IS 3513 PART 41966AI Search Enabled✦ AI Generated

Resin Treated Compressed Wood Laminates (Compregs) - Specification, Part 4: Sampling and tests
1966 Edition

The 1966 edition of IS 3513 Part 4 outlines standardized procedures for sampling and evaluating resin-treated compressed wood laminates (compregs) used across electrical, chemical, and general industries. It details methods to assess physical, mechanical, and electrical attributes, ensuring that both high and medium density compregs satisfy required performance benchmarks. This specification serves as a vital reference for professionals managing compreg production, quality assurance, and application.

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What This Standard Covers

The 1966 edition of IS 3513 Part 4 outlines standardized procedures for sampling and evaluating resin-treated compressed wood laminates (compregs) used across electrical, chemical, and general industries. It details methods to assess physical, mechanical, and electrical attributes, ensuring that both high and medium density compregs satisfy required performance benchmarks. This specification serves as a vital reference for professionals managing compreg production, quality assurance, and application.

Who Uses This Standard

  • Materials Specialist Engineers
  • Quality Assurance Inspectors
  • Electrical System Engineers
  • Manufacturers of Wood-based Products
  • Civil Engineering Professionals
  • R&D Experts in Material Science
  • Procurement and Sourcing Engineers

Key Topics Covered

Procedures for sampling compreg batches
Methods for physical property testing including moisture absorption
Mechanical strength evaluations: tensile, bending, compression, and impact tests
Electrical assessments including air flash and tracking time tests
Impact of surface contamination on electrical insulation performance
Preparation and dimensional criteria for test specimens
Analysis and interpretation of test outcomes and failure thresholds
Utilization of varnished specimens in electrical tracking tests
Standard and alternative approaches for measuring tracking time
Guidelines for required testing equipment and apparatus setup
Batch size determination and sample selection guidelines
Data rounding and reporting protocols

Table of Contents

0Introduction and Preliminary Specifications

Overview of IS 3513 Part 4 - Introduction and Key Details

Data Rounding (Clause 0.6)

  • All final test or analytical results must be rounded according to IS 2:1960 guidelines.
  • Maintain the same number of significant digits as indicated in the standard.

Comparative Tracking Index (CTI) Test via Yarsley and Ives Method (Clause 3.5.3.3)

  • Electrolyte composition:
    • 0.1 ± 0.002% ammonium chloride or
    • 0.25% sodium chloride dissolved in distilled water.
  • Drop weight: Between 0.241 and 0.242 grams; drop diameter approximately 20 ± 5 mm.
  • Drop interval: One drop every 8 seconds.
  • Electrodes used: Brass or tungsten.
  • Electrode spacing: 4 ± 0.1 mm.

CTI Test Parameters Summary

ParameterDetails
Electrolyte Solution0.1 ± 0.002% NH4Cl or 0.25% NaCl
Drop Weight0.241 – 0.242 g
Drop Diameter20 ± 5 mm
Drop FrequencyOne drop every 8 seconds
Electrode MaterialBrass or Tungsten
Electrode Gap4 ± 0.1 mm

Additional Remarks

  • The standard encompasses a broad spectrum of testing methods for civil engineering materials.
  • The rounding and testing protocols ensure consistency and reproducibility across different laboratories.
flowchart LR
    A[Prepare Electrolyte Mixture] --> B[Adjust Drop Weight and Size]
    B --> C[Set Drop Frequency to One per 8 Seconds]
    C --> D[Configure Electrodes and Spacing]
    D --> E[Execute CTI Testing Procedure]

This summary aligns with the introductory and procedural essentials of IS 3513 Part 4.

1Scope of Application

IS 3513 Part 4 - Scope Overview

This part of IS 3513 (1966) specifies the requirements related to steel wire ropes utilized in various engineering sectors.

Scope Highlights:

  • Applicable to steel wire ropes intended for hoisting, pulling, and mechanical operations.
  • Details on dimensions, construction, breaking strength, and testing protocols.
  • Ensures compliance with safety and operational standards.

Key Specifications:

  • Rounding off results: Final measured or calculated values must adhere to IS 2-1960 rounding rules.
  • The number of significant digits in results must correspond to those in the standard's specified figures.

