IS 146951999AI Search Enabled✦ AI Generated

Glass Fibre Base Coal Tar Pitch Outerwrap

IS 14695:1999 specifies requirements for glass fibre base coal tar pitch outerwraps used primarily for corrosion protection of buried mild steel pipelines. This standard details the composition, physical properties, testing methods, and quality criteria for outerwraps made from glass fibre mats coated with plasticized coal tar enamel and mineral powder surfacing. It is essential for manufacturers, quality inspectors, and engineers involved in pipeline protection to ensure durability and resistance under field conditions.

9Sections
90Clauses Indexed
AI Search Ready
1999Edition
Waterproofing and Damp-ProofingCategory
Alternative search terms: IS 14695 PDF, IS 14695 pdf free download, IS 14695 free download pdf, IS14695 PDF, IS-14695 PDF, IS 14695 1999 PDF, IS 14695:1999 PDF, IS 14695-1999 PDF, IS 14695 (1999) PDF, IS 14695 1999 edition PDF, IS 14695 edition 1999 PDF

What This Standard Covers

IS 14695:1999 specifies requirements for glass fibre base coal tar pitch outerwraps used primarily for corrosion protection of buried mild steel pipelines. This standard details the composition, physical properties, testing methods, and quality criteria for outerwraps made from glass fibre mats coated with plasticized coal tar enamel and mineral powder surfacing. It is essential for manufacturers, quality inspectors, and engineers involved in pipeline protection to ensure durability and resistance under field conditions.

Who Uses This Standard

  • Pipeline Engineers
  • Corrosion Protection Specialists
  • Quality Control Inspectors
  • Manufacturers of Pipeline Coatings
  • Civil and Mechanical Engineers
  • Materials Testing Laboratories
  • Procurement Professionals in Oil & Gas

Key Topics Covered

Composition of glass fibre base membrane
Physical properties of glass fibre tissue
Coal tar pitch characteristics
Mineral fillers and surfacing powders
Dimensional and weight requirements
Testing methods for thickness, strength, porosity, and pliability
Sampling procedures and conformity criteria
Marking and packaging requirements
Temperature resistance testing
Quality control for rolls and batches
Handling and storage guidelines
Standards referenced for testing methods

Table of Contents

1Scope

IS 14695: Scope & Key Specifications

  • Scope: IS 14695 covers specifications for glass fibre base outerwraps used in insulation systems.

  • Weight Specification (Clause 5.2 & Table 2):
    For 10 m² of glass fibre base outerwraps:

    Untreated Base (kg)Treated Base (kg)Total Dry Weight including Surfacing (kg)
    0.44.55.5
  • Rounding Off (Clause 2.4):
    Final test or analysis values must be rounded per IS 2:1960 rules, retaining the same number of significant figures as specified.


Summary:

  • Ensure minimum weights as per Table 2 for compliance.
  • Use IS 2:1960 rounding rules for all calculations and test results.
  • The standard applies primarily to glass fibre base outerwraps in insulation.
flowchart TD
    A[Start: Glass Fibre Outerwrap] --> B[Measure Ingredients Weight]
    B --> C{Check Weight per 10 m²}
    C -->|Untreated Base ≥ 0.4 kg| D
    C -->|Treated Base ≥ 4.5 kg| D
    D --> E[Total Weight ≥ 5.5 kg]
    E --> F[Apply IS 2:1960 Rounding]
    F --> G[Compliance Confirmed]

This ensures the product meets IS 14695 requirements for insulation outerwraps.

2Normative References

IS 14695 - Clause 2: Normative References Summary

  • Purpose: Lists standards referenced in IS 14695; these referenced standards form an integral part of IS 14695.
  • Revision Note: Always check for the latest editions of referenced standards for up-to-date compliance.
  • Rounding Off:
    • Follow IS 2:1960 for rounding numerical values.
    • Retain the same number of significant figures as specified in IS 14695.

Key Points for Compliance Checking:

AspectReference StandardNotes
Rounding off numerical dataIS 2:1960Round final test/analysis results; maintain significant figures as specified.
Technical Committee DetailsAnnex B of IS 14695Composition of committee responsible for the standard.

