IS 9222 Part 1:1990 provides detailed recommendations for the handling, storage, preparation, and dosing of coagulants such as alum and iron salts used in water treatment plants. It is essential for engineers and technicians involved in water treatment to ensure safe, efficient, and corrosion-resistant chemical dosing systems, including design of solution tanks, mixing devices, and feed equipment tailored to various plant sizes and operational conditions.
Overview
IS 9222 Part 1:1990 provides detailed recommendations for the handling, storage, preparation, and dosing of coagulants such as alum and iron salts used in water treatment plants. It is essential for engineers and technicians involved in water treatment to ensure safe, efficient, and corrosion-resistant chemical dosing systems, including design of solution tanks, mixing devices, and feed equipment tailored to various plant sizes and operational conditions.
Audience
Contents
Structure
IS 9222 Part 1 — Scope Summary & Key References
| Solution Type | Concentration (%) |
|---|---|
| Bleaching powder | Refer IS 9222 Pt 1 |
| Ferric chloride | Refer IS 711 |
| Aluminium sulphate | Refer IS 260 |
flowchart LR
A[IS 9222 Part 1 Scope] --> B[Solution Feed Devices]
A --> C[Rounding off per IS 2:1960]
A --> D[Solution Concentration - Table 1]
A --> E[Referenced IS Codes - Annex A]
E --> F[IS 210, IS 260, IS 325, IS 732, IS 1435, IS 5216]
This concise overview helps ensure correct application and compliance with IS 9222 Part 1.
IS 9222 Part 1 - Referenced Indian Standards Summary
| IS No. | Title |
|---|---|
| 210:1978 | Grey iron castings (3rd revision) |
| 260:1969 | Aluminium sulphate, non-ferric |
| 325:1978 | Three-phase induction motors (4th revision) |
| 732 (Parts 1-3) | Electrical wiring installations (definitions, design, testing) |
| 4691:1985 | Degrees of protection for rotating electrical machinery enclosures |
| 1435:1960 | Platform weighing machines |
flowchart LR
A[IS 9222 Part 1] --> B[Annex A: Referenced IS]
B --> C[Material Standards (e.g., IS 210)]
B --> D[Equipment Standards (e.g., IS 325)]
B --> E[Safety & Installation (e.g., IS 732)]
A --> F[Rounding off per IS 2:1960]
For detailed design or testing, refer to the individual IS documents listed in Annex A.
IS 9222 Part 1: General Recommendations for Handling Coagulants
| Chemical | Formula | Use | Forms & Appearances | Solubility (g/100 cm³) | Storage Container Material | Feeding Method & Solution Strength | Handling Material |
|---|---|---|---|---|---|---|---|
| Aluminium Sulphate | Al₂(SO₄)₃·18H₂O | Coagulation, sludge conditioning | Slabs, lumps, granules, liquid | 60 at 0°C | Concrete with acid-proof bricks, steel painted | Gravity feed solution up to 10% concentration | Lead, rubber, acid-resistant tile, PVC |
| Ferric Chloride | FeCl₃·6H₂O | Coagulation, sludge conditioning | Liquid solution, solid | Highly soluble | Acid-proof brick, stoneware, concrete | Solution 3-4%, feed liquid or solid | Acid proof brick, rubber-lined mild steel |
| Ferric Sulphate | Fe₂(SO₄)₃·xH₂O | Coagulation | Granules, liquid | Very soluble | Same as alum | Solution up to 25% | Plastic, rubber, mild steel, stainless steel |
| Sodium Aluminate | Na₂Al₂O₄ | Coagulation, boiler feed water | Powder, granules, briquettes | Soluble | Concrete or steel | Solution up to 10% | Rubber, iron |
| Sodium Silicate | Na₂SiO₃ | Coagulant acid treatment | Viscous aqueous solution | 7.0 at 20°C | Steel drums | Solution up to 5% | Rubber, iron |
| Calcium Oxide | CaO | pH correction, coagulation | White or light grey powder | 1.5% soluble | Drums | Solution or dry feed | Rubber, PVC |
| Calcium Hydroxide | Ca(OH)₂ | Same as CaO | White powder | 1.5% soluble | Drums | Solution or dry feed |
IS 9222 Part 1: Storage of Coagulants - Key Specifications & Tables
| Chemical | Storage Container Material | Space Required (m³/ton) | Special Attention | Feeding Form | Solution Strength | Suitable Handling Material |
|---|---|---|---|---|---|---|
| Aluminium Sulphate | Concrete with acid-proof bricks, steel painted, moisture-proof wood | 0.79 - 0.93 | Dusty, sticky, acidic, corrosive | Slabs, lumps, solution | Up to 10% solution | Lead, rubber, acid-resistant tile, PVC, mild steel |
