertyTypical Value / Range
Compaction Blows75 blows per face
Stability (kN)As per binder and aggregate size, multiplied by 2.25 if large aggregate
Flow (mm)2-4 typical; multiplied by 1.5 for large aggregate
Air Voids (%)3-5
VFB (%)65-75 (for modified bitumen)
Marshall Quotient2-5

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This process ensures the mix design meets durability and performance requirements.

?How is moisture susceptibility tested and what anti-stripping additives are recommended?

Moisture Susceptibility Testing and Recommended Anti-Stripping Measures (IRC 111 Annex A)

  • Prepare six specimens compacted using the Marshall compactor to achieve air voids of 7.0 ± 0.5%.

  • Divide specimens into two equal groups: dry and conditioned.

  • Dry group is soaked at 25°C for 2 hours, then tested for indirect tensile strength (ITS).

  • Conditioned group undergoes vacuum saturation, then is frozen at -18°C for at least 16 hours, thawed in 60°C water for 24 hours, soaked at 25°C for 2 hours, and tested for ITS.

  • Calculate tensile strength (St) using:

    [ St = \frac{2000 \times P}{t \times d} ]

    where:

    • (P) = maximum load (N)
    • (t) = specimen thickness (mm)
    • (d) = specimen diameter (mm)
  • Tensile Strength Ratio (TSR) is computed as:

    [ TSR = \frac{S_2}{S_1} \times 100% ]

    where:

    • (S_1) = average ITS of dry specimens
    • (S_2) = average ITS of conditioned specimens
  • Minimum acceptable TSR is 80%; lower values indicate susceptibility to moisture damage.


Anti-Stripping Additives:

  • Commonly used hydrated lime as mineral additive.
  • Liquid anti-stripping agents such as amines or proprietary chemicals added to bitumen.
  • Additives are recommended if TSR falls below 80% to enhance adhesion and durability.

Test Procedure Diagram

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This procedure evaluates resistance to moisture-induced damage in bituminous mixes.

?What are the compaction and rolling requirements to ensure proper density and surface finish?

Compaction and Rolling Specifications as per IRC 111

  • Initial Rolling: Employ a steel wheel roller weighing 8-10 tonnes (dead weight or vibratory) immediately after surface irregularities are remedied.
  • Intermediate Rolling: Use an 8-10 tonnes steel wheel or vibratory roller, or a pneumatic roller weighing 12-15 tonnes with tire pressure ≥ 0.56 MPa.
  • Final Rolling: Use a smooth wheel roller of 6-8 tonnes until roller marks vanish and the prescribed density is attained.
  • Rolling Pattern and Overlap: Roll longitudinally as close as possible behind the paver; overlap passes by at least one-third of the rear roller width or 300 mm for pneumatic rollers.
  • Rolling Speed: Maintain speed ≤ 5 km/h, and avoid stationary rolling on uncompacted pavement.
  • Moistening of Roller Wheels: Keep wheels moist to prevent bituminous mix adhesion but avoid water pooling.
  • Temperature Control: Compaction must commence promptly after laying and complete before the mix temperature drops below the minimum rolling temperature specified (refer Table 10).
  • Density Requirements: Achieve a final compacted layer density of at least 92% of the theoretical maximum specific gravity (Gmm) determined by ASTM D2041 (using 150 mm diameter cores).
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These guidelines ensure the pavement attains adequate density, smooth surface finish, and long-lasting performance.

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