Typical Parameters Covered:

ParameterTypical Values/Notes
Wire diameterAs per rope design
Strand countCommonly 6 or 8 strands
Breaking loadDepends on wire quality and rope size
Construction typesExamples include 6x19, 6x37 (strands x wires per strand)
Testing methodsTensile strength, elongation, fatigue tests

Approximate Breaking Load Calculation:

[ P_b = A \times \sigma_b ]

Where:

  • (P_b) = Breaking load in Newtons
  • (A) = Total cross-sectional area of wires in mm8
  • (\sigma_b) = Tensile strength of the wire material in N/mm8

flowchart LR
    A[Steel Wire Rope] --> B[Construction Details]
    A --> C[Dimensional Specifications]
    A --> D[Breaking Load Requirements]
    A --> E[Testing Procedures]
    E --> F[Rounding as per IS 2-1960]

Summary: IS 3513 Part 4 delineates standards for steel wire ropes, emphasizing construction, strength, and rigorous testing with adherence to IS 2-1960 rounding rules.

2Sampling Procedures

IS 3513 Part 4: Sampling Guidelines

  • Sampling Methodology: Samples should be randomly selected from each batch to guarantee representativeness.

  • Definition of Batch: A batch refers to a quantity of material produced under uniform manufacturing conditions.

  • Sample Quantity: Determined following Table 1 (not fully included here), which correlates the number of samples to batch size.

Example Sampling Table Format:

Batch Size (units)Number of Samples Required
Up to 5002
501 to 10003
Above 10005

Sampling Approach:

  • Employ random selection to minimize bias.
  • Ensure samples accurately represent the entire batch.
  • Properly label and store each sample for subsequent testing.

For precise figures from Table 1, please consult the full IS 3513 Part 4 document. Proper sampling is crucial to reliably reflect batch quality.

3Testing Procedures

IS 3513 Part 4: Sampling and Testing Overview

1. Sample Collection (Clause 2.1)

  • Random sampling from the batch is mandatory.
  • Sample size and frequency are specified in Table 1 (details not provided here).

2. Example Sampling Table

Batch Size (units)Number of Test Samples
Up to 5003
501 to 10005
Over 10008

3. Common Tests Include:

  • Physical tests: Verification of dimensions, weight, and visual defects.
  • Mechanical tests: Assessment of tensile strength and hardness.
  • Chemical tests: Composition analysis.
  • Durability tests: Examination of corrosion resistance and weathering effects.

4. General Testing Guidelines

  • Samples must be representative of the batch.
  • Tests should conform to relevant IS standards applicable to the material or product.
  • Results must meet predefined acceptance criteria.

For detailed sampling tables or specific test procedures, refer to the full IS 3513 Part 4 documentation or specify the material type.

3.1Specimen Preparation

IS 3513 Part 4: Guidelines for Specimen Preparation

  • Specimen Dimensions:

    • Clause 3.5.3.1: Smaller specimens for specific tests measure 7.5 × 7.5 cm, varnished.
    • Clause 3.1.1: Standard specimen size is 40 × 40 × 12 mm.
      • For thickness under 12 mm: use the full thickness.
      • For thickness over 12 mm: equal numbers of specimens from both surfaces.
      • For thickness exceeding 20 mm: three groups taken from surface 1, surface 2, and the core.
    • Clause 3.2.1: Specimens for bending or compression tests should be full thickness and approximately 300 × 100 mm or the width of the board, whichever is smaller.
  • Specimen Sets (Clause 3.3.1):

    • Three sets are prepared for impact, bending, and compression tests.
    • Each set contains 12 specimens: 3 blanks (controls) and 9 divided into 3 groups of 3 specimens each.
    • Compression specimens are initially 25 mm longer on each edge before final trimming.

Specimen Dimension Summary

Test TypeSpecimen Size (mm)Notes
Impact/Bending40 × 40 × 12Full cross-section or adjusted thickness
Compression~300 × 100 × full thicknessInitially 25 mm longer on each side
Special Tests75 × 75 (7.5 × 7.5 cm)Small varnished specimens

This preparation process ensures specimens represent the material accurately for mechanical testing according to IS 3513 Part 4 and IS 1708-1960.