| Ferric Chloride | Acid-proof brick, stoneware, concrete, PVC, wood | 1.13 - 1.86 | Acidic, corrosive, deliquescent | Liquid or solid | 3-4% solution | Rubber-lined steel, paraffin barrels |
| Ferric Sulphate | Same as Alum | 0.79 | Acidic, corrosive, stains | Granules, solution | Up to 25% solution | Plastic, rubber, mild steel, stainless steel |
| Sodium Aluminate | Concrete or steel | 1.02 - 1.19 | Hygroscopic | Powder, solution | Up to 10% solution | Rubber, iron |
| Sodium Silicate | Steel drums | 4.65 | Alkaline, sticky, incrustant | Solution | Up to 5% solution | Rubber, iron |
| Quick Lime (CaO) | Concrete, PVC, wood, steel | - | Dusty, caustic | Powder or slurry | - | Rubber, PVC |
| Hydrated Lime (Ca(OH)₂) | Same as CaO | - | Dusty | Powder, suspension | - | Rubber, PVC |
Weighing and Measuring Coagulants (IS 9222 Part 1)
| Chemical Name | Formula | Commercial Strength | Solubility (g/100cm³) | Feeding Form | Solution Strength | Storage Material |
|---|---|---|---|---|---|---|
| Aluminium Sulphate | Al₂(SO₄)₃·18H₂O | 960-1200 kg/m³ | 60 @ 0°C | Slabs, granules, solution | Up to 10% solution | Concrete, steel (acid-proof) |
| Ferric Chloride | FeCl₃·6H₂O | 1120 kg/m³ | 37-47 @ 60% solution | Liquid or solid | 3-4% solution | Acid-proof brick, steel |
| Ferric Sulphate | Fe₂(SO₄)₃·xH₂O | 1120-1152 kg/m³ | Very soluble | Granules, liquid | Up to 25% solution | Same as alum |
[ \text{Weight of coagulant} = \text{Volume of solution} \times \text{Strength of solution} \times \text{Density of solution} ]
flowchart LR
A[Coagulant Receipt] --> B[Weighing (IS 1435, 1439, 1854)]
B --> C[Preparation Tank]
IS 9222 Part 1: Solution Tanks and Preparation - Key Points
| Chemical | Form | Storage Material | Preparation Method | Solution Strength |
|---|---|---|---|---|
| Chlorinated ferrous sulphate | Dry powder | Plastic, rubber-lined mild steel | Mix chlorine and ferrous sulphate powders | 1 part Cl3 : 7.8 parts FeSO4 by mass |
| Sodium aluminate | Powder/granules | Concrete, steel | Stir water, slowly add powder | Up to 10% solution |
| Sodium silicate | Viscous liquid | Steel drums | Stir water, slowly add powder, continuous stirring | Up to 5% solution |
| Quick lime (CaO) | Powder | Concrete, PVC, wood | Stir water, slowly add powder | Dry or wet feed |
| Hydrated lime (Ca(OH)2) | Powder | Concrete, PVC, wood | Same as CaO | Dry feed generally |
flowchart LR
A[Raw Chemicals] --> B[Weighing Machine]
B --> C[Preparation Tank with Mixer]
C --> D[Dosing Tank]
D --> E[Chemical Feed to Process]
C --> F[Standby Tank (Clean/Ready)]
Note: Mixing devices and corrosion-resistant materials are
Mixing Devices for Coagulant Solutions
(IS 9222 Part 1: Clauses 7.1, 8.2, 9.2)
Mechanical Agitation:
Compressed Air Agitation:
| Parameter | Mechanical Agitation | Compressed Air Agitation |
|---|---|---|
| Turnover Time | 2 hours (for alum solution) | Not specified |
| Air Supply Rate | N/A | 0.1 to 0.15 m³/min per m³ tank volume |
| Materials | Shaft: per 7.1(c); Paddles: SS, wood, PP, fiberglass | Pipes: HDPE, PVC, polypropylene |
| Installation | Gears on concrete platform, cast iron housing | Pipes inside tank |
IS 9222 Part 1: Solution Feed and Drain Lines Key Points
| Line Type | Minimum Diameter |
|---|---|
| Gravity feed solution | ≥ 50 mm |
| Pressure feed solution | ≥ 25 mm |
| Drain lines | ≥ 100 mm |
| Parameter | Specification |
|---|---|
| Material | Corrosion-resistant (Table 1) |
| Gravity feed diameter | ≥ 50 mm |
| Pressure feed diameter | ≥ 25 mm |
| Drain line diameter | ≥ 100 mm |
| Cleaning provisions | Cleaning eye at bends |
| Freezing protection | Required if freezing probable |
| Flushing connection | Conveniently located |
flowchart LR
A[Solution Tank] -->|Gravity feed ≥ 50mm| B[Solution Feed Line]
B -->|Sharp bends with cleaning eye| C[Coagulant Feed Device]
C -->|Pressure feed ≥ 25mm| D[Injection Point]
D --> E[Drain Line ≥ 100mm]
E --> F[Disposal]
style B fill:#f9f,stroke:#333,stroke-width:2px
style E fill:#bbf,stroke:#333,stroke-width:2px
Use filtered or settled clear water for preparing coagulants (Clause 7.3).
