IS 3466:1988 specifies the requirements for masonry cement used in masonry mortars for brick, stone, and concrete block masonry, as well as for rendering and plastering. It defines physical properties, packaging, sampling, and testing methods to ensure quality and performance. This standard is essential for manufacturers, suppliers, and engineers involved in masonry construction to ensure durable, workable, and non-staining mortars, excluding use in structural concrete or foundations.
Overview
IS 3466:1988 specifies the requirements for masonry cement used in masonry mortars for brick, stone, and concrete block masonry, as well as for rendering and plastering. It defines physical properties, packaging, sampling, and testing methods to ensure quality and performance. This standard is essential for manufacturers, suppliers, and engineers involved in masonry construction to ensure durable, workable, and non-staining mortars, excluding use in structural concrete or foundations.
Audience
Contents
Structure
Scope:
| Property | Requirement |
|---|---|
| Fineness (Residue on 45-micron sieve) | Max 15% (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min, Final ≤ 24 h |
| Soundness | Le-Chatelier expansion ≤ 10 mm; Autoclave expansion ≤ 1% |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand) | 7 days ≥ 2.5 MPa; 28 days ≥ 5 MPa |
| Air Content (Mortar) | Min 6% |
| Water Retention (Mortar flow after suction) | Min 60% of original flow |
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 - 150 | 20 |
| 151 - 280 | 32 |
| 281 - 500 | 50 |
| 501 - 1,200 | 80 |
| 1,201 - 3,200 | 125 |
| > 3,201 | 200 |
flowchart TD
A[Masonry Cement] --> B[Physical Properties]
A --> C[Mechanical Properties]
A --> D[Sampling & Tolerance]
B --> E[Fineness, Setting Time, Soundness]
C --> F[Compressive Strength, Air Content, Water Retention]
D --> G[Sample Size & Tolerance Tables]
This summary covers the scope, key physical and mechanical requirements, and sampling/tolerance criteria from IS 3466.
Scope:
IS 3466 specifies requirements for masonry cement used in masonry construction.
| Characteristic | Requirement |
|---|---|
| Fineness | Max 15% residue on 45-micron IS sieve (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min; Final ≤ 24 h |
| Soundness | Le-Chatelier expansion ≤ 10 mm; Autoclave expansion ≤ 1% |
| Compressive Strength | Mortar cubes (1:3 cement:sand) of 50 mm size: <br>- 7 days ≥ 2.5 MPa <br>- 28 days ≥ 5 MPa |
| Air Content | Min 6% (mortar 1:3 cement:sand by volume) |
| Water Retention | Min 60% of original flow after suction (mortar 1:3 cement:sand) |
Standard sand conforms to IS 650:1965.
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| > 3,200 | 200 |
Tolerance for wagon/truck load (20-25 tonnes): 0 to +0.5% on net mass.
flowchart TD
A[Masonry Cement] --> B[Fineness ≤ 15% residue]
A --> C[Setting Time: Initial ≥ 90 min, Final ≤ 24 h]
A --> D[Soundness: Le-Chatelier ≤ 10 mm, Autoclave ≤ 1%]
A --> E[Compressive Strength: 7d ≥ 2.5 MPa, 28
IS 3466: Definitions & Key Specifications for Masonry Cement
| Characteristic | Requirement |
|---|---|
| Fineness | Max 15% residue on 45-micron IS sieve (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial min: 90 min<br>Final max: 24 hours |
| Soundness | Le-Chatelier expansion max: 10 mm<br>Autoclave expansion max: 1% |
| Compressive Strength | Mortar cubes (1 part masonry cement: 3 parts standard sand)<br>7 days min: 2.5 MPa<br>28 days min: 5 MPa |
| Air Content | Min 6% in mortar mix |
| Water Retention | Min 60% of original flow after suction |
Standard sand conforms to IS 650:1965.
