IS 9964 Part 11981AI Search Enabled✦ AI Generated

Recommendations for maintenance and operation of petroleum storage tanks, Part 1:Preparation of tanks for safe entry and work

IS 9964 Part 1 (1981) provides comprehensive recommendations for safely preparing petroleum storage tanks for entry, cleaning, maintenance, and repair. It addresses hazards such as toxic gases, flammable vapors, and physical risks, and outlines procedures for gas freeing, sludge removal, ventilation, and protective measures. This standard is essential for engineers and safety personnel involved in the operation and maintenance of petroleum storage tanks to ensure safe working conditions and compliance with safety protocols.

19Sections
129Clauses Indexed
AI Search Ready
1981Edition
Structural Engineering and structural sectionsCategory
Alternative search terms: IS 9964 Part 1 PDF, IS 9964 Part 1 pdf free download, IS 9964 Part 1 free download pdf, IS9964Part1 PDF, IS-9964-Part-1 PDF, IS 9964 Part 1 1981 PDF, IS 9964 Part 1:1981 PDF, IS 9964 Part 1-1981 PDF, IS 9964 Part 1 (1981) PDF, IS 9964 Part 1 1981 edition PDF, IS 9964 Part 1 edition 1981 PDF

What This Standard Covers

IS 9964 Part 1 (1981) provides comprehensive recommendations for safely preparing petroleum storage tanks for entry, cleaning, maintenance, and repair. It addresses hazards such as toxic gases, flammable vapors, and physical risks, and outlines procedures for gas freeing, sludge removal, ventilation, and protective measures. This standard is essential for engineers and safety personnel involved in the operation and maintenance of petroleum storage tanks to ensure safe working conditions and compliance with safety protocols.

Who Uses This Standard

  • Petroleum Storage Tank Operators
  • Maintenance Engineers
  • Safety Officers
  • Industrial Hygienists
  • Refinery Engineers
  • Environmental Compliance Specialists
  • Tank Cleaning Contractors

Key Topics Covered

Hazards in petroleum tank cleaning
Gas freeing and vapor testing procedures
Safe limits for oxygen and toxic gases
Handling of hydrogen sulphide and leaded gasoline residues
Sludge removal and disposal methods
Ventilation and atmospheric testing
Use of explosion-proof equipment
Precautions for hot work and flame cutting
Protective clothing and respiratory equipment
Inspection checklists for safe tank entry
Disposal and dismantling of tanks
Prevention of spontaneous combustion
Cleaning methods and sludge management
Safety permit and work authorization
Environmental and health safety considerations

Table of Contents

1Scope

IS 9964 Part 1 - Scope Summary & Key Specifications

Scope:

  • Covers design, fabrication, and inspection of atmospheric storage tanks only.
  • Emphasis on safety during tank cleaning and maintenance, especially for tanks with leaded products.

Key Safety & Cleaning Specifications (Clause 19.8 & Appendix A)

  • Tank plates scrap disposal: Must be heated or grit/shot blasted to remove scale and lead dust contamination.
  • Grit/shot blasting: Collect and treat used grit as contaminated; do not reuse.
  • Tank cleaning checklist includes:
    • Hazard review by supervisors.
    • Work permit system adherence.
    • Special precautions for leaded product tanks.
    • Use of respiratory protection and gas testing.
    • Complete removal of hydrocarbons before cleaning.
    • No water introduction until oil temperature < 100°C.
    • Use steam/air pumps preferred over electrical pumps.
    • Prevent vapor contact with ignition sources.
    • No tank entry until all lines blinded and gas readings zero.
    • Stand-by personnel during entry.
    • No entry if vapor concentration > 20% of lower explosive limit.

Important Notes

  • The standard excludes pressurized or vacuum tanks.
  • Safety during cleaning and maintenance is a major focus.
  • Refer to Petroleum Rules 1976 for electrical classification in hazardous areas.

flowchart TD
    A[Start Tank Cleaning] --> B{Hazard Review Done?}
    B -- No --> C[Stop Work]
    B -- Yes --> D[Remove Hydrocarbons]
    D --> E{Oil Temp < 100°C?}
    E -- No --> F[Wait]
    E -- Yes --> G[Gas Testing & Ventilation]
    G --> H{Gas < 20% LEL?}
    H -- No --> F
    H -- Yes --> I[Permit & PPE Ready]
    I --> J[Entry with Stand-by]
    J --> K[Complete Cleaning]
    K --> L[Exit & Seal Tank]

For detailed design formulas and fabrication requirements, refer to other parts of IS 9964 and related IS codes (e.g., IS 803, IS 2825).

2Types of Petroleum Storage Tanks

IS 9964 Part 1 focuses on atmospheric petroleum storage tanks, primarily covering their maintenance and operation.

Types of Petroleum Storage Tanks (per IS 9964 Part 1)

  • Fixed Roof Tanks: Simple, with a rigid roof fixed to the shell.
  • Floating Roof Tanks: Roof floats on the liquid surface to minimize vapor losses (Clause 4.3).
  • Open Top Tanks: No roof, used for certain storage needs.

Key Specifications:

  • Only atmospheric tanks are covered (Clause 1.1.2).
  • Floating roofs reduce vapor losses by eliminating vapor space or keeping it constant.
  • Compliance with Factory Act 1948 and Petroleum Act for safety during maintenance (Clause 3.1).

Typical Formulas (General Reference):

  • Vapor space volume in fixed roof tanks:
    [ V_v = \pi r^2 h_v ] where (r) = tank radius, (h_v) = vapor space height.