Practical Tip:

When applying IS 14695, cross-check all referenced standards for updates to ensure full compliance.

flowchart TD
    A[IS 14695 Standard] --> B[Referenced Standards]
    B --> C[Check Latest Editions]
    A --> D[Rounding Off Rules]
    D --> E[IS 2:1960]
    E --> F[Maintain Significant Figures]
3Materials and Composition

IS 14695: Materials and Composition Key Points

1. Glass Fibre Tissue (Base Membrane) - Clause 3.1 & Table 1

  • Composition: Borosilicate staple glass fibres bonded with phenolic resin.
  • Physical Properties:
CharacteristicRequirement
Weight per unit area≥ 40 g/m²
Nominal thickness0.50 mm ± 0.1 mm
Breaking strength≥ 45 kgf/150 mm (longitudinal)
Porosity0.6 mm to 1.9 mm
Temperature resistanceStable under 280°C hot bitumen for 1 min

2. Glass Fibre Outerwraps - Clause 5.2 & Table 2

  • Minimum weight for 10 m²:
Untreated Base (kg)Treated Base (kg)Total Dry Weight (kg)
0.44.55.5
  • Sampling method: Random selection per IS 4905; average weight calculated for 10 m².

3. Coal Tar Pitch - Clause 3.2

  • Softening point: 80°C to 90°C (IS 1205)
  • Penetration at 25°C: 20 to 30 (IS 1203)
  • Ash on incineration at 800°C: ≤ 15% by mass (IS 1217)

4. Glass Fibre Outerwrap Properties - Clause 6 & Table 3

PropertyRequirementTest Method (IS)
Breaking strength (kg)Wrap ≥ 30, Weft ≥ 1513826 (Part 1)
Pliability (after 3h at 5°C)No cracks on unrolling; no rupture >5 mm13826 (Part 2)

Summary Diagram of Material Composition

graph TD
  A[Glass Fibre Tissue] --> B[Borosilicate Glass Fibres]
  A --> C[Phenolic Resin Bond]
  D[Coal Tar Pitch
4Physical and Mechanical Requirements

IS 14695: Physical & Mechanical Requirements Summary


1. Glass Fibre Outerwraps (Clause 6, Table 3)

PropertyRequirementTest Method (IS)
Breaking StrengthWrap: ≥ 30 kg<br>Weft: ≥ 15 kgIS 13826 (Part 1)
Pliability (after 3h at 5°C)No cracks on unrolling<br>Surface rupture ≤ 5 mm allowedIS 13826 (Part 2)

2. Sampling & Conformity (Clause 7.1.3.1)

  • Calculate average (X) and range (R) of breaking strength separately for wrap and weft.
  • Criterion:
    [ X - 0.6R \geq \text{Specified Minimum Strength} ]
  • All samples must individually satisfy pliability requirements.

3. Glass Fibre Base Outerwrap Weight (Clause 5.2, Table 2)

Untreated Base (kg)Treated Base (kg)Total Dry Weight (kg)
0.44.55.5
  • Weight measured for 10 m² area.
  • Sampling follows IS 4905 for randomness.

4. Coal Tar Pitch (Clause 3.2)

  • Softening point: 80–90°C (IS 1205)
  • Penetration at 25°C: 20–30 (IS 1203)
  • Ash content ≤ 15% by mass (IS 1217)

5. Glass Fibre Tissue (Clause 3.1, Table 1)

PropertyRequirementTest Method
Weight per unit area≥ 40 g/m²A-1
Thickness0.50 mm ± 0.1 mmA-2
Breaking strength≥ 45 kgf/150 mm (longitudinal)A-3
Porosity0.6 mm to 1.9 mm
5Dimensions and Weight

IS 14695: Dimensions and Weight of Glass Fibre Base Outerwraps

Key Specifications:

  • Weight per 10 m² (Table 2):
Untreated Base (kg)Treated Base (kg)Total Dry Weight Including Surfacing (kg)
0.44.55.5
  • Surfacing Material:

    • Sand: 2.3 kg/10 m² (Clause 2.3 c)
  • Outerwrap Composition:

    • Glass fibre mat coated with plasticized coal tar enamel.
    • Dusting with mineral powder to prevent sticking.
    • Finished surface must be smooth and defect-free.

Weight Determination (Clause 5.2.1):

  • Randomly select rolls as per IS 4905.
  • Average roll weight → Calculate weight for 10 m².

