IS 14695:1999 specifies requirements for glass fibre base coal tar pitch outerwraps used primarily for corrosion protection of buried mild steel pipelines. This standard details the composition, physical properties, testing methods, and quality criteria for outerwraps made from glass fibre mats coated with plasticized coal tar enamel and mineral powder surfacing. It is essential for manufacturers, quality inspectors, and engineers involved in pipeline protection to ensure durability and resistance under field conditions.
Overview
IS 14695:1999 specifies requirements for glass fibre base coal tar pitch outerwraps used primarily for corrosion protection of buried mild steel pipelines. This standard details the composition, physical properties, testing methods, and quality criteria for outerwraps made from glass fibre mats coated with plasticized coal tar enamel and mineral powder surfacing. It is essential for manufacturers, quality inspectors, and engineers involved in pipeline protection to ensure durability and resistance under field conditions.
Audience
Contents
Structure
IS 14695: Scope & Key Specifications
Scope: IS 14695 covers specifications for glass fibre base outerwraps used in insulation systems.
Weight Specification (Clause 5.2 & Table 2):
For 10 m² of glass fibre base outerwraps:
| Untreated Base (kg) | Treated Base (kg) | Total Dry Weight including Surfacing (kg) |
|---|---|---|
| 0.4 | 4.5 | 5.5 |
Rounding Off (Clause 2.4):
Final test or analysis values must be rounded per IS 2:1960 rules, retaining the same number of significant figures as specified.
flowchart TD
A[Start: Glass Fibre Outerwrap] --> B[Measure Ingredients Weight]
B --> C{Check Weight per 10 m²}
C -->|Untreated Base ≥ 0.4 kg| D
C -->|Treated Base ≥ 4.5 kg| D
D --> E[Total Weight ≥ 5.5 kg]
E --> F[Apply IS 2:1960 Rounding]
F --> G[Compliance Confirmed]
This ensures the product meets IS 14695 requirements for insulation outerwraps.
IS 14695 - Clause 2: Normative References Summary
| Aspect | Reference Standard | Notes |
|---|---|---|
| Rounding off numerical data | IS 2:1960 | Round final test/analysis results; maintain significant figures as specified. |
| Technical Committee Details | Annex B of IS 14695 | Composition of committee responsible for the standard. |
When applying IS 14695, cross-check all referenced standards for updates to ensure full compliance.
flowchart TD
A[IS 14695 Standard] --> B[Referenced Standards]
B --> C[Check Latest Editions]
A --> D[Rounding Off Rules]
D --> E[IS 2:1960]
E --> F[Maintain Significant Figures]
IS 14695: Materials and Composition Key Points
| Characteristic | Requirement |
|---|---|
| Weight per unit area | ≥ 40 g/m² |
| Nominal thickness | 0.50 mm ± 0.1 mm |
| Breaking strength | ≥ 45 kgf/150 mm (longitudinal) |
| Porosity | 0.6 mm to 1.9 mm |
| Temperature resistance | Stable under 280°C hot bitumen for 1 min |
| Untreated Base (kg) | Treated Base (kg) | Total Dry Weight (kg) |
|---|---|---|
| 0.4 | 4.5 | 5.5 |
| Property | Requirement | Test Method (IS) |
|---|---|---|
| Breaking strength (kg) | Wrap ≥ 30, Weft ≥ 15 | 13826 (Part 1) |
| Pliability (after 3h at 5°C) | No cracks on unrolling; no rupture >5 mm | 13826 (Part 2) |
graph TD
A[Glass Fibre Tissue] --> B[Borosilicate Glass Fibres]
A --> C[Phenolic Resin Bond]
D[Coal Tar Pitch
IS 14695: Physical & Mechanical Requirements Summary
| Property | Requirement | Test Method (IS) |
|---|---|---|
| Breaking Strength | Wrap: ≥ 30 kg<br>Weft: ≥ 15 kg | IS 13826 (Part 1) |
| Pliability (after 3h at 5°C) | No cracks on unrolling<br>Surface rupture ≤ 5 mm allowed | IS 13826 (Part 2) |
| Untreated Base (kg) | Treated Base (kg) | Total Dry Weight (kg) |
|---|---|---|
| 0.4 | 4.5 | 5.5 |
| Property | Requirement | Test Method |
|---|---|---|
| Weight per unit area | ≥ 40 g/m² | A-1 |
| Thickness | 0.50 mm ± 0.1 mm | A-2 |
| Breaking strength | ≥ 45 kgf/150 mm (longitudinal) | A-3 |
| Porosity | 0.6 mm to 1.9 mm |
IS 14695: Dimensions and Weight of Glass Fibre Base Outerwraps
| Untreated Base (kg) | Treated Base (kg) | Total Dry Weight Including Surfacing (kg) |
|---|---|---|
| 0.4 | 4.5 | 5.5 |
Surfacing Material:
Outerwrap Composition:
| Property | Minimum Requirement | Test Method (IS Ref) |
|---|---|---|
| Breaking Strength (kg) | Wrap: 30, Weft: 15 | IS 13826 (Part 1) |
| Pliability (after 3h at 5°C) | No cracks on unrolling; no rupture >5 mm | IS 13826 (Part 2) |
[ \text{Weight per 10 m}^2 = \text{Base Weight} + \text{Surfacing Material Weight} ]
Where base weight and surfacing weights are as per Table 2 and Clause 2.3.
