IS 9197-1979 specifies the requirements and testing methods for epoxy resins, hardeners, and epoxy resin compositions used specifically for floor toppings. It covers material properties, chemical resistance, mechanical strength, and packaging standards to ensure durable, high-performance epoxy flooring solutions. This standard is essential for manufacturers, suppliers, and engineers involved in the formulation, quality control, and application of epoxy resin floor toppings in industrial and commercial environments.
Overview
IS 9197-1979 specifies the requirements and testing methods for epoxy resins, hardeners, and epoxy resin compositions used specifically for floor toppings. It covers material properties, chemical resistance, mechanical strength, and packaging standards to ensure durable, high-performance epoxy flooring solutions. This standard is essential for manufacturers, suppliers, and engineers involved in the formulation, quality control, and application of epoxy resin floor toppings in industrial and commercial environments.
Audience
Contents
Structure
IS 9197 Scope Summary:
| Class | Epoxy Content (min / 1000g) | Viscosity @ 27℃ (Pa.s) | Specific Gravity @ 27℃ | Hydrolyzable Chlorine (%) Max |
|---|---|---|---|---|
| I | 5 | 0.5 to 0.9 | 1.05 Min - 1.20 Max | 9.0 |
| II | 5 | 0.9 to 4 | Same as above | 0.6 |
| III | 5 | 4 to 10 | Same as above | 9.0 |
| Characteristic | Requirement | IS Test Reference |
|---|---|---|
| Viscosity @ 40℃ (Pa.s) | 14 to 16 | IS 1206-1958 |
| Specific Gravity @ 27℃ | 1.15 to 1.21 | IS 1202-1958 |
| Residue (pitch), % | 60 to 70 | IS 1204-1958 |
| Softening Point (°C) | 67 | IS 1205-1958 |
| Fractional Distillation (% mass) | 170°-270℃: 7.85 | IS 1213-1958 |
| 270°-300℃: 5.46 | ||
| 300°-350℃: 19.06 | ||
| Phenol, cresols, etc. (%) max | 3 | IS 121 |
IS 9197 - Definitions & Key Specifications
| Class | Epoxy Content (min/1000g) | Viscosity @ 27°C (Pa.s) | Specific Gravity @ 27°C | Hydrolyzable Chlorine (%) Max |
|---|---|---|---|---|
| I | 5 | 0.5 to 0.9 | 1.05 to 1.20 | 9.0 |
| II | 5 | 0.9 to 4 | 1.05 to 1.20 | 0.6 |
| III | 5 | 4 to 10 | 1.05 to 1.20 | 9.0 |
| Characteristic | Requirement | IS Test Reference |
|---|---|---|
| Viscosity @ 40°C (Pa.s) | 14 to 16 | IS 1206-1958 |
| Specific Gravity @ 27°C | 1.15 to 1.21 | IS 1202-1958 |
| Residue (pitch), % | 60 to 70 | IS 1204-1958 |
| Softening Point of Residual Pitch | 67°C | IS 1205-1958 |
| Fractional Distillation (%) | IS 1213-1958 | |
| - 170°-270°C | 7.85 | |
| - 270°-300°C | 5.46 | |
| - 300°-350°C | 19.06 | |
| Phenol, cresols, etc., % Max | 3 | IS 1218-1959 |
| Naphthalene, % Max | 2 |
IS 9197: Key Material Specifications & Tables
Grade 1 (No diluents):
| Class | Epoxy Content (Eq./1000g) | Weight/Epoxy Eq. | Viscosity @27℃ (Pa.s) | Specific Gravity @27℃ | Max Hydrolyzable Chlorine % |
|---|---|---|---|---|---|
| I | 5.0 to 5.88 | 200 to 170 | 3 to 20 | 1.05 Min - 1.20 Max | 9.0 |
Grade 2 (With reactive diluent):
| Class | Epoxy Content (Eq./1000g) Min | Viscosity @27℃ (Pa.s) | Specific Gravity @27℃ | Max Hydrolyzable Chlorine % |
|---|---|---|---|---|
| I | 5 | 0.5 to 0.9 | 1.05 Min - 1.20 Max | 9.0 |
| II | 5 | 0.9 to 4 | Same as above | 0.6 |
| III | 5 | 4 to 10 | Same as above | 9.0 |
| Type | Viscosity @25℃ (MPa.s) | Amine Value (mg KOH/g) | Specific Gravity @25℃ | Amount per Epoxy Eq. (g) | Remarks |
|---|---|---|---|---|---|
