IS 9964 Part 1 (1981) provides comprehensive recommendations for safely preparing petroleum storage tanks for entry, cleaning, maintenance, and repair. It addresses hazards such as toxic gases, flammable vapors, and physical risks, and outlines procedures for gas freeing, sludge removal, ventilation, and protective measures. This standard is essential for engineers and safety personnel involved in the operation and maintenance of petroleum storage tanks to ensure safe working conditions and compliance with safety protocols.
Overview
IS 9964 Part 1 (1981) provides comprehensive recommendations for safely preparing petroleum storage tanks for entry, cleaning, maintenance, and repair. It addresses hazards such as toxic gases, flammable vapors, and physical risks, and outlines procedures for gas freeing, sludge removal, ventilation, and protective measures. This standard is essential for engineers and safety personnel involved in the operation and maintenance of petroleum storage tanks to ensure safe working conditions and compliance with safety protocols.
Audience
Contents
Structure
Scope:
flowchart TD
A[Start Tank Cleaning] --> B{Hazard Review Done?}
B -- No --> C[Stop Work]
B -- Yes --> D[Remove Hydrocarbons]
D --> E{Oil Temp < 100°C?}
E -- No --> F[Wait]
E -- Yes --> G[Gas Testing & Ventilation]
G --> H{Gas < 20% LEL?}
H -- No --> F
H -- Yes --> I[Permit & PPE Ready]
I --> J[Entry with Stand-by]
J --> K[Complete Cleaning]
K --> L[Exit & Seal Tank]
For detailed design formulas and fabrication requirements, refer to other parts of IS 9964 and related IS codes (e.g., IS 803, IS 2825).
IS 9964 Part 1 focuses on atmospheric petroleum storage tanks, primarily covering their maintenance and operation.
Vapor space volume in fixed roof tanks:
[
V_v = \pi r^2 h_v
]
where (r) = tank radius, (h_v) = vapor space height.
Floating roof eliminates vapor space, reducing (V_v \to 0).
| Tank Type | Roof Type | Vapor Losses | Application |
|---|---|---|---|
| Fixed Roof | Rigid fixed roof | High | General storage |
| Floating Roof | Floating on liquid | Minimal | Volatile liquids, large tanks |
| Open Top | None | Very high | Non-volatile liquids |
flowchart LR
A[Petroleum Storage Tanks] --> B[Fixed Roof Tanks]
A --> C[Floating Roof Tanks]
A --> D[Open Top Tanks]
C --> E[Minimize Vapor Loss]
B --> F[Simple Construction]
D --> G[High Vapor Loss]
For detailed design and maintenance, refer to statutory safety acts and IS 9964 operational clauses.
IS 9964 Part 1 - Statutory Requirements Summary
| Parameter | Limit/Requirement |
|---|---|
| Maximum vapor concentration for entry | < 20% of Lower Explosive Limit (LEL) |
| Oil temperature before water addition | < 100°C |
flowchart TD
A[Review Hazards] --> B[Work Permit System]
B --> C[Remove Hydrocarbons]
C --> D[Check Oil Temp < 100°C]
D --> E[Gas Testing Equipment Ready]
E --> F[Blind All Lines]
F --> G[Check Vapor < 20% LEL]
G --> H[Entry with Respiratory Protection]
H --> I[Stand-by Personnel Present]
I --> J[Perform Cleaning & Repairs]
J --> K[Confirm Zero Gas Reading Before Hot Work]
K --> L[Seal Tank]
For detailed procedures and safety compliance, always refer to IS 9964 Part 1 and relevant statutory acts.
IS 9964 Part 1 (1981) — Tank Construction & Roof Types
| Roof Type | Diameter Range | Description |
|---|---|---|
| Cone Roof Tanks | Up to 75 m | Sloped conical roof, common for large tanks. |
| Umbrella Roof Tanks | Up to 20 m | Segmental plates arched on meridian center lines. |
| Dome Roof Tanks | Up to 20 m | Roof plates formed with spherically curved sections, self-supporting. |
| Floating Roof Tanks | Variable | Roof floats on liquid surface to minimize vapor loss. |
flowchart LR
A[Tank Types] --> B[Cone Roof (≤75m)]
A --> C[Umbrella Roof (≤20m)]
A --> D[Dome Roof (≤20m)]
A --> E[Floating Roof (variable)]
C & D --> F[Self-supporting curved plates]
E --> G[Minimize vapor loss]
For detailed design, refer to IS 9964 tables for plate thickness, joint design, and wind/snow loads.