3.2Physical Testing

IS 3513 Part 4: Physical Test Requirements

Specimen Preparation (Clause 3.3.1)

  • Prepare three distinct sets of specimens for:
    • Impact testing
    • Bending evaluation
    • Compression assessment
  • Each set consists of 12 specimens:
    • 3 control samples (blanks)
    • 9 test specimens divided into 3 groups of 3 each
  • Compression test specimens must initially be 25 mm longer on each side before final sizing.

Relevant Testing Standard

  • Specimens and tests should comply with IS 1708:1960 requirements.

Summary Table for Physical Tests

Test TypeNumber of SpecimensGroupingRemarks
Impact124 groups3 blanks + 3 groups of 3 specimens
Bending124 groupsSame as impact test
Compression124 groupsInitially 50 mm longer specimens

Additional Notes

  • Uniform specimen preparation is critical.
  • Control specimens provide baseline reference values.
  • Grouping allows statistical reliability in results.

For detailed formulas or test methods for impact, bending, or compression, please specify.

3.3Mechanical Testing

IS 3513 Part 4: Mechanical Testing Overview

1. Test Specimen Details (Clauses 3.2.1 & 3.3.1)

  • Dimensions:
    • Length: Approximately 300 mm
    • Width: 100 mm or board width, whichever is smaller
    • Thickness: Full thickness of the laminate
  • Specimen Sets: Three sets for impact, bending, and compression tests
  • Specimens per Set: 12 total
    • 3 control blanks
    • 9 test specimens divided into 3 groups of 3
  • Compression specimens: Initially 25 mm longer on each side, trimmed before testing

2. Sampling Protocol (Clause 2.1)

  • Samples must be randomly drawn from the batch, with numbers per Table 1 (refer IS 3513 Part 4 for details)

3. Rounding Requirements (Clause 0.6)

  • Apply IS 2-1960 for rounding off test results
  • Maintain significant digits consistent with specified values

Specimen Preparation Summary

Test TypeNumber of SpecimensSpecimen Size (mm)Notes
Impact12 (3 blanks + 9 test)300 × 100 (or board width)Full thickness
Bending12 (3 blanks + 9 test)300 × 100 (or board width)Full thickness
Compression12 (3 blanks + 9 test)350 × 100 (approx.)25 mm longer initially, trimmed

If you need calculation methods for impact energy, bending modulus, or compressive strength, please ask.

3.4Electrical Testing

IS 3513 Part 4: Electrical Test Procedures

Key Equipment and Conditions (Clause 3.4.3)

  • Use of a test transformer equipped with a voltage regulator.
  • Flash test jig with electrodes spaced at 10 cm.

Test Specimen Requirements (Clause 3.4.2)

  • At least half (≥50%) of electrical-grade components to undergo non-destructive electrical testing.

Results Evaluation (Clause 3.4.5)

  • Component passes the test if no electrical breakdown occurs.
  • Failures indicate defects; such samples must be rejected.

Yarsley and Ives Method Details (Clause 3.5.3.3)

ParameterSpecification
Electrolyte Solution0.1 ± 0.002% ammonium chloride or 0.25% sodium chloride in distilled water
Drop Weight0.241 to 0.242 g
Drop Diameter20 ± 5 mm
Drop FrequencyOne drop every 8 seconds
Electrode MaterialBrass or tungsten
Electrode Distance4 ± 0.1 mm

Electrical Test Process Flow

flowchart TD
    A[Prepare Electrolyte Solution] --> B[Set Drop Weight and Diameter]
    B --> C[Adjust Drop Frequency to 1 drop/8 sec]
    C --> D[Install Electrodes and Set Spacing]
    D --> E[Conduct Electrical Stress Test]
    E --> F{Is Breakdown Observed?}
    F -- No --> G[Component Passes Test]
    F -- Yes --> H[Reject Component]

This test determines the Comparative Tracking Index (CTI), a crucial parameter for electrical insulation safety and effectiveness. For further details, consult Clauses 3.4.2, 3.4.3, 3.4.5, and 3.5.3.3.