| Aliphatic Amine A | 10 to 20 | 1300 to 1700 | 0.97 to 0.99 | 16 to 25 | High reaction rate, sensitive to humidity |
| Aromatic Amine Adduct A | 3800 to 6000 | 260 to 290 | 1.11 to 1.12 | 110 to |
IS 9197: Key Properties & Specifications for Epoxy Resin Compositions
| Grade | Epoxy Content Equivalent/1000g | Viscosity at 27°C (Pa.s) | Specific Gravity at 27°C | Hydrolyzable Chlorine (%) Max |
|---|---|---|---|---|
| Grade 1 (No diluents) | 5.0 to 5.88 | 3 to 20 | 1.05 Min to 1.20 Max | 9.0 |
| Grade 2 (With reactive diluent) | 5 | 0.5 to 10 (varies by class) | 1.05 Min to 1.20 Max | 0.6 to 9.0 |
| Type | Viscosity at 25°C (mPa.s) | Amine Value (mg KOH/g) | Specific Gravity | Recommended Amount (g/eq epoxy) | Remarks |
|---|---|---|---|---|---|
| Aliphatic Amine A | 10-20 | 1300-1700 | 0.97-0.99 | 16-25 | Fast reaction, sensitive to humidity |
| Aromatic Amine Adduct A | 3800-6000 | 260-290 | 1.11-1.12 | 110-130 | Cures at high humidity, medium rate |
| Polyaminoamide A | 12500-17500 | 350-410 | 0.96-0.98 | 110-190 | Slow curing, low exotherm |
(Refer to full table for all types)
| Property | Minimum / Maximum | Unit |
|---|---|---|
| Compressive Strength | 80 | N/mm |
IS 9197: Sampling and Criteria for Acceptance
| Step | Action | Result |
|---|---|---|
| 1st Sample | Test as per Table 5 requirements | Pass → Accept lot |
| Fail → Test 2nd sample | ||
| 2nd Sample | Test as per Table 5 requirements | Pass → Accept lot |
| Fail → Reject entire lot |
flowchart TD
A[Sample Lot] --> B{Test 1st Sample}
B -- Pass --> C[Accept Lot]
B -- Fail --> D[Test 2nd Sample]
D -- Pass --> C
D -- Fail --> E[Reject Lot]
This approach ensures reliable quality assurance of epoxy resin materials per IS 9197.
IS 9197: Packing and Marking Key Points
Each package must be legibly marked with:
| Item | Requirement |
|---|---|
| Resin & Hardener | Separate, airtight sealed containers |
| Filler | Separate packaging |
| Marking Details | Manufacturer, product, batch/date, storage info, expiry |
| BIS Mark | Optional, indicates standard compliance |
flowchart LR
A[Resin] --> B[Sealed Airtight Container]
C[Hardener] --> D[Sealed Airtight Container]
E[Filler] --> F[Separate Packaging]
B & D & F --> G[Marking on Package]
G --> H{Marking Details}
H --> I[Manufacturer Name]
H --> J[Product Name]
H --> K[Batch/Date]
H --> L[Storage Requirements]
H --> M[Storage Life]
H --> N[Expiry Date]
IS 9197: Sampling Procedure & Conformity Criteria
| Test Result | Action |
|---|---|
| Pass first sample | Accept lot |
| Fail first sample | Prepare second sample and test |
| Pass second sample | Accept lot |
| Fail second sample | Reject lot |
flowchart TD
A[Select Sample from Lot] --> B[Test Sample]
B -->|Pass| C[Accept Lot]
B -->|Fail| D[Prepare Second Sample]
D --> E[Test Second Sample]
E -->|Pass| C
E -->|Fail| F[Reject Lot]
This ensures quality control by rigorous testing and clear acceptance/rejection rules.
Frequently Asked
Under IS 9197, epoxy resin is classified into two grades with specific classes for Grade 1:
| Class | Epoxy Content (Eq./1000g) | Weight per Epoxy Equivalent (g) | Viscosity at 27°C (Pa.s) | Specific Gravity at 27°C | Max Hydrolyzable Chlorine (%) |
|---|---|---|---|---|---|
| I | 5.0 to 5.88 | 170 to 200 | 3 to 20 | 1.05 min to 1.20 max | 9.0 |
This classification ensures proper selection for floor topping applications as per IS 9197.