IS 9222 Part 1: Solution Feed Devices Key Points
Purpose: Regulate coagulant dosing into water (Clause 9.1).
Flow Measurement: Use rotameter, orifices, or calibrated weirs with scale plates.
Material: Non-corrodible construction for solution feed equipment.
Strainers: Installed before feed devices; removable for cleaning to prevent clogging.
Feeding Mechanism (Clause 9.1.1):
Flushing (Clause 8.4):
Stirring & Recirculation (Clause 4.65):
[ Q = \frac{V}{t} ]
Where:
| Feature | Specification |
|---|---|
| Flow Measurement | Rotameter / Orifice / Calibrated Weir |
| Feed Pump Type | Positive Displacement / Constant Head |
| Material | Non-corrodible (SS, polypropylene) |
| Strainers | Removable, before feed device |
| Stirring | Air agitation 5 min on / 20-30 min off |
| Recirculation Pump | 2 hr turnover, SS/polypropylene parts |
| Motor Cooling | TEFC, IC41, IP54 or better |
flowchart LR
A[Coagul
IS 9222 Part 1: Safety and Maintenance Considerations for Chemical Handling in Water Treatment
Chemical Properties & Handling:
Storage:
Preparation & Feeding:
| Parameter | Details |
|---|---|
| Chemical Formula | Al₂(SO₄)₃·18H₂O |
| Appearance | Light tan to grey-green slabs |
| pH Range | 5.5 to 7.4 |
| Solubility | 60 g/100 cm³ at 0°C |
| Storage | Concrete tanks with acid-proof lining |
| Feeding Method | Granules, slabs, or solution |
| Solution Strength | Up to 10% |
| Handling Materials | Lead, rubber, PVC, stoneware |
flowchart TD
A[Chemical Storage] --> B[Preparation]
B --> C[Feeding System]
C --> D[Water Treatment Process]
A -. Safety Measures .-> E[PPE & Ventilation]
B -. Safety Measures
Frequently Asked
Recommended Storage Conditions and Capacities for Coagulants (IS 9222 Part 1):
Storage Environment:
Storage Capacity:
| Parameter | Recommendation |
|---|---|
| Storage Room | Damp-proof, water-tight, flood-safe |
| Storage Capacity | 3 months average consumption |
| Local Storage Near Feed | 1 week's supply |
| Bag Storage | Piled off floor at convenient level |
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This ensures safe, reliable supply and handling of coagulants.
Materials for Solution Tanks (IS 9222 Part 1 - Clause 6.6):
Materials for Solution Feed and Drain Lines (Clause 8.2):
| Component | Material | Protection/Lining | Min. Diameter (mm) |
|---|---|---|---|
| Solution Tank | Wood / RCC | Bituminous paint, PVC/epoxy | - |
| Mild Steel Tank | Mild steel | Rubber/PVC/epoxy lining | - |
| Feed & Drain Lines | Corrosion-resistant material* | - | Gravity: 50, Pressure: 25 |
*Refer to Table 1 of IS 9222 Part 1 for specific materials.
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Note: Always consult Table 1 of IS 9222 Part 1 for exact material specifications.
To ensure homogeneity of coagulant solutions as per IS 9222 Part 1:
Weighing: Use predetermined quantities of coagulants, with weighing arrangements both on receipt and before feeding (Clause 5.1).
Water Quality: Use filtered water for solution preparation; if unavailable, settled clear water is acceptable (Clause 7.3).
Mixing Methods (Clause 7.1):
Storage Tanks: Tanks must be corrosion-resistant and protected against moisture.
| Method | Key Parameters |
|---|---|
| Mechanical Agitation | 2-hour turnover, stainless/acid-resistant parts |
| Compressed Air | 0.1-0.15 m³/min air per m³ solution, corrosion-resistant pipes |
Proper mixing ensures complete dissolution and uniform distribution of coagulants for effective water treatment.
Recommended Types of Dosing Devices for Accurate Chemical Feed (IS 9222 Part 1):
These devices ensure precise dosing by accurate flow measurement and chemical compatibility, critical for effective water treatment.
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Safety Precautions for Electrical Installations in Dosing Equipment (IS 9222 Part 1)
This ensures electrical safety and durability in chemically aggressive environments typical of dosing systems.
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