IS 91971979AI Search Enabled✦ AI Generated

epoxy resin, hardeners and epoxy resin compositions for floor topping

IS 9197-1979 specifies the requirements and testing methods for epoxy resins, hardeners, and epoxy resin compositions used specifically for floor toppings. It covers material properties, chemical resistance, mechanical strength, and packaging standards to ensure durable, high-performance epoxy flooring solutions. This standard is essential for manufacturers, suppliers, and engineers involved in the formulation, quality control, and application of epoxy resin floor toppings in industrial and commercial environments.

7Sections
51Clauses Indexed
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1979Edition
Flooring Wall Finishing and RoofingCategory
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What This Standard Covers

IS 9197-1979 specifies the requirements and testing methods for epoxy resins, hardeners, and epoxy resin compositions used specifically for floor toppings. It covers material properties, chemical resistance, mechanical strength, and packaging standards to ensure durable, high-performance epoxy flooring solutions. This standard is essential for manufacturers, suppliers, and engineers involved in the formulation, quality control, and application of epoxy resin floor toppings in industrial and commercial environments.

Who Uses This Standard

  • Civil Engineers
  • Flooring Contractors
  • Materials Testing Laboratories
  • Epoxy Resin Manufacturers
  • Quality Control Engineers
  • Construction Project Managers
  • Chemical Formulation Specialists

Key Topics Covered

Specifications for epoxy resin grades and classes
Types and properties of hardeners
Formulation of epoxy resin compositions for floor toppings
Mechanical properties: compressive, tensile, flexural, and shear strength
Chemical resistance requirements
Pot life and curing characteristics
Use of plasticizers and diluents
Aggregate requirements and grading
Sampling and acceptance criteria
Packing and marking guidelines
Testing methods for physical and chemical properties
Resistance to wear and abrasion
Thermal properties including expansion and conductivity
Incorporation of liquid coal tar
Quality conformity and re-testing procedures

Table of Contents

1Scope

IS 9197 Scope Summary:

  • Purpose: Code of practice for laying epoxy resin floor toppings.
  • Flexibility: Clauses 3.1, 3.2, 3.4, and 3.6 allow purchaser options to suit requirements.
  • International Coordination: Harmonized with global standards and Indian field practices.
  • Rounding Off: Test results rounded per IS 2-1960, matching significant figures of specified values.

Key Tables & Specifications

1. Epoxy Resin Grade 2 (Clause 1.05)

ClassEpoxy Content (min / 1000g)Viscosity @ 27℃ (Pa.s)Specific Gravity @ 27℃Hydrolyzable Chlorine (%) Max
I50.5 to 0.91.05 Min - 1.20 Max9.0
II50.9 to 4Same as above0.6
III54 to 10Same as above9.0

2. Liquid Coal Tar Properties (Clause 3.5)

CharacteristicRequirementIS Test Reference
Viscosity @ 40℃ (Pa.s)14 to 16IS 1206-1958
Specific Gravity @ 27℃1.15 to 1.21IS 1202-1958
Residue (pitch), %60 to 70IS 1204-1958
Softening Point (°C)67IS 1205-1958
Fractional Distillation (% mass)170°-270℃: 7.85IS 1213-1958
270°-300℃: 5.46
300°-350℃: 19.06
Phenol, cresols, etc. (%) max3IS 121
2Definitions

IS 9197 - Definitions & Key Specifications

  • Definitions: As per Clause 2.1, all definitions refer to IS 4631-1968 (Code of practice for laying epoxy resin floor toppings).

Key Tables & Specifications

1. Epoxy Resin (Grade 2) Requirements (Clause 1.05, Table 2)

ClassEpoxy Content (min/1000g)Viscosity @ 27°C (Pa.s)Specific Gravity @ 27°CHydrolyzable Chlorine (%) Max
I50.5 to 0.91.05 to 1.209.0
II50.9 to 41.05 to 1.200.6
III54 to 101.05 to 1.209.0

2. Liquid Coal Tar Properties (Clause 3.5, Table 4)

CharacteristicRequirementIS Test Reference
Viscosity @ 40°C (Pa.s)14 to 16IS 1206-1958
Specific Gravity @ 27°C1.15 to 1.21IS 1202-1958
Residue (pitch), %60 to 70IS 1204-1958
Softening Point of Residual Pitch67°CIS 1205-1958
Fractional Distillation (%)IS 1213-1958
- 170°-270°C7.85
- 270°-300°C5.46
- 300°-350°C19.06
Phenol, cresols, etc., % Max3IS 1218-1959
Naphthalene, % Max2
3Materials