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| 3,201 and over | 200 |
flowchart TD
A[Masonry Cement] --> B[Fineness ≤ 15% residue]
A --> C[Setting Time: Initial ≥ 90 min, Final ≤ 24 hrs]
A --> D[Soundness: Le-Chatelier ≤ 10 mm, Autoclave ≤ 1%]
A --> E[Compressive Strength: 7d ≥ 2.5 MPa
IS 3466: Physical Requirements for Masonry Cement
| Characteristic | Requirement |
|---|---|
| Fineness (Residue on 45-micron IS Sieve, wet sieving) | Max 15% |
| Setting Time (Vicat Apparatus) | Initial: Min 90 min<br>Final: Max 24 h |
| Soundness | Le-Chatelier expansion: Max 10 mm<br>Autoclave expansion: Max 1% |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand by volume) | 7 days: Min 2.5 MPa<br>28 days: Min 5 MPa |
| Air Content (Mortar 1:3 cement:sand) | Min 6% |
| Water Retention (Flow after suction, mortar 1:3) | Min 60% of original flow |
Notes:
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| > 3,200 | 200 |
This summary ensures compliance with IS 3466 physical requirements for masonry cement quality control.
IS 3466: Non-staining Masonry Cement - Key Specifications & Physical Requirements
| Characteristic | Requirement |
|---|---|
| Fineness (Residue on 45-micron sieve, wet sieving) | Max 15% |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min<br>Final ≤ 24 h |
| Soundness | Le-Chatelier expansion ≤ 10 mm<br>Autoclave expansion ≤ 1% |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand by volume) | 7 days ≥ 2.5 MPa<br>28 days ≥ 5 MPa |
| Air Content (Mortar 1:3 cement:sand) | Min 6% |
| Water Retention (Flow after suction of mortar 1:3 cement:sand) | Min 60% of original flow |
flowchart TD
A[Masonry Cement] --> B[Fineness ≤ 15%]
A --> C[Setting Time: Initial ≥ 90 min, Final ≤ 24 h]
A --> D[Soundness: Le-Chatelier ≤ 10 mm, Autoclave ≤ 1%]
A --> E[Compressive Strength: 7d ≥ 2.5 MPa, 28d ≥ 5 MPa]
A --> F[Air Content ≥ 6%]
A --> G[Water Retention ≥ 60%]
B & C & D & E & F & G --> H[Conforms to IS 3466 for Non-staining Masonry Cement]
This summary aids specification, testing, and quality control for non-staining masonry cement per IS 3466.
IS 3466: Storage and Handling of Cement - Key Points
| Property | Requirement |
|---|---|
| Fineness (Residue on 45μ IS Sieve) | Max 15% (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min, Final ≤ 24 hrs |
| Soundness | Le-Chatelier expansion ≤ 10 mm |
| Autoclave expansion ≤ 1% | |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand) | 7 days ≥ 2.5 MPa, 28 days ≥ 5 MPa |
| Air Content (Mortar) | ≥ 6% |
| Water Retention (Mortar flow after suction) | ≥ 60% of original flow |
flowchart TD
A[Receive Cement] --> B[Store in Weather-tight Building]
B --> C[Allow Easy Access for Inspection]
B --> D[Protect from Dampness]
D --> E[Sample for Testing]
E --> F{Test within 4 weeks?}
F -- Yes --> G[Test Cement]
F -- No --> H[Store Sample in Airtight Container]
Note: Use standard sand per IS 650 for testing. Proper storage and handling ensure cement quality and durability.
IS 3466: Manufacturer's Certificate Key Specifications
| Characteristic | Requirement | Test Method |
|---|---|---|
| Fineness | Max 15% residue on 45-micron IS sieve (wet sieving) | Clause 3.1.1 |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min, Final ≤ 24 h | Clause 3.1.1 |
| Soundness | Le-Chatelier expansion ≤ 10 mm, Autoclave expansion ≤ 1% | Clause 3.1.1 |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand) | 7 days ≥ 2.5 MPa, 28 days ≥ 5 MPa | Clause 3.1.1 |
| Air Content (Mortar) | ≥ 6% | Clause 3.1.1 |
| Water Retention (Mortar) | ≥ 60% of original flow after suction | Clause 3.1.1 |
Additional Notes:
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100-150 | 20 |
| 151-280 | 32 |
| 281-500 | 50 |
| 501-1200 | 80 |
| 1201-3200 | 125 |
| >3200 | 200 |
flowchart TD
A[Manufacturer's Certificate] --> B[Fineness Test]
A --> C[Setting Time Test]
A --> D[Soundness Test]
A --> E[Compressive Strength Test]
A --> F[Air Content Test]
A --> G[Water Retention Test]
A --> H[Sampling & Mass Tolerance]
This ensures cement meets IS 346
IS 3466: Basis of Purchase - Key Specifications & Tables
| Characteristic | Requirement |
|---|---|
| Fineness | Max 15% residue on 45-micron sieve (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min, Final ≤ 24 hours |
| Soundness | Le-Chatelier expansion ≤ 10 mm; Autoclave expansion ≤ 1% |
| Compressive Strength | Mortar cubes (50 mm), 1:3 cement:sand by volume: <br>7 days ≥ 2.5 MPa, 28 days ≥ 5 MPa |
| Air Content | Min 6% (mortar 1:3 masonry cement to standard sand) |
| Water Retention | Flow after suction ≥ 60% of original flow (same mortar mix) |
flowchart TD
A[Masonry Cement] -->|1 part| M[Mortar Mix]
B[Standard Sand] -->|3 parts| M
M --> C[Test Specimens]
C --> D[Physical Tests]
D -->|Fineness, Setting Time, Soundness| E[Acceptance Criteria]
D -->|Compressive Strength, Air Content, Water Retention| E
This summary ensures compliance with IS 3466 "Basis of Purchase" requirements for masonry cement.
