IS 9222 Part 11990AI Search Enabled✦ AI Generated

Recommendations for handling and dosing devices for chemicals for water treatment, Part I: Coagulants

IS 9222 Part 1:1990 provides detailed recommendations for the handling, storage, preparation, and dosing of coagulants such as alum and iron salts used in water treatment plants. It is essential for engineers and technicians involved in water treatment to ensure safe, efficient, and corrosion-resistant chemical dosing systems, including design of solution tanks, mixing devices, and feed equipment tailored to various plant sizes and operational conditions.

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What This Standard Covers

IS 9222 Part 1:1990 provides detailed recommendations for the handling, storage, preparation, and dosing of coagulants such as alum and iron salts used in water treatment plants. It is essential for engineers and technicians involved in water treatment to ensure safe, efficient, and corrosion-resistant chemical dosing systems, including design of solution tanks, mixing devices, and feed equipment tailored to various plant sizes and operational conditions.

Who Uses This Standard

  • Water Treatment Plant Engineers
  • Public Health Engineers
  • Chemical Handling Supervisors
  • Process Control Technicians
  • Water Quality Analysts
  • Maintenance Engineers
  • Environmental Compliance Officers

Key Topics Covered

Storage and handling of coagulants
Design and construction of solution tanks
Preparation methods for coagulant solutions
Mixing and agitation devices for homogeneity
Dosing devices and feed systems
Material selection for corrosion resistance
Safety precautions in electrical wiring and equipment
Level indicators and monitoring of solution tanks
Recommended storage capacities and safety factors
Cleaning and maintenance of feed lines
Handling of various coagulant forms (powder, lumps, liquid)
Special considerations for monsoon and climatic conditions

Table of Contents

1Scope

IS 9222 Part 1 — Scope Summary & Key References

  • Scope: Specifies requirements for solution feed devices (chlorinators, bleaching powder feeders) and related equipment.
  • Rounding off: Final test/calculated values must be rounded per IS 2:1960 rules, retaining the same significant figures as specified.
  • Solution Concentration: Refer to Table 1 in the standard for recommended solution strengths.
  • Referenced IS Codes: Annex A lists essential Indian Standards related to materials, electrical installations, safety, and equipment, e.g.:
    • IS 210: Grey iron castings
    • IS 260: Aluminium sulphate
    • IS 325: Three-phase induction motors
    • IS 732 (Parts 1-3): Electrical wiring installation codes
    • IS 1435: Platform weighing machines
    • IS 5216: Safety procedures in electrical work

Table 1 (Example: Solution Concentration Reference)

Solution TypeConcentration (%)
Bleaching powderRefer IS 9222 Pt 1
Ferric chlorideRefer IS 711
Aluminium sulphateRefer IS 260

Notes:

  • Use the Standard Mark under BIS supervision to ensure compliance.
  • Keep updated with amendments from BIS.
  • For detailed specs, consult the full IS 9222 Part 1 document and Annex A for related IS codes.
flowchart LR
    A[IS 9222 Part 1 Scope] --> B[Solution Feed Devices]
    A --> C[Rounding off per IS 2:1960]
    A --> D[Solution Concentration - Table 1]
    A --> E[Referenced IS Codes - Annex A]
    E --> F[IS 210, IS 260, IS 325, IS 732, IS 1435, IS 5216]

This concise overview helps ensure correct application and compliance with IS 9222 Part 1.

2Referenced Indian Standards

IS 9222 Part 1 - Referenced Indian Standards Summary

Key Points from Clause 2.1 and Annex A:

  • The standard references multiple Indian Standards (IS) essential for compliance, covering materials, equipment, and safety.
  • Examples of referenced IS include:
IS No.Title
210:1978Grey iron castings (3rd revision)
260:1969Aluminium sulphate, non-ferric
325:1978Three-phase induction motors (4th revision)
732 (Parts 1-3)Electrical wiring installations (definitions, design, testing)
4691:1985Degrees of protection for rotating electrical machinery enclosures
1435:1960Platform weighing machines
  • These referenced standards ensure material quality, safety, and performance for components used in solution feed devices.

Rounding Off Values (IS 2:1960)

  • Final test values must be rounded off following IS 2:1960 rules.
  • Retain the same number of significant digits as specified in the standard.