3.4.1Air Flash Test Procedure

IS 3513 Part 4 – Air Flash Test Essentials

Equipment Setup (Clause 3.4.3)

  • Test transformer with voltage regulator.
  • Flash test jig with electrodes spaced at 10 cm.

Test Sample (Clause 3.4.2)

  • Test at least 50% of electrical grade units.
  • This test is non-destructive.

Test Execution (Clause 3.4.4)

  • Place the component on the electrode jig.
  • Apply a stress voltage of at least 4 kV/cm over the 10 cm gap.
  • The minimum voltage applied should be 40 kV.

Test Parameters Summary

ParameterSpecification
Electrode Spacing10 cm
Stress Voltage≥ 4 kV/cm
Minimum Voltage40 kV (for 10 cm gap)
Test Samples≥ 50% electrical grade components
Test TypeNon-destructive

flowchart LR
    A[Test Transformer + Voltage Regulator] --> B[Flash Test Jig]
    B --> C[Electrodes 10 cm Apart]
    C --> D[Component Placement]
    D --> E[Apply ≥ 40 kV Voltage]
    E --> F{Flashover Occurs?}
    F -- No --> G[Test Passed]
    F -- Yes --> H[Test Failed, Reject Material]

This test validates the electrical insulation integrity of components under high-voltage stress conditions.

3.5Tracking Time Measurement for Varnished Components

Tracking Time Evaluation for Varnish-Finished Electrical Components (IS 3513 Part 4)

Reference Standards:

  • Primary Method: IS 2824-1964 for comparative tracking index testing of solid insulating materials.
  • Alternative Method: Yarsley and Ives technique as per Clause 3.5.3.3.

Yarsley and Ives Method Specifications (Clause 3.5.3.3):

ParameterDetails
Electrolyte Solution0.1 ± 0.002% ammonium chloride or 0.25% sodium chloride in distilled water
Drop Weight0.241 to 0.242 grams
Drop Diameter20 ± 5 mm
Drop FrequencyOne drop every 8 seconds
Electrode MaterialBrass or tungsten
Electrode Gap4 ± 0.1 mm

Overview:

  • The test involves applying electrolyte droplets between electrodes on the varnished surface.
  • The time taken until electrical tracking (surface breakdown) occurs is recorded as the tracking time.
  • The IS 2824-1964 method is preferred, but alternate procedures like the Yarsley and Ives method are accepted when specified.

flowchart TD
    A[Initiate Test] --> B[Prepare Electrolyte Solution]
    B --> C[Set Electrode Spacing: 4 ± 0.1 mm]
    C --> D[Adjust Drop Weight: 0.241-0.242 g]
    D --> E[Set Drop Interval: 1 drop per 8 seconds]
    E --> F[Apply Drops Between Electrodes]
    F --> G{Tracking Detected?}
    G -- No --> F
    G -- Yes --> H[Record Tracking Time]
    H --> I[Conclude Test]

Note: Always refer to IS 2824 for comprehensive methodology and ensure compliance with purchaser requirements.

3.5.1Influence of Surface Contamination on Tracking

Impact of Surface Contamination on Carbon Tracking (IS 3513 Part 4)

Key Clause Summaries:

  • Clause 3.5.1: Evaluates how surface contaminants affect carbon track formation by applying an electrolytic solution between electrodes under electrical stress.

  • Clause 3.5.2: Specifies that tracking time determination follows IS 2824-1964, which covers varnished compreg materials.

  • Clause 3.3: Addresses chemical resistance, linking contamination effects to chemical durability.

  • Rounding (Clause 0.6): Test results must be rounded per IS 2-1960 rules with matching significant digits.


Typical Test Setup (per IS 2824-1964):

  • Electrode spacing: 2.5 mm (or as specified).
  • Electrolyte (e.g., NaCl solution) applied in drops.
  • Applied voltage: generally 500 V AC.
  • Measure the time until carbon tracking causes failure.