Mechanical Requirements (Table 3):

PropertyMinimum RequirementTest Method (IS Ref)
Breaking Strength (kg)Wrap: 30, Weft: 15IS 13826 (Part 1)
Pliability (after 3h at 5°C)No cracks on unrolling; no rupture >5 mmIS 13826 (Part 2)

Summary Formula for Weight per unit area:

[ \text{Weight per 10 m}^2 = \text{Base Weight} + \text{Surfacing Material Weight} ]

Where base weight and surfacing weights are as per Table 2 and Clause 2.3.


flowchart TD
    A[Glass Fibre Mat] --> B[Coated with Plasticized Coal Tar Enamel]
    B --> C[Dusted with Mineral Powder]
    C --> D[Finished Outerwrap]
    D --> E[Weight & Dimension Check]
    E --> F[Mechanical Testing]

This ensures compliance with IS 14695 for durable and standardized glass fibre outerwraps.

6Other Requirements of Glass Fibre Outerwraps

Key Specifications & Requirements for Glass Fibre Outerwraps (IS 14695)

1. Weight Requirements (Clause 5.2, Table 2)

  • For 10 m² of outerwrap:
    Untreated Base (kg)Treated Base (kg)Total Dry Weight (kg) Including Surfacing
    0.44.55.5

2. Physical Properties (Clause 6, Table 3)

PropertyRequirementTest Method (IS)
Breaking StrengthWrap: Min 30 kgIS 13826 (Part 1)
Weft: Min 15 kg
Pliability after ConditioningNo cracks on unrolling after 3 hrs at 5°CIS 13826 (Part 2)
Surface rupture > 5 mm = Fail

3. Sampling (Clause 5.2.1)

  • Select rolls randomly per IS 4905.
  • Compute average weight from selected rolls.
  • Calculate weight per 10 m² from average.

Summary:

  • Ensure minimum weight per 10 m² as above.
  • Confirm breaking strength and pliability per IS 13826.
  • Use random sampling as per IS 4905 for quality control.
flowchart LR
    A[Sampling per IS 4905] --> B[Select rolls randomly]
    B --> C[Measure weights]
    C --> D[Calculate average weight]
    D --> E[Verify weight ≥ specified in Table 2]
    E --> F[Conduct tests per IS 13826]
    F --> G{Pass?}
    G -- Yes --> H[Accept batch]
    G -- No --> I[Reject batch]
7Sampling and Criteria for Conformity

IS 14695: Sampling and Criteria for Conformity

Sampling (Clause 7.1.3.2 & Table 4)

No. of Rolls in LotSample Size (Rolls)Permissible Defective RollsSub-Sample Size (Rolls)
Up to 100502
101 to 150803
151 to 3001304
301 to 5002015
501 to 1,0003226
1,001 to 3,0005038
Above 3,00080510

Criteria for Conformity (Clause 7.1.4)

  • The lot conforms if the number of defective rolls in the sample is less than or equal to the permissible number.
  • Testing and inspection are conducted on selected samples (Clause 7.1.1.1).
  • Sub-samples are tested for detailed properties.

Summary:

  • Select sample size based on lot size (see table).
  • Check defectives against permissible limits.
  • If defects ≤ permissible, lot is accepted.
  • Use sub-samples for detailed tests.
flowchart LR
    A[Select Lot Size] --> B{Determine Sample Size}
    B --> C[Select Rolls for Sample]
    C --> D[Test Rolls]
    D --> E{Defective Rolls ≤ Permissible?}
    E -->|Yes| F[Lot Accepted]
    E -->|No| G[Lot Rejected]

This ensures quality control by statistical sampling per IS 14695.

8Marking and Packaging

IS 14695: Marking and Packaging Key Points

Marking (Clause 9.1 & 9.2)

Each package must be legibly and indelibly marked with:

  • Manufacturer identification
  • Length, width, and weight of the roll
  • Batch number (code) and date of manufacture
    Additionally, the BIS Standard Mark may be applied on each package.

Packaging Requirements

  • Rolls must be clean, smooth, square cut, and free from telescoping.
  • Use cardboard separators and end shields to prevent damage during stacking and transport.
  • Packaging should ensure safe handling and maintain product integrity.

Quality Criteria (Clause 7.1.3.1 & Table 3)

  • For breaking strength, calculate average (X) and range (R) for wrap and weft directions.
  • Conformance requires:
    [ X - 0.6R \geq \text{specified minimum breaking strength} ]
  • Minimum breaking strength (Table 3):
    • Wrap: 30 kg
    • Weft: 15 kg
  • Pliability: No cracks on unrolling after 3 hours conditioning at 5°C; surface ruptures >5 mm = failure.