Practical Use:

  • Always consult the relevant IS listed for detailed specifications on materials and equipment.
  • Use IS 2:1960 for rounding numerical results to maintain consistency.

flowchart LR
    A[IS 9222 Part 1] --> B[Annex A: Referenced IS]
    B --> C[Material Standards (e.g., IS 210)]
    B --> D[Equipment Standards (e.g., IS 325)]
    B --> E[Safety & Installation (e.g., IS 732)]
    A --> F[Rounding off per IS 2:1960]

For detailed design or testing, refer to the individual IS documents listed in Annex A.

3General Recommendations for Handling Coagulants

IS 9222 Part 1: General Recommendations for Handling Coagulants

Key Points from Table 1 (Clause 8.2):

ChemicalFormulaUseForms & AppearancesSolubility (g/100 cm³)Storage Container MaterialFeeding Method & Solution StrengthHandling Material
Aluminium SulphateAl₂(SO₄)₃·18H₂OCoagulation, sludge conditioningSlabs, lumps, granules, liquid60 at 0°CConcrete with acid-proof bricks, steel paintedGravity feed solution up to 10% concentrationLead, rubber, acid-resistant tile, PVC
Ferric ChlorideFeCl₃·6H₂OCoagulation, sludge conditioningLiquid solution, solidHighly solubleAcid-proof brick, stoneware, concreteSolution 3-4%, feed liquid or solidAcid proof brick, rubber-lined mild steel
Ferric SulphateFe₂(SO₄)₃·xH₂OCoagulationGranules, liquidVery solubleSame as alumSolution up to 25%Plastic, rubber, mild steel, stainless steel
Sodium AluminateNa₂Al₂O₄Coagulation, boiler feed waterPowder, granules, briquettesSolubleConcrete or steelSolution up to 10%Rubber, iron
Sodium SilicateNa₂SiO₃Coagulant acid treatmentViscous aqueous solution7.0 at 20°CSteel drumsSolution up to 5%Rubber, iron
Calcium OxideCaOpH correction, coagulationWhite or light grey powder1.5% solubleDrumsSolution or dry feedRubber, PVC
Calcium HydroxideCa(OH)₂Same as CaOWhite powder1.5% solubleDrumsSolution or dry feed
4Storage of Coagulants

IS 9222 Part 1: Storage of Coagulants - Key Specifications & Tables

Storage Requirements (Clauses 4.2 & 4.5)

  • Storage Room: Damp-proof to prevent moisture ingress.
  • Storage Space Near Feed: Minimum 1 week's supply near feeding device for operational convenience.
  • Flood Protection: Special precautions to avoid flooding damage.

Table 1: Common Coagulants Storage & Handling Summary

ChemicalStorage Container MaterialSpace Required (m³/ton)Special AttentionFeeding FormSolution StrengthSuitable Handling Material
Aluminium SulphateConcrete with acid-proof bricks, steel painted, moisture-proof wood0.79 - 0.93Dusty, sticky, acidic, corrosiveSlabs, lumps, solutionUp to 10% solutionLead, rubber, acid-resistant tile, PVC, mild steel
Ferric ChlorideAcid-proof brick, stoneware, concrete, PVC, wood1.13 - 1.86Acidic, corrosive, deliquescentLiquid or solid3-4% solutionRubber-lined steel, paraffin barrels
Ferric SulphateSame as Alum0.79Acidic, corrosive, stainsGranules, solutionUp to 25% solutionPlastic, rubber, mild steel, stainless steel
Sodium AluminateConcrete or steel1.02 - 1.19HygroscopicPowder, solutionUp to 10% solutionRubber, iron
Sodium SilicateSteel drums4.65Alkaline, sticky, incrustantSolutionUp to 5% solutionRubber, iron
Quick Lime (CaO)Concrete, PVC, wood, steel-Dusty, causticPowder or slurry-Rubber, PVC
Hydrated Lime (Ca(OH)₂)Same as CaO-DustyPowder, suspension-Rubber, PVC
5Weighing and Measuring Coagulants

Weighing and Measuring Coagulants (IS 9222 Part 1)

Key Specifications:

  • Clause 5.1: Predetermined quantities of coagulants must be weighed accurately both on receipt and before feeding.
  • Clause 5.2: Use weighing machines conforming to:
    • IS 1435 : 1960 (Platform Scales)
    • IS 1439 : 1959 (Spring Balances)
    • IS 1854 : 1964 (Weights)

Common Coagulants (Table 1 Highlights):

Chemical NameFormulaCommercial StrengthSolubility (g/100cm³)Feeding FormSolution StrengthStorage Material
Aluminium SulphateAl₂(SO₄)₃·18H₂O960-1200 kg/m³60 @ 0°CSlabs, granules, solutionUp to 10% solutionConcrete, steel (acid-proof)
Ferric ChlorideFeCl₃·6H₂O1120 kg/m³37-47 @ 60% solutionLiquid or solid3-4% solutionAcid-proof brick, steel
Ferric SulphateFe₂(SO₄)₃·xH₂O1120-1152 kg/m³Very solubleGranules, liquidUp to 25% solutionSame as alum

Preparation & Feeding:

  • Preparation: Slowly add powder to water with stirring to avoid dust combustion.
  • Feeding: Gravity feed preferred for solutions; granules or powder can be fed dry.
  • Storage: Tanks must be corrosion-resistant and protected against moisture.

Formula for Solution Preparation:

[ \text{Weight of coagulant} = \text{Volume of solution} \times \text{Strength of solution} \times \text{Density of solution} ]


flowchart LR
    A[Coagulant Receipt] --> B[Weighing (IS 1435, 1439, 1854)]
    B --> C[Preparation Tank]
6Solution Tanks and Preparation

IS 9222 Part 1: Solution Tanks and Preparation - Key Points

1. Number and Capacity of Tanks (Clause 6.1)

  • Minimum 3 tanks for continuous operation (8 hours dosing each):
    • 1 for preparation
    • 1 for dosing
    • 1 standby (cleaning/preparation)
  • If daily coagulant use ≤ 5000 L, 2 tanks suffice (each holds 24-hour solution).
  • For large quantities, multiple tanks to meet 8-hour dose.

2. Tank Design (Clause 6.2)

  • Tanks can be square, rectangular, or circular.
  • Must have mixing devices for intimate chemical mixing.

3. Chemical Preparation & Storage (Table 1 summary)

ChemicalFormStorage MaterialPreparation MethodSolution Strength
Chlorinated ferrous sulphateDry powderPlastic, rubber-lined mild steelMix chlorine and ferrous sulphate powders1 part Cl3 : 7.8 parts FeSO4 by mass
Sodium aluminatePowder/granulesConcrete, steelStir water, slowly add powderUp to 10% solution
Sodium silicateViscous liquidSteel drumsStir water, slowly add powder, continuous stirringUp to 5% solution
Quick lime (CaO)PowderConcrete, PVC, woodStir water, slowly add powderDry or wet feed
Hydrated lime (Ca(OH)2)PowderConcrete, PVC, woodSame as CaODry feed generally

4. Weighing Equipment (Clause 5.2)

  • Use weighing machines conforming to IS 1435, IS 1439, IS 1854 for dosing accuracy.

Summary Diagram of Solution Tank Setup

flowchart LR
    A[Raw Chemicals] --> B[Weighing Machine]
    B --> C[Preparation Tank with Mixer]
    C --> D[Dosing Tank]
    D --> E[Chemical Feed to Process]
    C --> F[Standby Tank (Clean/Ready)]

Note: Mixing devices and corrosion-resistant materials are

7Mixing Devices for Coagulant Solutions

Mixing Devices for Coagulant Solutions
(IS 9222 Part 1: Clauses 7.1, 8.2, 9.2)

Key Specifications:

1. Mixing Methods (Clause 7.1):

  • Mechanical Agitation:

    • Turnover capacity: 2 hours for alum solution tank.
    • Motor: Totally-enclosed fan-cooled.
    • Shaft: Material as per 7.1(c).
    • Paddles: Stainless steel, wood, polypropylene, or fiberglass.
    • Bottom guide: Stainless steel.
    • Gears: Mounted on concrete with cast iron housing.
  • Compressed Air Agitation:

    • Air supply: 0.1 to 0.15 m³/min per m³ of tank volume.
    • Pipe materials: HDPE, unplasticized PVC, or polypropylene.