  • Floating roof eliminates vapor space, reducing (V_v \to 0).

Summary Table of Tank Types:

Tank TypeRoof TypeVapor LossesApplication
Fixed RoofRigid fixed roofHighGeneral storage
Floating RoofFloating on liquidMinimalVolatile liquids, large tanks
Open TopNoneVery highNon-volatile liquids
flowchart LR
    A[Petroleum Storage Tanks] --> B[Fixed Roof Tanks]
    A --> C[Floating Roof Tanks]
    A --> D[Open Top Tanks]
    C --> E[Minimize Vapor Loss]
    B --> F[Simple Construction]
    D --> G[High Vapor Loss]

For detailed design and maintenance, refer to statutory safety acts and IS 9964 operational clauses.

3Statutory Requirements

IS 9964 Part 1 - Statutory Requirements Summary

Key Statutory References (Clause 3.1)

  • Compliance with Factory Act 1948 and Petroleum Act & associated rules is mandatory for:
    • Cleaning
    • Safe entry
    • Repair & maintenance of petroleum storage tanks.

Tank Cleaning & Safe Entry Checklist (Appendix A, Clause 17.1)

  • Hazard review by supervisors & engineers.
  • Work permit system enforced.
  • Special precautions for tanks with leaded products.
  • Respiratory protection & gas testing equipment in good condition.
  • Complete removal of hydrocarbons before cleaning.
  • Avoid water introduction until oil temperature < 100°C.
  • Use steam/air-driven pumps outside firewalls; follow electrical classification for hazardous areas.
  • Prevent vapor contact with ignition sources.
  • Blind all lines before entry.
  • Entry prohibited if flammable vapor > 20% LEL.
  • Stand-by personnel during tank entry.
  • Ensure zero combustible gas readings before hot work.
  • Confirm no personnel/material inside before sealing tank.

Safety for Scrap Disposal (Clause 19.8)

  • Tank plates safe for scrap only after:
    • Heating (flame cleaning), OR
    • Removal of scale by grit/shot blasting.
  • Collect and treat grit/shot as contaminated if lead dust is present.

Important Safety Limits

ParameterLimit/Requirement
Maximum vapor concentration for entry< 20% of Lower Explosive Limit (LEL)
Oil temperature before water addition< 100°C

Visual Summary: Tank Cleaning Safety Workflow

flowchart TD
    A[Review Hazards] --> B[Work Permit System]
    B --> C[Remove Hydrocarbons]
    C --> D[Check Oil Temp < 100°C]
    D --> E[Gas Testing Equipment Ready]
    E --> F[Blind All Lines]
    F --> G[Check Vapor < 20% LEL]
    G --> H[Entry with Respiratory Protection]
    H --> I[Stand-by Personnel Present]
    I --> J[Perform Cleaning & Repairs]
    J --> K[Confirm Zero Gas Reading Before Hot Work]
    K --> L[Seal Tank]

For detailed procedures and safety compliance, always refer to IS 9964 Part 1 and relevant statutory acts.

4Tank Construction and Roof Types

IS 9964 Part 1 (1981) — Tank Construction & Roof Types

Roof Types & Key Specs

Roof TypeDiameter RangeDescription
Cone Roof TanksUp to 75 mSloped conical roof, common for large tanks.
Umbrella Roof TanksUp to 20 mSegmental plates arched on meridian center lines.
Dome Roof TanksUp to 20 mRoof plates formed with spherically curved sections, self-supporting.
Floating Roof TanksVariableRoof floats on liquid surface to minimize vapor loss.

Important Specifications

  • Umbrella & Dome Roofs: Usually limited to ≤ 20 m diameter due to structural complexity.
  • Floating Roofs: Used to reduce vapor losses by eliminating or maintaining constant vapor space.
  • Safety: For thin roof plates, distribute worker load using planks (Clause 12.5).

Typical Structural Considerations

  • Roof Plate Thickness: Depends on diameter, roof type, and loading.
  • Meridian Arches: Umbrella roofs use segmental arches for self-support.
  • Spherical Curvature: Dome roofs use spherical sections for self-supporting strength.

flowchart LR
    A[Tank Types] --> B[Cone Roof (≤75m)]
    A --> C[Umbrella Roof (≤20m)]
    A --> D[Dome Roof (≤20m)]
    A --> E[Floating Roof (variable)]
    C & D --> F[Self-supporting curved plates]
    E --> G[Minimize vapor loss]

For detailed design, refer to IS 9964 tables for plate thickness, joint design, and wind/snow loads.

5Hazards in Tank Cleaning

Hazards in Tank Cleaning (IS 9964 Part 1)

Key Hazards (Clause 8.1 & 5.2)

  • Physical hazards: slipping, falling objects, falls from roofs, improper scaffolding.
  • Health hazards: exposure to toxic gases, hydrocarbons.
  • Fire hazards: ignition sources from residual vapors.

Tank Cleaning Operations (Clause 9.1)

  1. Preliminary preparations: external inspection, crew training, equipment check.
  2. Control ignition sources: eliminate sparks, static electricity.
  3. Emptying tank: pump out oil, blank off tank.
  4. Vapour-freeing: ventilate to remove hydrocarbon vapors.
  5. Testing: check for hydrocarbon vapors and toxic gases.
  6. Opening and sludge removal: safe entry and disposal.

Important Specifications

  • Testing for vapors: Use calibrated gas detectors; ensure below Lower Explosive Limit (LEL).
  • Ventilation: Continuous forced ventilation until safe atmosphere is confirmed.
  • Safety measures: Use of PPE, harnesses, and safety nets for fall protection.