IS 9197: Key Material Specifications & Tables


1. Epoxy Resin (Clause 3.1)

  • Grade 1 (No diluents):

    ClassEpoxy Content (Eq./1000g)Weight/Epoxy Eq.Viscosity @27℃ (Pa.s)Specific Gravity @27℃Max Hydrolyzable Chlorine %
    I5.0 to 5.88200 to 1703 to 201.05 Min - 1.20 Max9.0
  • Grade 2 (With reactive diluent):

    ClassEpoxy Content (Eq./1000g) MinViscosity @27℃ (Pa.s)Specific Gravity @27℃Max Hydrolyzable Chlorine %
    I50.5 to 0.91.05 Min - 1.20 Max9.0
    II50.9 to 4Same as above0.6
    III54 to 10Same as above9.0

2. Hardeners for Epoxy Resin (Clause 3.2)

TypeViscosity @25℃ (MPa.s)Amine Value (mg KOH/g)Specific Gravity @25℃Amount per Epoxy Eq. (g)Remarks
Aliphatic Amine A10 to 201300 to 17000.97 to 0.9916 to 25High reaction rate, sensitive to humidity
Aromatic Amine Adduct A3800 to 6000260 to 2901.11 to 1.12110 to
4Properties of Epoxy Resin Compositions

IS 9197: Key Properties & Specifications for Epoxy Resin Compositions


1. Pot Life (Clause 4.1)

  • Minimum 45 minutes at 27 ± 2°C and 65 ± 5% RH (IS: 9162-1979)

2. Epoxy Resin Grades (Clause 3.1)

GradeEpoxy Content Equivalent/1000gViscosity at 27°C (Pa.s)Specific Gravity at 27°CHydrolyzable Chlorine (%) Max
Grade 1 (No diluents)5.0 to 5.883 to 201.05 Min to 1.20 Max9.0
Grade 2 (With reactive diluent)50.5 to 10 (varies by class)1.05 Min to 1.20 Max0.6 to 9.0

3. Hardener Types & Properties (Table 3, Clause 3.2)

TypeViscosity at 25°C (mPa.s)Amine Value (mg KOH/g)Specific GravityRecommended Amount (g/eq epoxy)Remarks
Aliphatic Amine A10-201300-17000.97-0.9916-25Fast reaction, sensitive to humidity
Aromatic Amine Adduct A3800-6000260-2901.11-1.12110-130Cures at high humidity, medium rate
Polyaminoamide A12500-17500350-4100.96-0.98110-190Slow curing, low exotherm

(Refer to full table for all types)


4. Mechanical & Physical Properties for Floor Topping (Table 5)

PropertyMinimum / MaximumUnit
Compressive Strength80N/mm
5Sampling and Criteria for Acceptance

IS 9197: Sampling and Criteria for Acceptance

Sampling Procedure (Clause 5.1 & Appendix A)

  • Samples must be taken from each lot separately to verify conformity.
  • Sampling should follow the procedure detailed in Appendix A of IS 9197.
  • Each lot is tested independently.

Criteria for Acceptance (Table A-3, Clause 3.3)

  • If the first sample fails the requirements in Table 5, a second sample from the same lot is tested.
  • If the second sample also fails, the entire lot is rejected.
  • This ensures strict quality control.

Summary Table: Conformity Check

StepActionResult
1st SampleTest as per Table 5 requirementsPass → Accept lot
Fail → Test 2nd sample
2nd SampleTest as per Table 5 requirementsPass → Accept lot
Fail → Reject entire lot

Note:

  • Table 5 specifies detailed test requirements for epoxy resin hardeners and compositions.
  • Sampling size and frequency are per Appendix A.
flowchart TD
    A[Sample Lot] --> B{Test 1st Sample}
    B -- Pass --> C[Accept Lot]
    B -- Fail --> D[Test 2nd Sample]
    D -- Pass --> C
    D -- Fail --> E[Reject Lot]

This approach ensures reliable quality assurance of epoxy resin materials per IS 9197.