2. Coagulant Solution Preparation (Table 1, Clause 8.2):

  • Alum, Ferric chloride, Ferric sulphate, etc.
  • Solutions typically prepared by dissolving powder or lumps in water with stirring.
  • Strengths vary (e.g., Alum up to 10%, Ferric chloride 3-4%, Ferric sulphate up to 25%).
  • Storage tanks must be corrosion-resistant (concrete lined with acid-proof bricks, steel painted, or plastic-lined).

3. Feeding Devices (Clause 9.2):

  • Pumps made from corrosion-resistant materials (see Table 1 for suitable materials).
  • Ejectors also used for proportionate feeding.

Summary Table for Mixing Devices:

ParameterMechanical AgitationCompressed Air Agitation
Turnover Time2 hours (for alum solution)Not specified
Air Supply RateN/A0.1 to 0.15 m³/min per m³ tank volume
MaterialsShaft: per 7.1(c); Paddles: SS, wood, PP, fiberglassPipes: HDPE, PVC, polypropylene
InstallationGears on concrete platform, cast iron housingPipes inside tank

Important Notes:

  • Ensure complete dissolution before stirring.
8Solution Feed and Drain Lines

IS 9222 Part 1: Solution Feed and Drain Lines Key Points

Material & Durability (Clause 8.2)

  • Use corrosion-resistant materials as per Table 1.
  • Lines must be durable and accessible for maintenance.

Diameter Specifications

Line TypeMinimum Diameter
Gravity feed solution≥ 50 mm
Pressure feed solution≥ 25 mm
Drain lines≥ 100 mm

Layout & Installation (Clauses 8.2 & 8.3)

  • Avoid air trapping in lines.
  • Provide cleaning eyes at sharp bends.
  • Rubber hoses supported in troughs with easy bends.
  • Protect lines against freezing where applicable.

Maintenance (Clause 8.4)

  • Provide water flushing connections conveniently.
  • Clean coagulant feed lines frequently to prevent choking.

Summary Table:

ParameterSpecification
MaterialCorrosion-resistant (Table 1)
Gravity feed diameter≥ 50 mm
Pressure feed diameter≥ 25 mm
Drain line diameter≥ 100 mm
Cleaning provisionsCleaning eye at bends
Freezing protectionRequired if freezing probable
Flushing connectionConveniently located
flowchart LR
    A[Solution Tank] -->|Gravity feed ≥ 50mm| B[Solution Feed Line]
    B -->|Sharp bends with cleaning eye| C[Coagulant Feed Device]
    C -->|Pressure feed ≥ 25mm| D[Injection Point]
    D --> E[Drain Line ≥ 100mm]
    E --> F[Disposal]
    style B fill:#f9f,stroke:#333,stroke-width:2px
    style E fill:#bbf,stroke:#333,stroke-width:2px

Use filtered or settled clear water for preparing coagulants (Clause 7.3).

9Solution Feed Devices

IS 9222 Part 1: Solution Feed Devices Key Points

  • Purpose: Regulate coagulant dosing into water (Clause 9.1).

  • Flow Measurement: Use rotameter, orifices, or calibrated weirs with scale plates.

  • Material: Non-corrodible construction for solution feed equipment.

  • Strainers: Installed before feed devices; removable for cleaning to prevent clogging.

  • Feeding Mechanism (Clause 9.1.1):

    • Positive displacement pumps or constant head devices recommended for feeding.
  • Flushing (Clause 8.4):

    • Water connections for flushing solution lines should be accessible; frequent cleaning to avoid choking.
  • Stirring & Recirculation (Clause 4.65):

    • Continuous stirring essential; air agitation: 5 min on, 20-30 min rest cycle.
    • Recirculation pump capacity: turnover tank volume in 2 hours.
    • Pump parts: stainless steel/polypropylene impeller, shaft, sleeve; cast iron body (IS 210:1978).
    • Motor: Totally enclosed fan cooled (TEFC), IC41 cooling (IS 6362:1971), IP54 protection or better (IS 4691:1985).