IS 3466: Packing and Marking - Key Specifications
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| 3,201 and over | 200 |
| Parameter | Value/Requirement |
|---|---|
| Net mass per bag | ≥ 50 kg |
| Sample size (based on batch) | See table above |
| Mass tolerance (bulk load) | 0 to +0.5% for 20-25 tonnes load |
| Sampling method | Random (IS 4905-1968) |
| Marking | Standard Mark (optional, BIS governed) |
flowchart TD
A[Packed Cement Bags] --> B{Batch Size}
B -->|100-150| C[Sample 20 Bags]
B -->|151-280| D[Sample 32 Bags]
B -->|281-500| E[Sample 50 Bags]
B -->|501-1200| F[Sample 80 Bags]
B -->|1201-3200| G[Sample 125 Bags
IS 3466 Sampling Key Points
Sampling method: As per IS 3535-1986, sampling procedures must ensure representativeness and randomness.
Sample size (Clause 8.2, Appendix A):
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| 3,201 and over | 200 |
Mass requirement: Average net mass of cement per bag in the sample ≥ 50 kg.
Random selection: Bags must be selected randomly per IS 4905-1968.
Facilities and labor: Manufacturer/supplier must provide all facilities, labor, and materials for sampling and identification (Clause 9.3).
Testing timeline: Tests on the sample should be done as expeditiously as possible after sampling (Clause 10.4.2).
flowchart TD
A[Batch of Cement Bags] --> B[Random Sampling as per IS 4905]
B --> C[Sample Size per Batch Size Table]
C --> D[Average Mass ≥ 50 kg per bag]
D --> E[Testing of Sample (IS 3535)]
E --> F[Results & Identification]
This ensures quality control and compliance in cement packaging and testing.
IS 3466 - Testing Procedures: Key Formulas, Tables, and Specifications
| Characteristic | Requirement |
|---|---|
| Fineness (Residue on 45-micron sieve) | Max 15% (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial: Min 90 min <br> Final: Max 24 h |
| Soundness | Le-Chatelier expansion: Max 10 mm <br> Autoclave expansion: Max 1% |
| Compressive Strength (Mortar cubes 50 mm, 1:3 cement:sand by volume) | 7 days: Min 2.5 MPa <br> 28 days: Min 5 MPa |
| Air Content (Mortar 1:3) | Min 6% |
| Water Retention (Mortar 1:3) | Min 60% of original flow after suction |
Standard sand shall conform to IS 650:1965.
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| >3,201 | 200 |
Refer IS 4905:1968 for random selection.