Hazards in Tank Cleaning (IS 9964 Part 1)
| Hazard Type | Key Risk | Control Measures |
|---|---|---|
| Physical | Falls, slips | Proper scaffolding, PPE, training |
| Health | Toxic gases, vapors | Gas testing, ventilation |
| Fire | Ignition of residual vapors | Eliminate ignition sources, grounding |
flowchart TD
A[Start Cleaning] --> B[Preliminary Inspection]
B --> C[Control Ignition Sources]
C --> D[Empty Tank & Blank Off]
D --> E[Vapour-Freeing & Ventilation]
E --> F[Gas Testing]
F --> G[Safe Entry & Sludge Removal]
Follow strict planning, inspection, and training as per IS 9964 Part 1 for safe tank cleaning.
IS 9964 Part 1 (1981) – Atmospheric Conditions & Safe Breathing Limits
| Substance | Max Exposure (8 hrs) |
|---|---|
| Benzene | 25 ppm |
| Toluene | 200 ppm |
| Xylene | 200 ppm |
flowchart TD
A[Start: Prepare for Tank Entry] --> B[Ventilate Tank]
B --> C[Measure Gas Levels]
C --> D{Oxygen ≥ 19.5%?}
D -- Yes --> E[Check Toxic & Flammable Vapors]
D -- No --> F[Continue Ventilation]
E --> G{Vapors < Safe Limits?}
G -- Yes --> H[Entry Allowed without Respiratory Gear]
G -- No --> I[Use Respiratory Equipment or Delay Entry]
Always confirm gas tests before entry to prevent exposure to toxic or flammable atmospheres.
IS 9964 Part 1: Sources of Ignition & Static Electricity
Sources of Ignition:
Static Electricity Hazards (Clause 7.3):
Precautions for Sour Stock Tanks (Clause 7.2.1):
| Hazard Source | Control Measures |
|---|---|
| Static electricity on liquids | Proper bonding & grounding of equipment |
| Steam gas-freeing charges | Bond steam nozzles; ground metallic objects |
| Pyrophoric iron polysulphide | Prevent air entry; keep surfaces wet |
| Electrical tools | Use explosion-proof fixtures and cords |
To avoid spark generation, bonding resistance ( R_b ) should be low enough:
[ R_b \leq \frac{V_{spark}}{I_{max}} ]
Where:
flowchart LR
A[Steam Nozzle] -->|Bonding| B[Grounded Metal]
B --> C[No Spark Risk]
A --> D[Steam Charges]
D --> E[Insulated Metal Object]
E -->|Charge Accumulation| F[Spark Risk]
Summary: Control static electricity by bonding & grounding, avoid ignition sources, and take special care with sour stock tanks to prevent pyrophoric ignition.
IS 9964 Part 1: Physical Hazards in Tank Cleaning
| Hazard Type | Control Measure | Reference Standard/Practice |
|---|---|---|
| Slipping | Anti-slip surfaces, housekeeping | IS 14489 (Safety in workplaces) |
| Falling objects | Tool lanyards, barricades | IS 3696 (Safety helmets) |
| Falls from height | Guardrails, harnesses | IS 3521 (Safety nets) |
| Scaffolding safety | Load checks, inspections | IS 3696 (Scaffolding safety) |
flowchart TD
A[Physical Hazards] --> B[Slipping]
A --> C[Falling Objects]
A --> D[Fall from Height]
A --> E[Improper Scaffolding]
B --> F[Anti-slip surfaces]
C --> G[Secure tools]
D --> H[Guardrails, harness]
E --> I[Load checks, inspections]
Summary: Control physical hazards by proper planning, safe scaffolding, fall protection, and housekeeping as per IS 9964 and related IS codes.