6Packing and Marking

IS 9197: Packing and Marking Key Points

Packing (Clause 6.1)

  • Resins and Hardeners: Packed separately in sealed airtight containers to prevent contamination and degradation.
  • Fillers: Supplied in separate packaging from resins and hardeners.

Marking Requirements (Clause 6.1.1)

Each package must be legibly marked with:

  • Manufacturer's name
  • Product name
  • Date of manufacture or batch number
  • Storage requirements
  • Storage life
  • Date of expiry

BIS Certification (Clause 6.2)

  • Products may carry the BIS Standard Mark to indicate conformity with IS 9197.

Summary Table for Packing & Marking

ItemRequirement
Resin & HardenerSeparate, airtight sealed containers
FillerSeparate packaging
Marking DetailsManufacturer, product, batch/date, storage info, expiry
BIS MarkOptional, indicates standard compliance

flowchart LR
    A[Resin] --> B[Sealed Airtight Container]
    C[Hardener] --> D[Sealed Airtight Container]
    E[Filler] --> F[Separate Packaging]
    B & D & F --> G[Marking on Package]
    G --> H{Marking Details}
    H --> I[Manufacturer Name]
    H --> J[Product Name]
    H --> K[Batch/Date]
    H --> L[Storage Requirements]
    H --> M[Storage Life]
    H --> N[Expiry Date]
Appendix ASampling Procedure and Conformity Criteria

IS 9197: Sampling Procedure & Conformity Criteria

Sampling Procedure (Clause 5.1, Appendix A)

  • Samples are selected from each lot separately to verify conformity (Clause A-1.2).
  • If a sample fails, a re-test is done on a fresh sample from the same lot (Clause 3.3).
  • If the second sample also fails, the entire lot is rejected.

Conformity Criteria (Table A-3, Clause 3.3)

Test ResultAction
Pass first sampleAccept lot
Fail first samplePrepare second sample and test
Pass second sampleAccept lot
Fail second sampleReject lot

Additional Notes

  • Final test values must be rounded off as per IS 2:1960, matching the significant figures of the specified values (Clause 3.4).
  • Purchaser may select options as per Clauses 3.1, 3.2, 3.4, and 3.6 to suit requirements.
flowchart TD
    A[Select Sample from Lot] --> B[Test Sample]
    B -->|Pass| C[Accept Lot]
    B -->|Fail| D[Prepare Second Sample]
    D --> E[Test Second Sample]
    E -->|Pass| C
    E -->|Fail| F[Reject Lot]

This ensures quality control by rigorous testing and clear acceptance/rejection rules.

Popular Questions About IS 9197

?What are the specified grades and classes of epoxy resin under IS 9197?

Under IS 9197, epoxy resin is classified into two grades with specific classes for Grade 1:

Grades of Epoxy Resin:

  • Grade 1: Resins containing no diluents.
  • Grade 2: Resins modified with a reactive diluent; each class of Grade 2 can be made from Grade 1 resin.

Grade 1 Resin Classes (per Table 1):

ClassEpoxy Content (Eq./1000g)Weight per Epoxy Equivalent (g)Viscosity at 27°C (Pa.s)Specific Gravity at 27°CMax Hydrolyzable Chlorine (%)
I5.0 to 5.88170 to 2003 to 201.05 min to 1.20 max9.0

Notes:

  • Grade 1 resins have higher purity (no diluents).
  • Grade 2 resins include reactive diluents to modify properties.
  • Other grades may be used if agreed upon by purchaser and supplier.

This classification ensures proper selection for floor topping applications as per IS 9197.

?Which types of hardeners are permitted and what are their characteristics?