Summary Table: Hazards & Controls

Hazard TypeKey RiskControl Measures
PhysicalFalls, slipsProper scaffolding, PPE, training
HealthToxic gases, vaporsGas testing, ventilation
FireIgnition of residual vaporsEliminate ignition sources, grounding
flowchart TD
    A[Start Cleaning] --> B[Preliminary Inspection]
    B --> C[Control Ignition Sources]
    C --> D[Empty Tank & Blank Off]
    D --> E[Vapour-Freeing & Ventilation]
    E --> F[Gas Testing]
    F --> G[Safe Entry & Sludge Removal]

Follow strict planning, inspection, and training as per IS 9964 Part 1 for safe tank cleaning.

6Atmospheric Conditions and Safe Breathing Limits

IS 9964 Part 1 (1981) – Atmospheric Conditions & Safe Breathing Limits

Key Specifications:

  • Oxygen Content: Minimum safe oxygen level inside tanks is 19.5% for entry without respiratory equipment (Clause 6.1.3.2).
  • Ventilation: Must ensure removal of flammable/toxic vapors and maintain oxygen above 19.5% (Clause 6.1.4.1).
  • Gas Testing: Use portable, approved meters for:
    • Combustible gas
    • Toxic gas
    • Oxygen levels

Safe Exposure Limits for Aromatic Hydrocarbons (Clause 6.1.1.2):

SubstanceMax Exposure (8 hrs)
Benzene25 ppm
Toluene200 ppm
Xylene200 ppm
  • Special detection methods like gas spectrometry or gas-liquid chromatography are required for aromatic vapors.

Summary Flow for Safe Entry:

flowchart TD
    A[Start: Prepare for Tank Entry] --> B[Ventilate Tank]
    B --> C[Measure Gas Levels]
    C --> D{Oxygen ≥ 19.5%?}
    D -- Yes --> E[Check Toxic & Flammable Vapors]
    D -- No --> F[Continue Ventilation]
    E --> G{Vapors < Safe Limits?}
    G -- Yes --> H[Entry Allowed without Respiratory Gear]
    G -- No --> I[Use Respiratory Equipment or Delay Entry]

Always confirm gas tests before entry to prevent exposure to toxic or flammable atmospheres.

7Sources of Ignition and Static Electricity

IS 9964 Part 1: Sources of Ignition & Static Electricity

Key Points from Clauses 7.1.3, 7.2.1 & 7.3

  • Sources of Ignition:

    • Open flames, sparks from non-explosion-proof electrical tools, defective cords.
    • Lightning and static electricity discharges on liquid surfaces.
    • Pyrophoric iron polysulphide deposits in sour stock tanks can spontaneously ignite on air exposure.
  • Static Electricity Hazards (Clause 7.3):

    • Steam used for gas-freeing tanks can carry charges.
    • Charges on steam nozzles controlled by bonding.
    • Charges may accumulate on insulated metallic objects inside tanks → spark risk.
    • Spark discharge within steam clouds is unsubstantiated.
  • Precautions for Sour Stock Tanks (Clause 7.2.1):

    • Prevent air entry until surfaces are wetted.
    • Keep interior surfaces wet until gas-free.

Practical Specifications & Controls

Hazard SourceControl Measures
Static electricity on liquidsProper bonding & grounding of equipment
Steam gas-freeing chargesBond steam nozzles; ground metallic objects
Pyrophoric iron polysulphidePrevent air entry; keep surfaces wet
Electrical toolsUse explosion-proof fixtures and cords

Static Electricity Control Formula (Bonding Resistance)

To avoid spark generation, bonding resistance ( R_b ) should be low enough:

[ R_b \leq \frac{V_{spark}}{I_{max}} ]

Where:

  • ( V_{spark} ) = Minimum spark voltage (depends on gas mixture)
  • ( I_{max} ) = Maximum allowable leakage current (mA)

flowchart LR
    A[Steam Nozzle] -->|Bonding| B[Grounded Metal]
    B --> C[No Spark Risk]
    A --> D[Steam Charges]
    D --> E[Insulated Metal Object]
    E -->|Charge Accumulation| F[Spark Risk]

Summary: Control static electricity by bonding & grounding, avoid ignition sources, and take special care with sour stock tanks to prevent pyrophoric ignition.

8Physical Hazards

IS 9964 Part 1: Physical Hazards in Tank Cleaning

Key Points on Physical Hazards (Clause 8.1 & related)

  • Physical hazards include:
    • Slipping on wet or oily surfaces
    • Falling objects inside or outside the tank
    • Falling from or through tank roofs
    • Improper scaffolding or support structures

Safety Specifications:

  • Scaffolding: Must comply with safe load capacity and proper anchorage.
  • Fall Protection: Use guardrails, safety nets, or personal fall arrest systems when working at heights.
  • Surface Conditions: Ensure non-slip surfaces or use anti-slip mats.
  • Object Handling: Secure loose objects and tools to prevent falling.