IS 9964 Part 1: Key Points for Tank Cleaning Operations
| Operation Step | Key Specification/Notes |
|---|---|
| Water velocity for washing | ≤ 1 m/s (to avoid damage) |
| Sludge removal method | Manual sweeping, flushing, pumps/ejectors |
| Safety checks | Use checklist before personnel entry |
flowchart TD
A[Start: Preliminary Prep] --> B[Control Ignition]
B --> C[Empty Tank (Pump & Float)]
C --> D[Blank Off Tank]
D --> E[Vapour-Freeing]
E --> F[Test for Vapours & Toxic Gas]
F --> G[Open Tank & Remove Sludge]
G --> H[Dispose Sludge Safely]
This structured approach ensures safe and effective cleaning per IS 9964 Part 1 guidelines.
IS 9964 Part 1 (1981) — Gas Freeing and Ventilation: Key Points
| Aspect | Specification |
|---|---|
| Safe distance for vapours | ≥ 45 to 50 meters from tank |
| Ventilation method | Forced ventilation with air/steam eductor |
| Monitoring instruments | Combustible, toxic gas & oxygen portable meters |
| Protective equipment | Respiratory protection for personnel near tank |
| Manhole cover removal order | Roof covers first, then shell covers |
flowchart LR
A[Gas-Freeing Tank] --> B[Release of Vapours]
B --> C{Vapour Movement}
C -->|Upwards| D[Roof Manholes]
C -->|Outwards| E[Danger Zone ≥ 45m]
D --> F[Forced Ventilation with Eductor]
E --> G[Personnel Safety Zone]
F --> H[Safe Atmosphere Inside Tank]
G --> I[Respiratory Equipment Required]
Note: Always follow statutory authority approvals for instruments and procedures.
Explosion-Proof Equipment Usage (IS 9964 Part 1)
Clause 11.3:
Key Safety Checks:
| Vapor Concentration (% LFL) | Entry Condition |
|---|---|
| < 5% | Entry without respiratory equipment |
| 5% to 20% | Entry with independent air supply only |
| > 20% | No entry permitted |
flowchart TD
A[Outside Tank Vapor Path] --> B[Explosion-Proof Equipment]
B --> C[Inspection: No Ignition Source]
C --> D{Gas Testing}
D -->|<5% LFL| E[Entry without Respirator]
D -->|5-20% LFL| F[Entry with Air Supply Respirator]
D -->|>20% LFL| G[No Entry Allowed]
Note: Use canister masks only outside tanks; they do not protect against high vapor or oxygen deficiency (Clause 10.3).
IS 9964 Part 1: Emptying and Blanking Off Tanks - Key Points
| Step | Action |
|---|---|
| 1. Valve Closure | Close valves nearest to tank |
| 2. Line Drainage | Drain/flush all lines entering tank |
| 3. Break Connections | Disconnect pipe lines |
| 4. Insert Spades | Place blanks to isolate tank |
| 5. Safety Check | Use explosion-proof equipment & inspect |
flowchart TD
A[Close Valves Nearest to Tank] --> B[Drain/Flush Lines]
B --> C[Break Connections]
C --> D[Insert Spades (Blanks)]
D --> E[Ensure Explosion-Proof Equipment]
This ensures safe isolation of the tank from connected pipelines and prevents vapor or liquid ingress during maintenance or emergency.
IS 9964 Part 1: Vapour Testing Procedures - Key Points
| Parameter | Specification |
|---|---|
| Minimum tank temperature | ≥ 77°C (170°F) |
| Steam type | Dry or superheated steam only |
| Steam inlet location | Near tank bottom |
| Roof manway/gauge hatch status | Open during steaming |
| Venting | Must prevent vacuum formation |
flowchart LR
Steam[Steam Supply (Dry/Superheated)]
TankBottom((Tank Bottom))
TankRoof((Roof Manway/Gauge Hatch Open))
Venting((Vacuum Venting))
Steam -->|Bonded Pipe| TankBottom
TankBottom --> Tank
Tank --> TankRoof
Tank --> Venting
Note: Always follow safety protocols for static control and vapour testing to prevent ignition hazards during vapour-freeing operations.