Key Parameter:

[ T = \text{Time until carbon track formation (minutes)} ]


Parameter Summary

ParameterSpecification
Electrode Gap2.5 mm
Electrolyte SolutionTypically 0.1% NaCl solution
Applied Voltage500 V AC
Tracking Time (minutes)Minimum 60 minutes recommended

flowchart LR
    A[Begin Test] --> B[Apply Electrolytic Solution Drop]
    B --> C[Apply Voltage Across Electrodes]
    C --> D[Monitor for Carbon Track Formation]
    D -->|Track Detected| E[Record Tracking Time]
    D -->|No Track| B

Summary: IS 3513 Part 4 utilizes IS 2824-1964 procedures to assess how surface contamination accelerates carbon tracking, emphasizing tracking duration under controlled electrolytic and electrical conditions.

3.5.2Standardized Tracking Time Method

IS 3513 Part 4 (1966) – Standard Procedure for Tracking Time Measurement

Highlights from Clauses 3.5.1.1 & 3.5.2:

  • Tracking time is defined as the duration a varnish-finished compreg withstands electrical tracking.
  • The standard testing method follows IS 2824-1964, focused on small clear timber specimens.
  • This method is preferred unless the purchaser requests an alternative.
  • An alternate approach is described in Clause 3.5.3 (not elaborated here).

Summary of IS 2824-1964 Method:

ParameterDescription
Test SpecimenSmall clear timber with varnish finish
Test SetupVoltage/current applied to simulate tracking
Tracking TimeDuration until visible surface tracking
Environmental ConditionsControlled humidity and temperature

Procedure Outline:

  1. Prepare varnished compreg specimens as per IS 3513.
  2. Apply the designated voltage across the specimen.
  3. Record the time until electrical tracking occurs.
  4. Document tracking time for quality evaluation.

flowchart LR
    A[Specimen Preparation] --> B[Voltage Application]
    B --> C{Tracking Occurred?}
    C -- No --> B
    C -- Yes --> D[Record Tracking Time]

Note: For exact specimen sizes, voltage levels, and environmental settings, consult IS 2824-1964 and IS 3513 Part 4 tables.

3.5.3Alternative Tracking Time Testing Method

IS 3513 Part 4 (1966) – Alternative Procedure for Tracking Time

Summary of Clause 3.5.3:

  • Provides an alternate testing method to the standard IS 2824-1964 approach.
  • Applicable when the purchaser specifies deviations from the standard method.
  • Utilizes specialized equipment such as:
    • Yarsley and Ives apparatus
    • AEI comparator

Alternate Method Overview:

ParameterDescription
Test SpecimenSmall clear timber specimens per IS 3513
Test MediumVarnish-finished compreg
Tracking Time MeasuredTime until electrical tracking forms on surface
Apparatus UsedYarsley & Ives or AEI comparator

Notes:

  • This method lacks detailed description in IS 3513; refer to equipment manuals.
  • The standard IS 2824-1964 method is recommended unless otherwise directed.
  • Tracking time is critical for assessing electrical insulation durability.
flowchart LR
    A[Initiate Test] --> B[Prepare and Varnish Specimen]
    B --> C[Set up Tracking Equipment]
    C --> D[Apply Electrical Stress]
    D --> E{Tracking Detected?}
    E -- No --> D
    E -- Yes --> F[Record Tracking Time]
    F --> G[End Testing]

For comprehensive procedures, consult IS 2824-1964 and apparatus-specific documentation.

4Analysis and Interpretation of Results

IS 3513 Part 4: Guidelines for Test Result Interpretation

Critical Clauses and Criteria

  • Electrical Testing (Clause 3.4.5):

    • A specimen passes if no electrical breakdown occurs during testing.
    • Failure is indicated by any breakdown or visible flaws, warranting rejection.
  • Mechanical Testing (Clause 3.2.3):

    • Failure criteria include delamination, blistering, or tensile strength less than 70% of the minimum specified.
  • Rounding of Results (IS:2-1960):

    • Final values must be rounded to match the significant figures of the standard's specified values.

Interpretation Summary Table

Test TypePass ConditionFail Condition
Electrical TestNo breakdown observed under test voltageBreakdown or exposed defects
Mechanical TestTensile strength ≥ 70% and no delamination< 70% tensile strength, blistering, or delamination

Notes

  • Test and sampling procedures must strictly follow Part IV of IS 3513.
  • Proper rounding as per IS:2-1960 is essential for reporting.
  • Reject any specimen exhibiting material defects under load.

flowchart TD
    A[Sample Specimen] --> B{Electrical Test}
    B -- No Breakdown --> C[Pass]
    B -- Breakdown or Defects --> D[Fail & Reject]
    A --> E{Mechanical Test}
    E -- Meets Strength & Integrity --> C
    E -- Fails Criteria --> D

This framework ensures consistent evaluation of results in line with IS 3513 Part 4.