No direct formulas are specified for physical hazards in IS 9964, but general safety design follows:

Hazard TypeControl MeasureReference Standard/Practice
SlippingAnti-slip surfaces, housekeepingIS 14489 (Safety in workplaces)
Falling objectsTool lanyards, barricadesIS 3696 (Safety helmets)
Falls from heightGuardrails, harnessesIS 3521 (Safety nets)
Scaffolding safetyLoad checks, inspectionsIS 3696 (Scaffolding safety)

General Engineering Notes on Fall Protection:

  • Fall arrest force limit: ≤ 6 kN
  • Minimum guardrail height: 1.0 m above working platform
  • Scaffolding load: Designed for at least 4 kN/m² live load
flowchart TD
    A[Physical Hazards] --> B[Slipping]
    A --> C[Falling Objects]
    A --> D[Fall from Height]
    A --> E[Improper Scaffolding]
    B --> F[Anti-slip surfaces]
    C --> G[Secure tools]
    D --> H[Guardrails, harness]
    E --> I[Load checks, inspections]

Summary: Control physical hazards by proper planning, safe scaffolding, fall protection, and housekeeping as per IS 9964 and related IS codes.

9Tank Cleaning Operations

IS 9964 Part 1: Key Points for Tank Cleaning Operations

Major Steps (Clause 9.1)

  1. Preliminary Preparations
    • External tank inspection and area survey
    • Crew training and equipment inspection
  2. Control Ignition Sources
  3. Emptying Tank
    • Pumping and floating oil out
    • Blanking-off tank after oil removal
  4. Vapour-Freeing
  5. Testing for Hydrocarbon Vapour & Toxic Gas
  6. Opening Tank & Sludge Removal

Sludge Removal Methods (Clause 15.2)

  • Sweep sludge into piles → shovel into buckets/wheelbarrows
  • Wash down tank with water hose (velocity ≤ 1 m/s)
  • Use floor-level manways for flushing if available
  • Use self-priming pumps or water-operated ejectors if no manways

Safety & Preparation (Clause 8.1, 17.1)

  • Beware physical hazards (slipping, falling objects, scaffolding)
  • Use checklist (Appendix A) to confirm tank safety before entry

Important Specifications Summary

Operation StepKey Specification/Notes
Water velocity for washing1 m/s (to avoid damage)
Sludge removal methodManual sweeping, flushing, pumps/ejectors
Safety checksUse checklist before personnel entry

flowchart TD
    A[Start: Preliminary Prep] --> B[Control Ignition]
    B --> C[Empty Tank (Pump & Float)]
    C --> D[Blank Off Tank]
    D --> E[Vapour-Freeing]
    E --> F[Test for Vapours & Toxic Gas]
    F --> G[Open Tank & Remove Sludge]
    G --> H[Dispose Sludge Safely]

This structured approach ensures safe and effective cleaning per IS 9964 Part 1 guidelines.

10Gas Freeing and Ventilation

IS 9964 Part 1 (1981) — Gas Freeing and Ventilation: Key Points

Ventilation Requirements (Clause 6.1.4 & 6.1.4.1)

  • Ventilation must prevent unsafe levels of flammable/toxic vapours and oxygen deficiency.
  • Use approved portable meters for:
    • Combustible gas detection
    • Toxic gas detection
    • Oxygen level measurement
  • Knowledge of tank contents is essential to determine testing needs.

Gas-Freeing Hazards (Clause 11.1)

  • Gas freeing releases inflammable/toxic vapours.
  • Vapours can travel 45-50 meters or more, extending danger zones.
  • Continuous monitoring near ignition sources is mandatory.

Ventilation Methods (Clause 13.2)

  • Forced ventilation via air/steam-driven eductor at lower tank manholes recommended.
  • Avoid working on the roof of tanks that are empty but not gas-free to prevent sparks.
  • Natural ventilation is allowed by removing roof and shell manhole covers in sequence for free airflow.

Summary Table of Ventilation Safety

AspectSpecification
Safe distance for vapours≥ 45 to 50 meters from tank
Ventilation methodForced ventilation with air/steam eductor
Monitoring instrumentsCombustible, toxic gas & oxygen portable meters
Protective equipmentRespiratory protection for personnel near tank
Manhole cover removal orderRoof covers first, then shell covers

flowchart LR
    A[Gas-Freeing Tank] --> B[Release of Vapours]
    B --> C{Vapour Movement}
    C -->|Upwards| D[Roof Manholes]
    C -->|Outwards| E[Danger Zone ≥ 45m]
    D --> F[Forced Ventilation with Eductor]
    E --> G[Personnel Safety Zone]
    F --> H[Safe Atmosphere Inside Tank]
    G --> I[Respiratory Equipment Required]

Note: Always follow statutory authority approvals for instruments and procedures.

11Explosion-Proof Equipment Usage

Explosion-Proof Equipment Usage (IS 9964 Part 1)

  • Clause 11.3:

    • Portable lights, electric motors, and switch gears outside the tank in vapor paths must be explosion-proof.
    • Use explosion-proof extension cords with approved connectors.
    • Equipment must be thoroughly inspected to ensure no ignition sources.
  • Key Safety Checks:

    • Gas testing (Clause 6.1.4.1 & 14.2) with combustible gas, toxic gas, and oxygen indicators is mandatory before and during work.
    • Ventilation must maintain vapor concentration below 5% of LFL (Lower Flammable Limit) for entry without respiratory gear.
    • Entry with independent air supply respiratory equipment allowed up to 20% LFL for cold work only.
    • No entry allowed if vapor concentration exceeds 20% LFL.