IS 9964 Part 1 (1981) - Detection of Toxic Gases: Key Points
| Gas/Vapour | Safe Limit (8 hrs exposure) |
|---|---|
| Benzene | 25 ppm |
| Toluene/Xylene | 200 ppm |
| Parameter | Value/Specification |
|---|---|
| Benzene safe limit | 25 ppm |
| Toluene/Xylene safe limit | 200 ppm |
| Organo-lead TLV | 75 µg/m³ lead |
| Flammable vapour safe limit | < 1% LFL (~10,000 ppm) |
| Equipment | Combustible, toxic, oxygen meters (approved) |
| Protective gear | Respirators + protective clothing |
flowchart LR
A[Tank Contents Known] --> B[Gas Testing]
B --> C{Gas Type?}
IS 9964 Part 1: Key Points on Opening Tank & Sludge Removal
| Parameter | Value/Specification |
|---|---|
| Water velocity for washing | ≤ 1 m/s |
| LFL for entry | < 20% |
| Oxygen content for entry | > 19.5% |
| Protective equipment | Fresh air mask, gloves, boots, light overalls |
flowchart TD
A[Tank Vapour-free] --> B[Open Tank]
B --> C{Sludge Removal Method}
C -->|Manways present| D[Flush with water]
C -->|No manways| E[Use pumps/ejectors]
D --> F[Discharge sludge water to pit]
E --> F
F --> G[Sludge settles in pit]
G --> H[Water drains to sewer with dilution]
B --> I[Personnel enter with PPE &
IS 9964 Part 1: Surface Preparation and Painting of Storage Tanks
| Coat No. | Type | Purpose | Thickness (microns) |
|---|---|---|---|
| 1 | Amine cured epoxy clear lacquer | Seal blasted surface | Part of 125 total |
| 2 - 4 | Amine cured epoxy resin paint | Protective coating | Part of 125 total |
| 5 | Amine cured epoxy clear lacquer | Final protective layer | Part of 125 total |
flowchart LR
A[Shot Blasting] --> B[1st Coat: Clear Lacquer]
B --> C[3 Coats: Epoxy Resin Paint]
C --> D[5th Coat: Clear Lacquer]
D --> E[Total DFT ≥ 125 microns]
This ensures corrosion protection and safe tank operation per IS 9964 Part 1.
IS 9964 Part 1: Checklist for Tank Cleaning and Entry
Appendix A (IS 9964 Part 1) provides a detailed checklist to ensure tank safety before personnel entry for cleaning, inspection, or repair.
Major steps for tank cleaning (Clause 9.1):
Hazards to consider (Clause 8.1):
| Task | Description | Status (✓/✗) |
|---|---|---|
| External tank inspection | Check for structural integrity and leaks | |
| Surrounding area survey | Identify hazards, ignition sources | |
| Equipment inspection | Verify safety and functionality | |
| Tank emptied & blanked off | Ensure minimal residual hydrocarbons | |
| Tank vapour-free confirmation | Use gas detectors to confirm safe atmosphere | |
| Safety equipment ready | PPE, harnesses, ventilation, communication | |
| Scaffolding & fall protection | Properly installed and secured |
flowchart TD
A[Preliminary Prep] --> B[Control Ignition]
B --> C[Empty Tank]
C --> D[Vapour-Free Tank]
D --> E[Test Atmosphere]
E --> F[Safe Entry & Cleaning]
Summary: Follow Appendix A checklist strictly; ensure vapour concentration is below 10
1. Weathering Method (Clause 18.2.2):
2. Burying Method (Clause 18.2.1):
3. Discharge Restrictions (Clause 15.2.1):
| Parameter | Specification |
|---|---|
| Sludge layer thickness | 50 mm (for weathering) |
| Weathering duration | 4 to 8 weeks |
| Sludge to earth/sand mix | 1 : 1 |
| Earth cover after burial | 300 to 600 mm (burying), 600 mm (weathering) |
| Lead content after treatment | < 0.5% total lead |
flowchart LR
A[Sludge from Leaded Tank] --> B{Disposal Method}
B -->|Weathering| C[Spread 50mm layer]
C --> D[Expose 4-8 weeks]
D --> E[Mix 1:1 with sand/earth]
E --> F[Bury with 600mm earth cover]
B -->|Burying| G[Dig pit]
G --> H[Dump sludge]
H --> I[Cover with 300-600mm earth]
I --> J[Mark site permanently]
Note: Always follow safety precautions during sludge handling and disposal.