Summary Table: Marking & Packaging

AspectRequirement
MarkingManufacturer, dimensions, weight, batch, date, BIS mark
PackagingClean rolls, square cut, no telescoping, cardboard separators & end shields
Breaking Strength(X - 0.6R \geq) Min. strength (Wrap 30 kg, Weft 15 kg)
PliabilityNo cracks after conditioning; rupture ≤5 mm

flowchart TD
    A[Roll Manufacturing] --> B[Marking]
    B --> C{Marking Details}
    C -->|Manufacturer| D[Identification]
    C -->|Dimensions| E[Length, Width, Weight]
    C -->|Batch Info| F[Batch No. & Date]
    B --> G[BIS Certification Mark]
    A --> H[Packaging]
    H --> I[Clean, Smooth, Square Cut Rolls]
    H --> J[Cardboard Separators & End Shields]
    H --> K[Prevent Damage During Transport]

This ensures

Annex AMethods of Test for Various Properties of Glass Fibre Tissue

IS 14695: Key Methods & Specifications for Testing Glass Fibre Tissue

1. Weight of Glass Fibre Tissue (Annex A, Clause 3.1 & 5.2.1)

  • Randomly select rolls as per IS 4905.
  • Weigh selected rolls; average weight represents consignment.
  • Calculate weight per 10 m² from average.

2. Thickness Measurement (Fig. 1)

  • Use metallic cylinder and clamp setup.
  • Mount specimen without distortion.
  • Measure thickness using calibrated device.

3. Tensile Strength (Fig. 2, Table 3)

PropertyRequirement (kg)Test Ref.
Breaking StrengthWrap: ≥ 30IS 13826 Part 1
Weft: ≥ 15

4. Pliability (Clause 6, Table 3)

  • Condition sample 3h at 5°C.
  • On unrolling, no cracks allowed.
  • Surface ruptures > 5 mm = failure.

5. Air Permeability Test (Clause A-4.3)

  • Clamp specimen over orifice.
  • Draw air at 1 m/s.
  • Record pressure drop in mm water.
  • Average over 5 specimens.

6. Temperature Resistance (Clause A-5)

  • Test 5 specimens, size 25 cm × 25 cm.
  • Evaluate per specified procedure.
flowchart LR
    A[Select Specimens] --> B[Measure Weight]
    B --> C[Calculate Weight per 10 m²]
    A --> D[Measure Thickness]
    A --> E[Test Tensile Strength]
    A --> F[Test Pliability]
    A --> G[Test Air Permeability]
    A --> H[Test Temperature Resistance]

This summarizes essential test methods and requirements per IS 14695 for glass fibre tissue quality control.

Popular Questions About IS 14695

?What are the required physical properties of the glass fibre tissue specified in IS 14695?

Physical Properties of Glass Fibre Tissue as per IS 14695:

  • Composition: Thin, flexible, uniformly bonded mat of chemically resistant borosilicate staple glass fibres, randomly distributed and bonded with phenolic thermosetting resin (Clause 3.1).

  • Thickness Measurement (Clause 6.45):

    • Sample placed on glass plate.
    • Metallic cylinder with foot and anvil area = 6.45 cm² applies pressure of 35 g/cm².
    • Deflection measured by dial gauge (least count 0.01 mm).
  • Breaking Strength (Table 3, Clause 6):

    • Wrap direction: Minimum 30 kg
    • Weft direction: Minimum 15 kg
    • Test as per IS 13826 (Part 1).
  • Pliability (Table 3, Clause 6):

    • After 3 hours conditioning at 5°C, roll shall not crack on unrolling.
    • Surface ruptures >5 mm considered failure (IS 13826 Part 2).
  • Porosity & Air Permeability:

    • Conditioned specimen clamped and air drawn at 1 m/s through known area.
    • Pressure drop recorded in mm water column.

Summary Table of Key Properties

PropertyRequirementTest Reference
ThicknessMeasured under 35 g/cm² pressureClause 6.45
Breaking StrengthWrap ≥ 30 kg, Weft ≥ 15 kgIS 13826 (Part 1)
PliabilityNo cracks after 3h at 5°CIS 13826 (Part 2)
CompositionBorosilicate glass fibres + phenolic resinClause 3.1
Air PermeabilityPressure drop at 1 m/s airflowClause 4.3

Loading diagram...
?How is the thickness of the glass fibre base outerwrap measured according to this standard?

