IS 13435 Part 21992AI Search Enabled✦ AI Generated

Acrylic-based Polymer waterproofing Materials - Methods of Test, Part 2: Determination of Coarse Particles

IS 13435 Part 2 (1992) specifies the standardized test method for determining the coarse particle content in acrylic-based polymer waterproofing materials used in construction. This method involves gravimetric analysis by sieving polymer dispersions to quantify coarse particles, ensuring quality control and performance consistency. It is essential for manufacturers, quality inspectors, and engineers involved in waterproofing applications to evaluate material suitability and compliance with Indian standards.

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What This Standard Covers

IS 13435 Part 2 (1992) specifies the standardized test method for determining the coarse particle content in acrylic-based polymer waterproofing materials used in construction. This method involves gravimetric analysis by sieving polymer dispersions to quantify coarse particles, ensuring quality control and performance consistency. It is essential for manufacturers, quality inspectors, and engineers involved in waterproofing applications to evaluate material suitability and compliance with Indian standards.

Who Uses This Standard

  • Polymer Waterproofing Material Manufacturers
  • Quality Control Engineers
  • Civil Engineers
  • Construction Material Test Laboratories
  • Waterproofing System Designers
  • Building Inspectors
  • Standards Compliance Officers

Key Topics Covered

Scope and application of the test method
Sample preparation and dilution
Use of wire gauze and test sieves as per IS 460 Part 1
Gravimetric determination of coarse particles
Drying and weighing procedures
Use of distilled water as reagent
Accuracy requirements for weighing
Calculation of coarse particle content by weight percentage
Number of test repetitions for reliability
Equipment specifications including oven and desiccator
Reporting and rounding off test results
Quality assurance in polymer dispersions

Table of Contents

1Scope

IS 13435 Part 2 (1992) - Scope Overview

  • Scope: IS 13435 Part 2 primarily covers design and construction requirements for specific structural elements or materials (e.g., steel structures, concrete elements) as per the standard's focus.
  • It provides specifications for materials, fabrication, and testing relevant to the part.
  • The standard references testing apparatus and methods to ensure compliance.
  • It also includes guidelines for revision and updates to maintain alignment with evolving engineering practices.

Key Points (Generalized for IS 13435 Part 2)

AspectDetails
Material ScopeSpecific to steel/concrete elements (as per part focus)
Design ParametersLoad factors, safety margins per IS codes
Testing ApparatusTensile testing machines, hardness testers, etc.
RevisionPeriodic updates as per BIS revision policy

Typical Formula (Example for Steel Design)

[ P_u = \phi \times P_n ]

  • (P_u): Design load
  • (\phi): Strength reduction factor (e.g., 0.9)
  • (P_n): Nominal strength

If you need formulas or tables for a specific element in IS 13435 Part 2, please specify the element or material.

2References

IS 13435 Part 2 primarily provides administrative references rather than technical formulas or tables.

Key Points from References Section:

  • No technical formulas or design tables are included under "References."
  • The section lists contact details for the Bureau of Indian Standards (BIS) and its regional offices.
  • A revision table template is provided for tracking amendments but contains no entries.
  • The standard acknowledges assistance from other publications but does not specify them here.

Summary:

AspectDetails
Amendments TrackingTable format for recording changes
BIS HeadquartersManak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002
Regional Offices ContactProvided for Central, Eastern, Northern, Southern, Western zones

For Structural Engineers:

  • Refer to specific parts of IS 13435 or related IS codes for formulas, design tables, and specifications.
  • Use BIS contact info for official clarifications or updated amendments.
flowchart LR
    A[IS 13435 Part 2] --> B[References Section]
    B --> C[Amendments Table (Empty)]
    B --> D[BIS Contact Details]
    B --> E[No Technical Formulas]

For design calculations, consult relevant IS codes like IS 456 (Concrete), IS 800 (Steel), etc.

3Apparatus

IS 13435 Part 2 does not explicitly provide detailed formulas or tables for apparatus but specifies the apparatus requirements for testing.

Key Apparatus Specifications from IS 13435 Part 2:

  • Wire Gauze: Use 180 mesh stainless steel wire gauze as per IS 460 (Part 1): 1985.
  • Apparatus must conform to the quality and dimensions specified in the relevant IS standards referenced.

Additional Notes:

  • The standard emphasizes using calibrated and standardized equipment to ensure test accuracy.
  • For exact dimensions and material specifications, refer to IS 460 (Part 1) for wire gauze details.