Summary Table: Entry Conditions Based on Vapor Concentration

Vapor Concentration (% LFL)Entry Condition
< 5%Entry without respiratory equipment
5% to 20%Entry with independent air supply only
> 20%No entry permitted

Inspection & Equipment Specifications:

  • Explosion-proof equipment per IS standards.
  • Approved connectors and cords.
  • Regular inspection to prevent ignition sources.
flowchart TD
    A[Outside Tank Vapor Path] --> B[Explosion-Proof Equipment]
    B --> C[Inspection: No Ignition Source]
    C --> D{Gas Testing}
    D -->|<5% LFL| E[Entry without Respirator]
    D -->|5-20% LFL| F[Entry with Air Supply Respirator]
    D -->|>20% LFL| G[No Entry Allowed]

Note: Use canister masks only outside tanks; they do not protect against high vapor or oxygen deficiency (Clause 10.3).

12Emptying and Blanking Off the Tank

IS 9964 Part 1: Emptying and Blanking Off Tanks - Key Points

1. Procedure for Blanking Off (Clause 12.3 & 12.2)

  • Close valves nearest to the tank on all connected lines.
  • Drain or flush all lines entering the tank before breaking connections.
  • Break connections and insert spades (blanks) in all lines to prevent vapor or liquid ingress.
  • If blanking is not possible, fill dead ends with water or test lines individually.
  • Close valves outside firewalls nearest to the tank.

2. Safety Specifications (Clause 11.3)

  • Use explosion-proof portable lights, motors, and switchgear outside the tank in vapor paths.
  • Connect equipment with approved explosion-proof extension cords.
  • Thoroughly inspect equipment to ensure no ignition source.

3. Important Notes

  • Residual oil should be removed as far as practicable before blanking.
  • Floating roof tanks (Clause 4.3) reduce vapor losses by maintaining minimal vapor space.

Summary Table: Blanking Off Steps

StepAction
1. Valve ClosureClose valves nearest to tank
2. Line DrainageDrain/flush all lines entering tank
3. Break ConnectionsDisconnect pipe lines
4. Insert SpadesPlace blanks to isolate tank
5. Safety CheckUse explosion-proof equipment & inspect

flowchart TD
    A[Close Valves Nearest to Tank] --> B[Drain/Flush Lines]
    B --> C[Break Connections]
    C --> D[Insert Spades (Blanks)]
    D --> E[Ensure Explosion-Proof Equipment]

This ensures safe isolation of the tank from connected pipelines and prevents vapor or liquid ingress during maintenance or emergency.

13Vapour Testing Procedures

IS 9964 Part 1: Vapour Testing Procedures - Key Points

Steam Ventilation (Clause 13.4)

  • Minimum tank temperature: 77°C (170°F) to effectively expel vapours.
  • Steam quality: Use dry or superheated steam only. Avoid wet steam to prevent static charge and sparking.
  • Static electricity hazard: Steam flow can generate static; bond steam pipe/nozzle to tank.
  • Steam introduction: Near tank bottom; roof manway/gauge hatch must remain open to prevent pressure build-up or vacuum.
  • Vacuum venting: Ensure sufficient venting during rapid steam condensation.

Vapour-Freeing & Testing (Clauses 13.1, 14, 15.3)

  • Vapour-freeing: Complete replacement of hydrocarbon vapours with fresh air.
  • Area evacuation: Only enter for occasional vapour testing.
  • Continuous ventilation: Maintain forced ventilation until all sludge/oil removed.
  • Repeat tests: Before re-entry after breaks or interruptions.
  • Test gases: Hydrocarbon vapours and hydrogen sulphide must be monitored.

Summary Table: Steam Ventilation Parameters

ParameterSpecification
Minimum tank temperature≥ 77°C (170°F)
Steam typeDry or superheated steam only
Steam inlet locationNear tank bottom
Roof manway/gauge hatch statusOpen during steaming
VentingMust prevent vacuum formation

flowchart LR
    Steam[Steam Supply (Dry/Superheated)]
    TankBottom((Tank Bottom))
    TankRoof((Roof Manway/Gauge Hatch Open))
    Venting((Vacuum Venting))

    Steam -->|Bonded Pipe| TankBottom
    TankBottom --> Tank
    Tank --> TankRoof
    Tank --> Venting

Note: Always follow safety protocols for static control and vapour testing to prevent ignition hazards during vapour-freeing operations.

14Detection of Toxic Gases

IS 9964 Part 1 (1981) - Detection of Toxic Gases: Key Points

1. Gas Testing Requirements (Clause 6.1.4.1)

  • Use approved portable meters:
    • Combustible gas indicator
    • Toxic gas indicator
    • Oxygen indicator
  • Testing must be based on knowledge of tank contents.
  • Ensure ventilation prevents unsafe vapour concentration and oxygen deficiency.

2. Safe Exposure Limits for Aromatic Hydrocarbons (Clause 6.1.1.2)

Gas/VapourSafe Limit (8 hrs exposure)
Benzene25 ppm
Toluene/Xylene200 ppm
  • Use gas spectrometry or gas-liquid chromatography if aromatics suspected.

3. Toxicity Expression & Protective Measures (Clause 6.2.2)

  • Toxicity expressed as Threshold Limit Value (TLV)
  • Example: Volatile organo-lead compounds TLV = 75 µg/m³ lead
  • Ventilation alone may not reduce toxic vapours to safe levels.
  • Use respiratory and protective clothing when entering tanks with toxic vapours.

4. Flammable Vapour Limits for Hot Work (Clause 7.1.2)

  • Remove flammable liquids and purge vapours to < 1% of Lower Flammable Limit (LFL)
  • Vapour content at 14-20% LFL corresponds to zero on combustible gas indicator.
  • Note: 1% LFL ≈ 10,000 ppm (unsafe for breathing).