flowchart TD
A[Glass Fibre Mat] --> B[Coated with Plasticized Coal Tar Enamel]
B --> C[Dusted with Mineral Powder]
C --> D[Finished Outerwrap]
D --> E[Weight & Dimension Check]
E --> F[Mechanical Testing]
This ensures compliance with IS 14695 for durable and standardized glass fibre outerwraps.
Key Specifications & Requirements for Glass Fibre Outerwraps (IS 14695)
| Untreated Base (kg) | Treated Base (kg) | Total Dry Weight (kg) Including Surfacing |
|---|---|---|
| 0.4 | 4.5 | 5.5 |
| Property | Requirement | Test Method (IS) |
|---|---|---|
| Breaking Strength | Wrap: Min 30 kg | IS 13826 (Part 1) |
| Weft: Min 15 kg | ||
| Pliability after Conditioning | No cracks on unrolling after 3 hrs at 5°C | IS 13826 (Part 2) |
| Surface rupture > 5 mm = Fail |
flowchart LR
A[Sampling per IS 4905] --> B[Select rolls randomly]
B --> C[Measure weights]
C --> D[Calculate average weight]
D --> E[Verify weight ≥ specified in Table 2]
E --> F[Conduct tests per IS 13826]
F --> G{Pass?}
G -- Yes --> H[Accept batch]
G -- No --> I[Reject batch]
IS 14695: Sampling and Criteria for Conformity
| No. of Rolls in Lot | Sample Size (Rolls) | Permissible Defective Rolls | Sub-Sample Size (Rolls) |
|---|---|---|---|
| Up to 100 | 5 | 0 | 2 |
| 101 to 150 | 8 | 0 | 3 |
| 151 to 300 | 13 | 0 | 4 |
| 301 to 500 | 20 | 1 | 5 |
| 501 to 1,000 | 32 | 2 | 6 |
| 1,001 to 3,000 | 50 | 3 | 8 |
| Above 3,000 | 80 | 5 | 10 |
flowchart LR
A[Select Lot Size] --> B{Determine Sample Size}
B --> C[Select Rolls for Sample]
C --> D[Test Rolls]
D --> E{Defective Rolls ≤ Permissible?}
E -->|Yes| F[Lot Accepted]
E -->|No| G[Lot Rejected]
This ensures quality control by statistical sampling per IS 14695.