Typical Formula for Pump Capacity (Recirculation):

[ Q = \frac{V}{t} ]

Where:

  • (Q) = Pump flow rate (m³/hr)
  • (V) = Volume of solution tank (m³)
  • (t) = Turnover time (hr), typically 2 hr

Summary Table: Solution Feed Device Features

FeatureSpecification
Flow MeasurementRotameter / Orifice / Calibrated Weir
Feed Pump TypePositive Displacement / Constant Head
MaterialNon-corrodible (SS, polypropylene)
StrainersRemovable, before feed device
StirringAir agitation 5 min on / 20-30 min off
Recirculation Pump2 hr turnover, SS/polypropylene parts
Motor CoolingTEFC, IC41, IP54 or better
flowchart LR
    A[Coagul
10Safety and Maintenance Considerations

IS 9222 Part 1: Safety and Maintenance Considerations for Chemical Handling in Water Treatment

Key Specifications from Clause 8.2 & Table 1:

  • Chemical Properties & Handling:

    • Coagulants like Aluminium Sulphate, Ferric Chloride, Ferric Sulphate, Sodium Aluminate, etc., are acidic or alkaline, corrosive, and hygroscopic.
    • Special attention required for dustiness, corrosiveness, and hygroscopic nature.
  • Storage:

    • Use corrosion-resistant materials: concrete with acid-proof bricks, PVC, rubber-lined steel, stainless steel, or plastic containers.
    • Store in ventilated, cool, and dry spaces.
    • Use hessian or polyethylene bags for powders; drums or carboys for liquids.
  • Preparation & Feeding:

    • Powders: Slowly add to water with stirring to avoid dust explosions.
    • Solutions: Gravity feed or chemical feed pumps recommended.
    • Strength of solutions typically ranges from 3% to 25% depending on chemical.
    • Feeding forms: dry powder, granules, or liquid solutions.

Safety Recommendations:

  • Follow IS 732 and IS 5216 for electrical safety during installation of dosing devices.
  • Use appropriate personal protective equipment (PPE) due to corrosive and toxic nature.
  • Ensure proper ventilation and spill containment.
  • Regular maintenance of dosing pumps and mixers to avoid clogging and leaks.

Summary Table (Example for Aluminium Sulphate):

ParameterDetails
Chemical FormulaAl₂(SO₄)₃·18H₂O
AppearanceLight tan to grey-green slabs
pH Range5.5 to 7.4
Solubility60 g/100 cm³ at 0°C
StorageConcrete tanks with acid-proof lining
Feeding MethodGranules, slabs, or solution
Solution StrengthUp to 10%
Handling MaterialsLead, rubber, PVC, stoneware

flowchart TD
    A[Chemical Storage] --> B[Preparation]
    B --> C[Feeding System]
    C --> D[Water Treatment Process]
    A -. Safety Measures .-> E[PPE & Ventilation]
    B -. Safety Measures

Popular Questions About IS 9222 Part 1

?What are the recommended storage conditions and capacities for coagulants?

Recommended Storage Conditions and Capacities for Coagulants (IS 9222 Part 1):

  • Storage Environment:

    • Store coagulants in a damp-proof, water-tight room to prevent moisture ingress (Clauses 4.1 & 4.2).
    • The store should be located to prevent flooding and water entry.
    • For bagged coagulants, stack bags off the floor at a convenient height.
  • Storage Capacity:

    • Maintain a minimum 3 months' supply based on average consumption for safety (Clause 4.4).
    • Consider monsoon season demands, plant size, coagulant type, supply source, and transport reliability.
    • If major storage is remote from the feeding device, keep at least 1 week's supply near the feeding point for ease of handling (Clause 4.5).

Summary Table

ParameterRecommendation
Storage RoomDamp-proof, water-tight, flood-safe
Storage Capacity3 months average consumption
Local Storage Near Feed1 week's supply
Bag StoragePiled off floor at convenient level
Loading diagram...

This ensures safe, reliable supply and handling of coagulants.

?Which materials are specified for constructing solution tanks and feed lines to resist corrosion?

Materials for Solution Tanks (IS 9222 Part 1 - Clause 6.6):

  • Wood or Reinforced Cement Concrete (RCC) coated with bituminous paint.
  • RCC tanks preferably lined with PVC or epoxy for corrosion resistance.
  • Mild steel tanks must be lined with rubber, PVC, or epoxy to resist corrosion.