Summary Table: Safe Gas Concentrations & Equipment

ParameterValue/Specification
Benzene safe limit25 ppm
Toluene/Xylene safe limit200 ppm
Organo-lead TLV75 µg/m³ lead
Flammable vapour safe limit< 1% LFL (~10,000 ppm)
EquipmentCombustible, toxic, oxygen meters (approved)
Protective gearRespirators + protective clothing
flowchart LR
    A[Tank Contents Known] --> B[Gas Testing]
    B --> C{Gas Type?}
   
15Opening the Tank and Sludge Removal

IS 9964 Part 1: Key Points on Opening Tank & Sludge Removal


1. Sludge Removal Methods (Clause 15.2)

  • Sweep sludge into piles → shovel into buckets/wheelbarrows.
  • Wash tank with water hose; keep water velocity ≤ 1 m/s.
  • Use floor-level clean-out manways for flushing sludge-laden water.
  • If no manways, use self-priming pumps or water-operated ejectors.

2. Sludge Disposal (Clause 15.2.2)

  • Discharge sludge-laden water into a sludge pit near the tank.
  • Size pit based on sludge volume.
  • Sludge settles; water drains to sewer with extra downstream water to dilute hydrocarbons.
  • Use steam/air pumps to drain excess water from pit.

3. Safety for Personnel (Clause 15.1 & 15.2.2)

  • Tank must be vapour-freed before opening.
  • Entry conditions:
    • Lower Flammable Limit (LFL) < 20%
    • Oxygen content > 19.5%
  • Personnel protective gear:
    • Fresh air hose mask, gloves, rubber boots, light-colored overalls.
  • Rotate men periodically.

4. Checklist for Safe Entry (Clause 17.1)

  • Refer Appendix A for detailed safety checklist before entry.

Summary Table: Sludge Removal Parameters

ParameterValue/Specification
Water velocity for washing1 m/s
LFL for entry< 20%
Oxygen content for entry> 19.5%
Protective equipmentFresh air mask, gloves, boots, light overalls

flowchart TD
    A[Tank Vapour-free] --> B[Open Tank]
    B --> C{Sludge Removal Method}
    C -->|Manways present| D[Flush with water]
    C -->|No manways| E[Use pumps/ejectors]
    D --> F[Discharge sludge water to pit]
    E --> F
    F --> G[Sludge settles in pit]
    G --> H[Water drains to sewer with dilution]
    B --> I[Personnel enter with PPE &
16Surface Preparation and Painting

IS 9964 Part 1: Surface Preparation and Painting of Storage Tanks

Key Specifications (Clause 16.1.2)

  • Surface Preparation:
    • Clean by shot blasting to remove rust, scale, and contaminants completely.
  • Painting Sequence:
    1. Apply 1 coat of amine cured epoxy resin clear lacquer immediately after blasting.
    2. Apply 3 coats of amine cured epoxy resin paint.
    3. Finish with 1 coat of clear lacquer (5th coat overall).
  • Dry Film Thickness (DFT):
    • Minimum total DFT = 125 microns.

Maintenance Painting (Clause 16.2)

  • Avoid scratching painted surfaces during sludge removal.
  • Visual inspection after cleaning:
    • If deteriorated area ≤ 25% → patch painting with 3 coats of epoxy paint.
    • If > 25% → complete repainting required.

Lead Hazard Treatment (Clause 6.2.4)

  • Remove lead hazard by:
    i) Shot blasting to bare metal, or
    ii) Heating tank to cherry-red heat to destroy organic lead.

Summary Table: Painting Coats & Thickness

Coat No.TypePurposeThickness (microns)
1Amine cured epoxy clear lacquerSeal blasted surfacePart of 125 total
2 - 4Amine cured epoxy resin paintProtective coatingPart of 125 total
5Amine cured epoxy clear lacquerFinal protective layerPart of 125 total

flowchart LR
    A[Shot Blasting] --> B[1st Coat: Clear Lacquer]
    B --> C[3 Coats: Epoxy Resin Paint]
    C --> D[5th Coat: Clear Lacquer]
    D --> E[Total DFT ≥ 125 microns]

This ensures corrosion protection and safe tank operation per IS 9964 Part 1.

17Checklist for Tank Cleaning and Entry

IS 9964 Part 1: Checklist for Tank Cleaning and Entry

Key Points from Clause 17.1 & Related Clauses:

  • Appendix A (IS 9964 Part 1) provides a detailed checklist to ensure tank safety before personnel entry for cleaning, inspection, or repair.

  • Major steps for tank cleaning (Clause 9.1):

    1. Preliminary preparations:
      • External tank inspection
      • Surrounding area survey
      • Crew training and equipment inspection
    2. Control ignition sources to prevent fire/explosion.
    3. Empty tank by pumping and floating; blank-off after oil removal.
    4. Vapour-free the tank to ensure safe atmosphere.
    5. Test for hydrocarbon vapour and toxic gases using gas detectors.
    6. Open tank and remove sludge safely.
  • Hazards to consider (Clause 8.1):

    • Slipping, falling objects
    • Falling from or through tank roof
    • Improper scaffolding

Typical Checklist Items (Summary):

TaskDescriptionStatus (✓/✗)
External tank inspectionCheck for structural integrity and leaks
Surrounding area surveyIdentify hazards, ignition sources
Equipment inspectionVerify safety and functionality
Tank emptied & blanked offEnsure minimal residual hydrocarbons
Tank vapour-free confirmationUse gas detectors to confirm safe atmosphere
Safety equipment readyPPE, harnesses, ventilation, communication
Scaffolding & fall protectionProperly installed and secured