Permitted Hardeners as per IS 9197 Clause 3.2 & Table 3:

  • Hardeners must be liquid type reacting with epoxy resin above 5°C.
  • Types include:
    • Aliphatic amines (fast or slow curing, sensitive to humidity)
    • Aromatic amine adducts (good for high humidity & low temp curing)
    • Polyaminoamides (slow curing, low exotherm)
    • Amino resin compounds (adjustable pot-life & exotherm)
TypeViscosity (mPa.s)Amine Value (mg KOH/g)Specific GravityRecommended Amount (g/eq epoxy)Characteristics
Aliphatic Amine A10–201300–17000.97–0.9916–25Fast reaction, strong exotherm, humidity sensitive
Aliphatic Amine B20–40450–500-50–55Slow curing, long pot life, low exotherm
Aromatic Amine Adduct A3800–6000260–2901.11–1.12110–130Cures well in humidity & low temp, medium rate
Polyaminoamide A12,500–17,500350–4100.96–0.98110–190Slow curing, low exotherm
Amino Resin Compound A17,000–23,000300–360-100–110Adjustable pot life & exotherm

Additional Notes:

  • Plasticizers/non-reactive diluents can be added up to 25 parts per 100 parts resin without affecting pot life or strength.
  • Pot life must be ≥ 45 minutes at 27±2°C, 65±5% RH (Clause 4.1).

This ensures selection based on curing speed, environmental conditions, and application requirements.

?How does the standard define the mechanical strength requirements for epoxy floor toppings?

IS 9197 defines the mechanical strength requirements for epoxy floor toppings in Table 5, summarized as follows (tested after 7 days curing per Clause 4.4):

PropertyMinimum/Maximum ValueUnit
Compressive Strength80N/mm²
Bond Strength2N/mm²
Flexural Strength20N/mm²
Tensile Strength15N/mm²
Modulus of Elasticity35 × 10³N/mm²
Coefficient of Thermal Expansion≤ 45 × 10⁻⁶mm/mm/°C
Thermal Conductivity (optional)≤ 1W/mK
Linear Shrinkage≤ 0.10%
Water Absorption≤ 0.50%
Resistance to WearAvg. ≤ 2 mm, Individual ≤ 25 mmmm
Shear Strength≥ 3.2N/mm²

Testing follows IS 9162-1979 methods (Clauses 8-17).


Key Points:

  • Mechanical strengths (compressive, tensile, flexural, shear) ensure durability under loads.
  • Wear resistance limits abrasion ensuring longevity.
  • Thermal and shrinkage limits maintain dimensional stability.
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This ensures epoxy

?What testing methods are recommended for verifying chemical resistance and wear properties?

Testing Methods for Chemical Resistance and Wear Properties as per IS 9197:

  • Chemical Resistance (Clause 4.2):
    Test the cured epoxy resin composition according to IS 9162-1979 referencing Table 1 of IS 4631-1968. This ensures the epoxy withstands specified chemicals without degradation.

  • Resistance to Wear (Clause 4.3):
    Conduct wear tests per IS 9162-1979.

    • Test at least 6 specimens.
    • Permissible wear limits (from Table 5):
      • Average wear ≤ 2 mm
      • Individual wear ≤ 25 mm

Summary Table for Wear Limits (from IS 9197 Table 5):

ParameterLimit
Average wear≤ 2 mm
Individual wear≤ 25 mm

Key Reference:

  • IS 9162-1979 outlines detailed procedures for both chemical resistance and wear testing of epoxy resin floor toppings.
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This ensures compliance with IS 9197 for durable epoxy flooring.

?How should epoxy resin compositions be sampled and what are the acceptance criteria?

Sampling and Acceptance Criteria for Epoxy Resin Compositions (IS 9197)

  • Sampling: Samples of epoxy resin-hardeners and compositions (including fillers and aggregates) should be taken as per Clause 5 of IS 9197, ensuring representative sampling from batches intended for floor toppings.

  • Acceptance Criteria: After 7 days curing, the cured samples must meet the mechanical and physical properties specified in Table 5 (Clause 4.4):

CharacteristicRequirementUnit
Compressive strength≥ 80N/mm²
Bond strength≥ 2N/mm²
Flexural strength≥ 20N/mm²
Tensile strength≥ 15N/mm²
Modulus of elasticity≥ 35 × 10³N/mm²
Coefficient of thermal expansion≤ 45 × 10⁻⁶mm/mm/°C
Thermal conductivity (opt.)≤ 1W/mK
Linear shrinkage≤ 0.10%
Water absorption≤ 0.50%
Resistance to wearAvg ≤ 2, Individual ≤ 25mm
Shear strength≥ 3.2N/mm²
  • Chemical Resistance: Must comply with IS 4631:1968 Table 1, tested as per IS 9162.

This ensures the epoxy floor topping performs structurally and durably under service conditions.

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