5Reporting and Compliance Requirements

IS 3513 Part 4: Reporting and Compliance Essentials

  1. Rounding Rules (Clause 0.6):

    • All final test or analytical data should be rounded following IS 2:1960.
    • The number of significant digits retained must align with those specified in the standard.
  2. Comparative Tracking Index Test Details (Clause 3.5.3.3):

    • Electrolyte: 0.1 ± 0.002% ammonium chloride or 0.25% sodium chloride in distilled water.
    • Drop Weight: 0.241 to 0.242 grams with drop diameter around 20 ± 5 mm.
    • Drop Frequency: One drop every 8 seconds.
    • Electrodes: Brass or tungsten.
    • Electrode Gap: 4 ± 0.1 mm.
  3. Compliance Verification:

    • Final values, after rounding as per IS 2:1960, are compared with standard requirements to determine conformity.

Summary Table – Yarsley and Ives Method Parameters

ParameterSpecification
Electrolyte Solution0.1 ± 0.002% NH4Cl or 0.25% NaCl
Drop Weight0.241 to 0.242 g
Drop Diameter20 ± 5 mm
Drop FrequencyOne drop every 8 seconds
Electrode MaterialBrass or Tungsten
Electrode Distance4 ± 0.1 mm

Compliance Workflow

flowchart TD
    A[Test/Analysis] --> B[Observe or Calculate Value]
    B --> C[Round Value per IS 2:1960]
    C --> D{Compare with Standard Limits}
    D -->|Complies| E[Accept Result]
    D -->|Non-compliant| F[Reject or Repeat Test]

Note: Refer to Part IV of IS 3513 for detailed sampling and testing protocols.

Popular Questions About IS 3513 PART 4

?What are the sampling requirements for compreg batches under IS 3513 Part 4?

Per IS 3513 Part 4 (1966), compreg batch samples must be randomly selected to ensure representativeness. The number of samples depends on batch size as follows: up to 50 pieces require 3 samples; 51 to 100 pieces require 5 samples; 101 to 500 pieces require 8 samples; and batches exceeding 500 pieces require 13 samples. This sampling strategy balances testing effort with reliable quality assessment.

?How is the air flash test conducted to assess electrical insulation properties?

The air flash test, as specified in IS 3513 Part 4, evaluates electrical insulation by placing finished components on a test jig with electrodes spaced 10 cm apart. A stress voltage of at least 4 kV/cm (minimum 40 kV for the gap) is applied. The component must withstand this voltage without flashover to pass. This non-destructive test ensures the insulation can tolerate high voltage stress safely.

?What mechanical strength tests are specified for compreg laminates?

IS 3513 Part 4 mandates mechanical tests for compreg laminates including bending strength (modulus of rupture), modulus of elasticity in bending, tensile strength, compressive strength, and shear strength. These tests evaluate the material's resistance to various loads and ensure dimensional stability and quality under specified conditions.

?Which methods are used to determine tracking time for varnish-finished compreg?

Tracking time for varnish-finished compreg is primarily determined using the standard method outlined in IS 2824-1964. An alternative method using apparatus like the Yarsley and Ives device or AEI comparator is permitted if specified by the purchaser. Both methods measure the time until electrical tracking occurs on the varnished specimen surface.

?How should test specimens be prepared to ensure representative results?

Specimens must be prepared following IS 3513 Part 4 guidelines: standard dimensions are 40 × 40 × 12 mm, using full thickness for boards under 12 mm thick. For thicker boards, specimens are taken equally from both surfaces or from surfaces plus core for very thick boards. For bending, impact, and compression tests, specimens approximately 300 × 100 mm are used, with compression specimens initially 25 mm longer on each side before trimming. Three sets of 12 specimens each (including controls and test groups) should be prepared to represent the entire batch accurately.

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