Safety Formula for Vapour Testing:

  • Lower Explosive Limit (LEL) Safety Margin: Entry only if hydrocarbon vapour < 10% LEL.

flowchart TD
    A[Preliminary Prep] --> B[Control Ignition]
    B --> C[Empty Tank]
    C --> D[Vapour-Free Tank]
    D --> E[Test Atmosphere]
    E --> F[Safe Entry & Cleaning]

Summary: Follow Appendix A checklist strictly; ensure vapour concentration is below 10

18Sludge Disposal

IS 9964 Part 1: Sludge Disposal Key Points & Specifications

1. Weathering Method (Clause 18.2.2):

  • Spread sludge in 50 mm thick even layers in a pit.
  • Expose to sunny weather for 4 to 8 weeks.
  • Mix sludge with sand/earth in 1:1 ratio to reduce total lead < 0.5%.
  • Bury sludge-earth mix with 600 mm earth cover.
  • Mark burial site permanently with a signboard.

2. Burying Method (Clause 18.2.1):

  • Dig a pit and dump sludge.
  • Cover with 300 to 600 mm fresh earth.
  • Mark the area to prevent accidental disturbance.
  • Organic lead compounds decompose slowly; protective clothing recommended if disturbed.

3. Discharge Restrictions (Clause 15.2.1):

  • Sludge from leaded tanks must not be discharged into sewers.
  • Follow prescribed disposal methods (weathering or burying).

Summary Table:

ParameterSpecification
Sludge layer thickness50 mm (for weathering)
Weathering duration4 to 8 weeks
Sludge to earth/sand mix1 : 1
Earth cover after burial300 to 600 mm (burying), 600 mm (weathering)
Lead content after treatment< 0.5% total lead

flowchart LR
    A[Sludge from Leaded Tank] --> B{Disposal Method}
    B -->|Weathering| C[Spread 50mm layer]
    C --> D[Expose 4-8 weeks]
    D --> E[Mix 1:1 with sand/earth]
    E --> F[Bury with 600mm earth cover]
    B -->|Burying| G[Dig pit]
    G --> H[Dump sludge]
    H --> I[Cover with 300-600mm earth]
    I --> J[Mark site permanently]

Note: Always follow safety precautions during sludge handling and disposal.

19Dismantling and Disposal of Tanks

IS 9964 Part 1 - Key Points on Dismantling and Disposal of Tanks

1. Procedure Reference

  • Follow Clauses 19.2 to 19.8 for detailed dismantling and disposal steps.
  • Checklist for safe entry & inspection: Appendix A (Clause 17.1).

2. Sludge Disposal (Clause 18.2.2.1)

  • If organic lead ≤ 20 ppm (0.002 wt%) after weathering, sludge can be treated as non-toxic industrial waste.
  • Then, remove signs and fences safely.

3. Dismantling Precautions (Clause 19.4)

  • Dismantling causes dust from scale and rust, especially during cold-cutting or sandblasting.
  • To reduce dust, use water spray or fog.
  • Prefer dismantling from outside to minimize dust exposure.

Summary Table for Sludge Lead Content:

Organic Lead Content (ppm)Treatment CategoryAction
≤ 20 ppm (0.002 wt%)Non-toxic industrial wasteNormal disposal; remove signs/fences
> 20 ppmToxic wasteFollow hazardous waste protocols

Safety Flowchart for Tank Dismantling

flowchart TD
    A[Check tank safety (Appendix A)] --> B{Sludge Lead ≤ 20 ppm?}
    B -- Yes --> C[Treat sludge as non-toxic waste]
    B -- No --> D[Follow hazardous sludge disposal]
    C --> E[Remove signs/fences]
    E --> F[Dismantle tank from outside]
    F --> G[Control dust with water spray/fog]
    D --> G

Note: Always comply with local environmental and safety regulations beyond IS 9964.

Popular Questions About IS 9964 Part 1

?What are the recommended procedures for gas freeing petroleum storage tanks before entry?

Recommended Procedures for Gas Freeing Petroleum Storage Tanks (IS 9964 Part 1):

  1. Preparatory Work & Ventilation:

    • Completely replace hydrocarbon vapours with fresh air (vapour-freeing).
    • Continue forced ventilation until all sludge is removed and men remain inside (Clause 15.3).
    • Area must be vacated during vapour-freeing except for occasional vapour tests (Clause 13.1).
  2. Testing Before Entry:

    • Test vapour concentration at tank openings where vapours exit (Clause 14.2).
    • Continue ventilation until zero reading on vapour indicator is obtained.
    • For large tanks, respiratory protective equipment may be needed for testers inside.
  3. Entry Conditions Based on Vapour Concentration:

    • < 5% LFL (Lower Flammable Limit): Entry without respiratory equipment allowed.
    • 5% to 20% LFL: Entry allowed only with independent air supply respiratory equipment for cold work.
    • > 20% LFL: No entry permitted, even with respiratory equipment.
  4. Re-testing:

    • Repeat vapour tests after any extended work interruption or overnight breaks.

Key Limits Summary:

Vapour Concentration (% LFL)Entry Allowed?Equipment Required
< 5%YesNone
5% - 20%Yes (cold work only)Respiratory equipment with air supply
> 20%NoEntry prohibited

Loading diagram...

Note: Always adhere strictly to IS 9964 Part 1 for safety and compliance.

?How should sludge containing leaded gasoline residues be safely handled and disposed of?