According to IS 14695, the thickness of the glass fibre base outerwrap is measured as follows:

  • Sample Preparation: Place the glass fibre tissue sample on a glass plate.
  • Measuring Device: Use a metallic cylinder with a foot and anvil area of 6.45 cm².
  • Pressure Applied: Apply a pressure of 35 g/cm² on the sample.
  • Measurement: Measure the deflection using a dial gauge with a least count of 0.01 mm.

This method is detailed in Clause 6.45 and illustrated in Fig. 1 of the standard.


Summary Table

ParameterValue
Foot & Anvil Area6.45 cm²
Pressure Applied35 g/cm²
Dial Gauge Least Count0.01 mm

This ensures consistent and precise thickness measurement of the glass fibre outerwrap.

?What are the criteria for sampling and acceptance of rolls in a batch?

Criteria for Sampling and Acceptance of Rolls in a Batch (IS 14695)

  1. Sampling Procedure (Clause 7.1.2.1):

    • Rolls are selected randomly from the lot.
    • Randomness should follow procedures in IS 4905.
  2. Sample Size & Acceptance (Table 4, Clause 7.1.3.2):

    Lot Size (No. of Rolls)Sample Size (Rolls)Max Defective Rolls AllowedSub-Sample Size (Rolls)
    Up to 100502
    101 to 150803
    151 to 3001304
    301 to 5002015
    501 to 1,0003226
    1,001 to 3,0005038
    Above 3,00080510
  3. Acceptance Criteria (Clause 7.1.3.1):

    • Number of defective rolls ≤ permissible defective rolls (col 3).
    • For breaking strength:
      [ X - 0.6R \geq \text{specified value} ] where:
      • (X) = average breaking strength
      • (R) = range (max - min) of breaking strength
    • All test pieces must satisfy pliability requirements (Table 3).
  4. Additional Notes:

    • Rolls must be clean, smooth, square cut, and protected during handling.

This ensures quality control and uniformity in batch acceptance.

?Which tests are mandatory to ensure the temperature resistance of the outerwrap?

Mandatory Test for Temperature Resistance of Outerwrap (IS 14695):

  • Requirement: Outerwrap must remain unaffected under load in hot bitumen at 280°C for 1 minute (Clause 1.9).
  • Test Method: The outerwrap is subjected to hot bitumen at 280°C for 1 minute to ensure it retains integrity and performance.
  • Acceptance Criteria: No visible damage, deformation, or loss of properties after exposure.

Summary of Key Tests for Outerwrap Temperature Resistance:

PropertyRequirementTest ConditionReference
Temperature ResistanceUnaffected under loadHot bitumen at 280°C for 1 minIS 14695 Clause 1.9

Additional Relevant Tests (for overall quality):

  • Breaking Strength: Wrap ≥ 30 kg, Weft ≥ 15 kg (IS 13826 Part 1)
  • Pliability after conditioning at 5°C for 3 hrs: No cracks or ruptures >5 mm (IS 13826 Part 2)

Loading diagram...

In brief: The mandatory temperature resistance test per IS 14695 is the exposure of the outerwrap to hot bitumen at 280°C for 1 minute under load, ensuring no adverse effects.

?What mineral fillers and surfacing powders are specified for use in the outerwrap?

Mineral Fillers and Surfacing Powders for Outerwrap (IS 14695):

  • Mineral Filler (Clause 3.3):

    • Finely divided inert mineral matter
    • Insoluble in water
    • Particle size: passes through 75 microns IS Sieve (IS 460 Part 1)
  • Mineral Powder for Surfacing (Clause 3.4.1):

    • Powdered mineral matter such as talc or mica
    • Particle size: passes through 600 microns IS Sieve (IS 460 Part 1)
    • Alternatively, sand passing through 250 microns IS Sieve may be used
  • Additional Info (Clause 2.3):

    • Sand quantity: 2.3 kg per 10 m² of outerwrap surface

Purpose:
The mineral powder dusting prevents layers from sticking and ensures a smooth, uniform outerwrap surface free from defects.


Summary Table

MaterialParticle Size (IS Sieve)Notes
Mineral Filler75 micronsInsoluble inert mineral
Talc/Mica600 micronsPowdered mineral matter
Sand250 micronsAlternative for surfacing
Loading diagram...

Need Detailed Clause Answers?

Ask AI about any clause, requirement, or provision in IS 14695. Get instant, clause-cited responses powered by our indexed library.

Free tier includes 150 queries (50 AI + 100 Reference) · No credit card required