Materials for Solution Feed and Drain Lines (Clause 8.2):

  • Lines should be made of durable corrosion-resisting materials as per Table 1 (not provided here, but typically includes PVC, rubber-lined steel, or acid-resistant alloys).
  • Minimum diameters:
    • Gravity feed lines: 50 mm
    • Pressure feed lines: 25 mm
  • Provide cleaning eyes at sharp bends.
  • Additional protection required in freezing conditions.

Summary Table:

ComponentMaterialProtection/LiningMin. Diameter (mm)
Solution TankWood / RCCBituminous paint, PVC/epoxy-
Mild Steel TankMild steelRubber/PVC/epoxy lining-
Feed & Drain LinesCorrosion-resistant material*-Gravity: 50, Pressure: 25

*Refer to Table 1 of IS 9222 Part 1 for specific materials.

Loading diagram...

Note: Always consult Table 1 of IS 9222 Part 1 for exact material specifications.

?How should coagulant solutions be prepared and mixed to ensure homogeneity?

To ensure homogeneity of coagulant solutions as per IS 9222 Part 1:

Preparation & Mixing Guidelines:

  • Weighing: Use predetermined quantities of coagulants, with weighing arrangements both on receipt and before feeding (Clause 5.1).

  • Water Quality: Use filtered water for solution preparation; if unavailable, settled clear water is acceptable (Clause 7.3).

  • Mixing Methods (Clause 7.1):

    • Mechanical Agitation:
      • Agitator turnover capacity: 2 hours for alum solution tanks.
      • Shaft material as specified; paddles made of stainless steel, wood, polypropylene, or fiberglass.
      • Bottom shaft guide: stainless steel.
      • Gears mounted on concrete platform with cast iron housing.
    • Compressed Air:
      • Air supply: 0.1 to 0.15 m³/min per m³ of liquid.
      • Air pressure depends on liquid depth and pipe losses.
      • Use HDPE, unplasticized PVC, or polypropylene pipes for air distribution.
  • Storage Tanks: Tanks must be corrosion-resistant and protected against moisture.

Summary Table for Mixing Devices:

MethodKey Parameters
Mechanical Agitation2-hour turnover, stainless/acid-resistant parts
Compressed Air0.1-0.15 m³/min air per m³ solution, corrosion-resistant pipes

Proper mixing ensures complete dissolution and uniform distribution of coagulants for effective water treatment.

?What types of dosing devices are recommended for accurate chemical feed?

Recommended Types of Dosing Devices for Accurate Chemical Feed (IS 9222 Part 1):

  • Solution Feed Devices: Used to regulate coagulant dosing.
  • Flow Measurement Methods:
    • Rotameter: Measures flow rate visually with a float in a tapered tube.
    • Orifices: Calibrated openings creating a pressure drop to measure flow.
    • Weirs: Calibrated overflow structures for flow measurement.
  • Material: Devices must be non-corrodible to handle chemical solutions.
  • Strainers: Installed before dosing devices to remove suspended impurities and prevent clogging (removable for cleaning).

These devices ensure precise dosing by accurate flow measurement and chemical compatibility, critical for effective water treatment.

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?What safety precautions are advised for electrical installations related to dosing equipment?

Safety Precautions for Electrical Installations in Dosing Equipment (IS 9222 Part 1)

  • Follow adequate safety measures during electrical wiring and fixture installation to ensure safe electricity use.
  • Refer to relevant IS standards for detailed guidance:
    • IS 732 (Part 1, 2, 3) – Code of Practice for Electrical Wiring Installations.
    • IS 5216 (Part 1, 2) – Code of Practice for Electrical Wiring Accessories.
  • Use totally enclosed fan-cooled motors (TEFC) for pumps, conforming to:
    • IS 325:1978 with cooling method IC41 (IS 6362:1971).
    • Enclosures with protection level IP54 or higher (IS 4691:1985).
  • Ensure motor and pump materials are corrosion-resistant (stainless steel, polypropylene, cast iron per IS 210:1978).
  • Maintain proper spacing and secure wiring to prevent moisture ingress and chemical exposure.

This ensures electrical safety and durability in chemically aggressive environments typical of dosing systems.

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