IS 14695: Marking and Packaging Key Points
Each package must be legibly and indelibly marked with:
| Aspect | Requirement |
|---|---|
| Marking | Manufacturer, dimensions, weight, batch, date, BIS mark |
| Packaging | Clean rolls, square cut, no telescoping, cardboard separators & end shields |
| Breaking Strength | (X - 0.6R \geq) Min. strength (Wrap 30 kg, Weft 15 kg) |
| Pliability | No cracks after conditioning; rupture ≤5 mm |
flowchart TD
A[Roll Manufacturing] --> B[Marking]
B --> C{Marking Details}
C -->|Manufacturer| D[Identification]
C -->|Dimensions| E[Length, Width, Weight]
C -->|Batch Info| F[Batch No. & Date]
B --> G[BIS Certification Mark]
A --> H[Packaging]
H --> I[Clean, Smooth, Square Cut Rolls]
H --> J[Cardboard Separators & End Shields]
H --> K[Prevent Damage During Transport]
This ensures
IS 14695: Key Methods & Specifications for Testing Glass Fibre Tissue
| Property | Requirement (kg) | Test Ref. |
|---|---|---|
| Breaking Strength | Wrap: ≥ 30 | IS 13826 Part 1 |
| Weft: ≥ 15 |
flowchart LR
A[Select Specimens] --> B[Measure Weight]
B --> C[Calculate Weight per 10 m²]
A --> D[Measure Thickness]
A --> E[Test Tensile Strength]
A --> F[Test Pliability]
A --> G[Test Air Permeability]
A --> H[Test Temperature Resistance]
This summarizes essential test methods and requirements per IS 14695 for glass fibre tissue quality control.
Frequently Asked
Physical Properties of Glass Fibre Tissue as per IS 14695:
Composition: Thin, flexible, uniformly bonded mat of chemically resistant borosilicate staple glass fibres, randomly distributed and bonded with phenolic thermosetting resin (Clause 3.1).
Thickness Measurement (Clause 6.45):
Breaking Strength (Table 3, Clause 6):
Pliability (Table 3, Clause 6):
Porosity & Air Permeability:
| Property | Requirement | Test Reference |
|---|---|---|
| Thickness | Measured under 35 g/cm² pressure | Clause 6.45 |
| Breaking Strength | Wrap ≥ 30 kg, Weft ≥ 15 kg | IS 13826 (Part 1) |
| Pliability | No cracks after 3h at 5°C | IS 13826 (Part 2) |
| Composition | Borosilicate glass fibres + phenolic resin | Clause 3.1 |
| Air Permeability | Pressure drop at 1 m/s airflow | Clause 4.3 |
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According to IS 14695, the thickness of the glass fibre base outerwrap is measured as follows:
This method is detailed in Clause 6.45 and illustrated in Fig. 1 of the standard.
| Parameter | Value |
|---|---|
| Foot & Anvil Area | 6.45 cm² |
| Pressure Applied | 35 g/cm² |
| Dial Gauge Least Count | 0.01 mm |
This ensures consistent and precise thickness measurement of the glass fibre outerwrap.
Criteria for Sampling and Acceptance of Rolls in a Batch (IS 14695)
Sampling Procedure (Clause 7.1.2.1):
Sample Size & Acceptance (Table 4, Clause 7.1.3.2):
| Lot Size (No. of Rolls) | Sample Size (Rolls) | Max Defective Rolls Allowed | Sub-Sample Size (Rolls) |
|---|---|---|---|
| Up to 100 | 5 | 0 | 2 |
| 101 to 150 | 8 | 0 | 3 |
| 151 to 300 | 13 | 0 | 4 |
| 301 to 500 | 20 | 1 | 5 |
| 501 to 1,000 | 32 | 2 | 6 |
| 1,001 to 3,000 | 50 | 3 | 8 |
| Above 3,000 | 80 | 5 | 10 |
Acceptance Criteria (Clause 7.1.3.1):
Additional Notes:
This ensures quality control and uniformity in batch acceptance.
Mandatory Test for Temperature Resistance of Outerwrap (IS 14695):
| Property | Requirement | Test Condition | Reference |
|---|---|---|---|
| Temperature Resistance | Unaffected under load | Hot bitumen at 280°C for 1 min | IS 14695 Clause 1.9 |
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In brief: The mandatory temperature resistance test per IS 14695 is the exposure of the outerwrap to hot bitumen at 280°C for 1 minute under load, ensuring no adverse effects.
Mineral Fillers and Surfacing Powders for Outerwrap (IS 14695):
Mineral Filler (Clause 3.3):
Mineral Powder for Surfacing (Clause 3.4.1):
Additional Info (Clause 2.3):
Purpose:
The mineral powder dusting prevents layers from sticking and ensures a smooth, uniform outerwrap surface free from defects.
| Material | Particle Size (IS Sieve) | Notes |
|---|---|---|
| Mineral Filler | 75 microns | Insoluble inert mineral |
| Talc/Mica | 600 microns | Powdered mineral matter |
| Sand | 250 microns | Alternative for surfacing |
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