IS 9964 Part 1 - Key Points on Dismantling and Disposal of Tanks
| Organic Lead Content (ppm) | Treatment Category | Action |
|---|---|---|
| ≤ 20 ppm (0.002 wt%) | Non-toxic industrial waste | Normal disposal; remove signs/fences |
| > 20 ppm | Toxic waste | Follow hazardous waste protocols |
flowchart TD
A[Check tank safety (Appendix A)] --> B{Sludge Lead ≤ 20 ppm?}
B -- Yes --> C[Treat sludge as non-toxic waste]
B -- No --> D[Follow hazardous sludge disposal]
C --> E[Remove signs/fences]
E --> F[Dismantle tank from outside]
F --> G[Control dust with water spray/fog]
D --> G
Note: Always comply with local environmental and safety regulations beyond IS 9964.
Frequently Asked
Recommended Procedures for Gas Freeing Petroleum Storage Tanks (IS 9964 Part 1):
Preparatory Work & Ventilation:
Testing Before Entry:
Entry Conditions Based on Vapour Concentration:
Re-testing:
| Vapour Concentration (% LFL) | Entry Allowed? | Equipment Required |
|---|---|---|
| < 5% | Yes | None |
| 5% - 20% | Yes (cold work only) | Respiratory equipment with air supply |
| > 20% | No | Entry prohibited |
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Note: Always adhere strictly to IS 9964 Part 1 for safety and compliance.
Safe Handling and Disposal of Sludge Containing Leaded Gasoline Residues (IS 9964 Part 1):
Sludge Composition: Solid phase of insoluble deposits wetted with water and hydrocarbons containing organic lead.
Handling Precautions (Clause 6.3 & 6.3.1):
Disposal Methods (Clause 18.2):
Liquid phase disposal: Dispose as wastewater per pollution regulations after gasoline recovery.
| Aspect | Recommendation |
|---|---|
| Protective Gear | Protective clothing + approved respirators |
| Respirator Canister Life | 100 hours use |
| Disposal Methods | Burying, Weathering, (Thermal incineration) |
| Liquid Phase Disposal | Wastewater as per pollution norms |
Loading diagram...
This ensures safety and environmental compliance per IS 9964 Part 1.
Protective Equipment for Workers Entering Tanks with Toxic/Flammable Atmospheres (IS 9964 Part 1)
Pre-entry atmosphere conditions:
Respiratory protection:
Additional PPE:
Ventilation & Testing:
| Condition inside Tank | PPE Required | Notes |
|---|---|---|
| O₂ ≥ 19.5%, Vapour < 5% LFL | No respiratory equipment needed | Ventilate & test before entry |
| Vapour 5% – 20% LFL | Supplied-air respiratory equipment | Entry allowed for cold work only |
| Vapour > 20% LFL | Entry prohibited | No entry allowed |
Loading diagram...
Detection and Management of Hydrogen Sulphide (H₂S) during Tank Cleaning (IS 9964 Part 1)
Detection:
Properties of H₂S:
Safety Measures:
Loading diagram...
Summary: Detect H₂S using lead acetate paper or detectors, ensure vapour-free conditions, and use respiratory protection to manage H₂S hazards safely.
To prevent ignition during hot work inside petroleum storage tanks (IS 9964 Part 1):
| Vapor Concentration | Safety Status |
|---|---|
| < 1% LFL | Safe for hot work |
| 14-20% LFL | Unsafe, ignition risk high |
Loading diagram...
Summary: Thorough cleaning, vapor purging, respiratory protection, and wetting interior surfaces are essential to prevent ignition during hot work inside petroleum tanks.
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