flowchart TD
A[Sampling of Cement Bags] --> B[Physical Tests]
B --> C[Fineness Test]
B --> D[Setting Time Test]
B --> E[Soundness Test]
B --> F[Compressive Strength Test]
B --> G[Air Content Test]
B
IS 3466: Tolerance Requirements for Mass of Cement Packed in Bags
Average net mass per bag:
Tolerance on net mass for wagon/truck load (20 to 25 tonnes):
| Batch Size (bags) | Sample Size (bags) |
|---|---|
| 100 to 150 | 20 |
| 151 to 280 | 32 |
| 281 to 500 | 50 |
| 501 to 1,200 | 80 |
| 1,201 to 3,200 | 125 |
| > 3,200 | 200 |
[ \text{Tolerance range} = \text{Nominal mass} \times (1 + \text{Tolerance %}) ]
Example: For 50 kg bag with +0.5% tolerance, max mass = 50 × 1.005 = 50.25 kg
flowchart TD
A[Batch Size] --> B{Select Sample Size}
B -->|100-150| C[20 Bags]
B -->|151-280| D[32 Bags]
B -->|281-500| E[50 Bags]
B -->|501-1200| F[80 Bags]
B -->|1201-3200| G[125 Bags]
B -->|>3200| H[200 Bags]
C & D & E & F & G & H --> I[Random Sampling per IS 4905]
I --> J[Check Average Mass ≥ 50 kg]
J --> K[Check Tolerance: 0 to +0.5%]
Note:
Frequently Asked
According to IS 3466, masonry cement must meet the following key physical properties (Table 1, Clause 3.1):
| Characteristic | Requirement |
|---|---|
| Fineness | Max 15% residue on 45-micron sieve (wet sieving) |
| Setting Time (Vicat Apparatus) | Initial ≥ 90 min, Final ≤ 24 hours |
| Soundness | Le-Chatelier expansion ≤ 10 mm, Autoclave expansion ≤ 1% |
| Compressive Strength | Mortar cubes (50 mm) with 1:3 cement:sand mix: <br> - 7 days ≥ 2.5 MPa <br> - 28 days ≥ 5 MPa |
| Air Content | Minimum 6% in mortar mix |
| Water Retention | Minimum 60% of original flow after suction in mortar |
Standard sand for testing must conform to IS 650:1965.
These ensure proper workability, durability, and strength for masonry applications.
IS 3466 on False Set in Masonry Cement:
Definition: False set is identified by the ratio of final penetration (after 5 minutes of mixing) to initial penetration (at 20 seconds), expressed as a percentage.
Control Criterion (Clause 3.1.1):
[
\text{False set ratio} = \frac{\text{Final penetration at 5 min}}{\text{Initial penetration at 20 sec}} \times 100 \geq 50%
]
If false set occurs, the cement must be retested for initial and final setting times after breaking the false set, following IS 4031 (1988) methods.
These setting times must meet the requirements in Table 1 of IS 3466:
| Parameter | Requirement |
|---|---|
| False set penetration ratio | ≥ 50% |
| Initial setting time (after break) | ≥ 90 minutes |
| Final setting time (after break) | ≤ 24 hours |
This ensures that false setting does not affect the usability and durability of masonry cement.
Packaging and Marking Requirements for Masonry Cement (IS 3466: Clause 8.1 & 8.1.3)
Bag Types: Masonry cement shall be packed in bags conforming to Indian Standards such as:
Marking on Bags:
Distinctive Mark:
This ensures easy identification and maintains quality during storage and transport.
IS 3466 prescribes the following testing methods for verifying masonry cement quality, as per IS 4031-1988:
| Characteristic | Test Method / Apparatus | Requirement |
|---|---|---|
| Fineness | Wet sieving on 45-micron IS sieve | Max 15% residue |
| Setting Time | Vicat Apparatus | Initial ≥ 90 min, Final ≤ 24 h |
| Soundness | Le-Chatelier method & Autoclave | Expansion ≤ 10 mm (Le-Chatelier), ≤ 1% (Autoclave) |
| Compressive Strength | Mortar cubes (50 mm), 1:3 cement to standard sand | ≥ 2.5 MPa (7 days), ≥ 5 MPa (28 days) |
| Air Content | Mortar test | ≥ 6% air content |
| Water Retention | Flow test after suction on mortar | ≥ 60% of original flow |
These tests ensure physical and mechanical properties meet the standard for durable masonry work.
According to IS 3466:1988 and its amendments, masonry cement is explicitly NOT suitable for structural concrete or foundation work.
Key points from the code:
Clause 8.4 clearly states:
"The words 'Not for structural concrete, flooring and foundation' shall be marked on each bag or package."
Masonry cement is designed primarily for masonry mortar applications like brickwork and plastering, not for load-bearing concrete.
Use ordinary Portland cement (OPC) or other structural-grade cements conforming to IS 269 or IS 12269 for such applications.
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