Safe Handling and Disposal of Sludge Containing Leaded Gasoline Residues (IS 9964 Part 1):

  • Sludge Composition: Solid phase of insoluble deposits wetted with water and hydrocarbons containing organic lead.

  • Handling Precautions (Clause 6.3 & 6.3.1):

    • Toxic hazard mainly from volatile organic lead vapors.
    • Use protective clothing and canister respirators with 500 cc activated carbon, approved for tetraethyl lead.
    • Replace respirator canisters after 100 hours of use.
    • Monitor lead levels; usually low but precautions mandatory during open-air operations.
  • Disposal Methods (Clause 18.2):

    • Burying: Controlled burial in designated hazardous waste sites.
    • Weathering: Controlled exposure to air to degrade hydrocarbons.
    • Thermal methods (incineration): Effective but less common due to equipment availability.
  • Liquid phase disposal: Dispose as wastewater per pollution regulations after gasoline recovery.


Summary Table

AspectRecommendation
Protective GearProtective clothing + approved respirators
Respirator Canister Life100 hours use
Disposal MethodsBurying, Weathering, (Thermal incineration)
Liquid Phase DisposalWastewater as per pollution norms
Loading diagram...

This ensures safety and environmental compliance per IS 9964 Part 1.

?What protective equipment is required for workers entering tanks with toxic or flammable atmospheres?

Protective Equipment for Workers Entering Tanks with Toxic/Flammable Atmospheres (IS 9964 Part 1)

  • Pre-entry atmosphere conditions:

    • Oxygen level ≥ 19.5% for entry without respiratory equipment.
    • Vapour concentration < 5% of Lower Flammable Limit (LFL) for entry without respiratory gear.
    • Vapour concentration between 5% and 20% LFL requires entry with respiratory protective equipment providing independent air supply (e.g., supplied-air respirators).
    • Entry prohibited if vapour concentration > 20% LFL, even with respiratory equipment.
  • Respiratory protection:

    • Canister-type masks: Only for use outside tanks; limited protection, not suitable for oxygen deficiency or high vapor concentration.
    • Air-supplied respiratory equipment: Required inside tanks when vapour levels exceed 5% LFL but are ≤ 20% LFL.
  • Additional PPE:

    • Boots, gloves, and breathing apparatus must be inspected and in perfect condition before use.
  • Ventilation & Testing:

    • Continuous ventilation until zero combustible gas reading at tank openings.
    • Use portable gas indicators for combustible gases, toxic gases, and oxygen.

Summary Table:

Condition inside TankPPE RequiredNotes
O₂ ≥ 19.5%, Vapour < 5% LFLNo respiratory equipment neededVentilate & test before entry
Vapour 5% – 20% LFLSupplied-air respiratory equipmentEntry allowed for cold work only
Vapour > 20% LFLEntry prohibitedNo entry allowed

Loading diagram...
?How is the presence of hydrogen sulphide detected and managed during tank cleaning?

Detection and Management of Hydrogen Sulphide (H₂S) during Tank Cleaning (IS 9964 Part 1)

  • Detection:

    • Use moistened lead acetate paper which blackens in presence of H₂S.
    • Employ hydrogen sulphide detectors (gas monitors) to test tank atmosphere.
    • Always check instrument functionality before use.
  • Properties of H₂S:

    • Highly toxic, flammable gas.
    • Heavier than air (1.189 times).
    • Flammable limits: 4.3% to 45% by volume in air.
  • Safety Measures:

    • Tanks must be vapour-freed before opening for sludge removal.
    • Workers must wear protective respiratory equipment when working inside tanks that contained sour stocks.
    • Continuously monitor atmosphere for H₂S and hydrocarbons during vapour-freeing.
Loading diagram...

Summary: Detect H₂S using lead acetate paper or detectors, ensure vapour-free conditions, and use respiratory protection to manage H₂S hazards safely.

?What precautions are necessary to prevent ignition during hot work inside petroleum storage tanks?

To prevent ignition during hot work inside petroleum storage tanks (IS 9964 Part 1):

Key Precautions:

  • Remove all flammable/combustible liquids and purge vapors until vapor concentration is much less than 1% of the Lower Flammable Limit (LFL) (Clause 7.1.2).
  • Use fresh air respiratory equipment during welding/flame-cutting on tank bottom plates and first shell ring (Clause 6.3.1.2).
  • For hot work above the first shell ring, clean the area to bare metal by wire brushing or sandblasting to remove lead-containing particles; otherwise, use respiratory protection.
  • For tanks storing high sulfur ("sour stocks"), prevent air entry until all interior surfaces are wetted and keep surfaces wet until gas-free to avoid pyrophoric iron polysulfide ignition (Clause 7.2.1).
  • Inspect all personal protective equipment (boots, gloves, breathing apparatus) for perfect condition before use (Clause 10.3).
  • Avoid ignition sources; ensure hot work is done only after confirming safe vapor levels and proper ventilation.

Vapor Purging Safety:

Vapor ConcentrationSafety Status
< 1% LFLSafe for hot work
14-20% LFLUnsafe, ignition risk high

Loading diagram...

Summary: Thorough cleaning, vapor purging, respiratory protection, and wetting interior surfaces are essential to prevent ignition during hot work inside petroleum tanks.

Need Detailed Clause Answers?

Ask AI about any clause, requirement, or provision in IS 9964 Part 1. Get instant, clause-cited responses powered by our indexed library.

Free tier includes 150 queries (50 AI + 100 Reference) · No credit card required