Permitted Hardeners as per IS 9197 Clause 3.2 & Table 3:
| Type | Viscosity (mPa.s) | Amine Value (mg KOH/g) | Specific Gravity | Recommended Amount (g/eq epoxy) | Characteristics |
|---|---|---|---|---|---|
| Aliphatic Amine A | 10–20 | 1300–1700 | 0.97–0.99 | 16–25 | Fast reaction, strong exotherm, humidity sensitive |
| Aliphatic Amine B | 20–40 | 450–500 | - | 50–55 | Slow curing, long pot life, low exotherm |
| Aromatic Amine Adduct A | 3800–6000 | 260–290 | 1.11–1.12 | 110–130 | Cures well in humidity & low temp, medium rate |
| Polyaminoamide A | 12,500–17,500 | 350–410 | 0.96–0.98 | 110–190 | Slow curing, low exotherm |
| Amino Resin Compound A | 17,000–23,000 | 300–360 | - | 100–110 | Adjustable pot life & exotherm |
Additional Notes:
This ensures selection based on curing speed, environmental conditions, and application requirements.
IS 9197 defines the mechanical strength requirements for epoxy floor toppings in Table 5, summarized as follows (tested after 7 days curing per Clause 4.4):
| Property | Minimum/Maximum Value | Unit |
|---|---|---|
| Compressive Strength | 80 | N/mm² |
| Bond Strength | 2 | N/mm² |
| Flexural Strength | 20 | N/mm² |
| Tensile Strength | 15 | N/mm² |
| Modulus of Elasticity | 35 × 10³ | N/mm² |
| Coefficient of Thermal Expansion | ≤ 45 × 10⁻⁶ | mm/mm/°C |
| Thermal Conductivity (optional) | ≤ 1 | W/mK |
| Linear Shrinkage | ≤ 0.10 | % |
| Water Absorption | ≤ 0.50 | % |
| Resistance to Wear | Avg. ≤ 2 mm, Individual ≤ 25 mm | mm |
| Shear Strength | ≥ 3.2 | N/mm² |
Testing follows IS 9162-1979 methods (Clauses 8-17).
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This ensures epoxy
Testing Methods for Chemical Resistance and Wear Properties as per IS 9197:
Chemical Resistance (Clause 4.2):
Test the cured epoxy resin composition according to IS 9162-1979 referencing Table 1 of IS 4631-1968. This ensures the epoxy withstands specified chemicals without degradation.
Resistance to Wear (Clause 4.3):
Conduct wear tests per IS 9162-1979.
| Parameter | Limit |
|---|---|
| Average wear | ≤ 2 mm |
| Individual wear | ≤ 25 mm |
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This ensures compliance with IS 9197 for durable epoxy flooring.
Sampling and Acceptance Criteria for Epoxy Resin Compositions (IS 9197)
Sampling: Samples of epoxy resin-hardeners and compositions (including fillers and aggregates) should be taken as per Clause 5 of IS 9197, ensuring representative sampling from batches intended for floor toppings.
Acceptance Criteria: After 7 days curing, the cured samples must meet the mechanical and physical properties specified in Table 5 (Clause 4.4):
| Characteristic | Requirement | Unit |
|---|---|---|
| Compressive strength | ≥ 80 | N/mm² |
| Bond strength | ≥ 2 | N/mm² |
| Flexural strength | ≥ 20 | N/mm² |
| Tensile strength | ≥ 15 | N/mm² |
| Modulus of elasticity | ≥ 35 × 10³ | N/mm² |
| Coefficient of thermal expansion | ≤ 45 × 10⁻⁶ | mm/mm/°C |
| Thermal conductivity (opt.) | ≤ 1 | W/mK |
| Linear shrinkage | ≤ 0.10 | % |
| Water absorption | ≤ 0.50 | % |
| Resistance to wear | Avg ≤ 2, Individual ≤ 25 | mm |
| Shear strength | ≥ 3.2 | N/mm² |
This ensures the epoxy floor topping performs structurally and durably under service conditions.
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