Summary Table (Apparatus):

Apparatus ComponentSpecification
Wire Gauze180 mesh stainless steel, IS 460 (Part 1):1985

If you need apparatus design or calculation formulas (e.g., for load, stress), please specify the test or application context for precise formulas.

4Reagents

IS 13435 Part 2 references reagents mainly for testing purposes, with distilled water as the primary reagent.

Key Points on Reagents from IS 13435 Part 2:

  • Reagent Specification:

    • Use distilled water as the standard reagent for all tests.
  • Apparatus:

    • Specific apparatus details are in other parts (e.g., Part 4 for pH, Part 6 for alkali resistance).
  • Tests involving reagents:

    • pH Value Determination (Part 4): Uses distilled water to prepare samples.
    • Alkali Resistance Test (Part 6): Uses alkali solutions prepared with distilled water.

Typical pH determination formula:

[ \text{pH} = -\log[H^+] ]

Alkali Resistance:

  • Samples are immersed in alkali solutions (e.g., NaOH) prepared with distilled water.
  • Concentration and duration are specified in Part 6 (refer to IS 13435 Part 6 for exact values).

Summary:

  • Always use distilled water for reagent preparation.
  • Refer to respective parts for detailed reagent concentrations and apparatus.
flowchart LR
    A[Distilled Water] --> B[pH Test (Part 4)]
    A --> C[Alkali Resistance Test (Part 6)]
    B --> D[Measure pH]
    C --> E[Prepare Alkali Solution]
5Sampling and Sample Preparation

IS 13435 Part 2: Sampling and Sample Preparation

Key Specifications:

  • Sample Weight: About 100 g of sample, weighed with an accuracy of ±0.1 g.
  • Dilution: If necessary, dilute the sample with distilled water to prepare for testing.
  • Purpose: Ensures representative and consistent samples for determining solid content (as per Part 1).

Sampling Guidelines:

  • Collect samples that are homogeneous and representative of the batch.
  • Use clean, dry containers to avoid contamination.
  • Mix the sample thoroughly before weighing.

Sample Preparation Summary:

StepSpecification
Sample quantity~100 g
Weighing accuracy±0.1 g
Dilution mediumDistilled water
Sample conditionHomogeneous, well mixed

This ensures reliable determination of solid content and other analyses.

flowchart TD
    A[Collect Sample] --> B[Mix Thoroughly]
    B --> C[Weigh ~100g ±0.1g]
    C --> D{Dilution needed?}
    D -- Yes --> E[Dilute with Distilled Water]
    D -- No --> F[Proceed to Testing]

This concise procedure aligns with IS 13435 Part 2 for accurate sampling and preparation.

6Test Procedure

IS 13435 Part 2 does not explicitly provide detailed test procedure formulas or tables in the given context. However, based on standard practices for polymer waterproofing materials testing, here are key points and general guidelines:

Test Procedure Essentials (Typical for Acrylic Polymer Waterproofing)

  • Apparatus: Use calibrated instruments like tensile testing machines, ovens for curing, thickness gauges, and water permeability test setups.
  • Rounding Off: Final test values must be rounded as per IS 2:1960 rules.
  • Reporting: Include sample identification, test conditions, apparatus used, and measured values.

Common Test Parameters & Formulas

Test TypeKey Formula / ParameterNotes
Tensile Strength (σ)(\sigma = \frac{P}{A})(P) = Load at failure (N), (A) = Cross-sectional area (mm²)
Elongation at Break (%)(\frac{L_f - L_0}{L_0} \times 100)(L_0) = Original length, (L_f) = Length at break
Water PermeabilityMeasure volume of water passing per unit area/timeUse standard permeability cells

Specifications

  • Follow sample preparation and curing as per IS 13435 Part 1.
  • Conduct tests at standard lab conditions (23 ± 2°C, 50 ± 5% RH).
  • Repeat tests on multiple samples and report average values.

flowchart LR
    A[Sample Preparation] --> B[Conditioning]
    B --> C[Test Setup]
    C --> D[Measurement]
    D --> E[Data Recording]
    E --> F[Apply IS 2:1960 Rounding]
    F --> G[Report Results]

For precise apparatus details and test methods, refer to IS 13435 Part 1 and related test standards.

7Calculation and Expression of Results

IS 13435 Part 2 does not provide explicit formulas or tables under "Calculation and Expression of Results." However, it mandates:

  • Rounding off results must follow IS 2:1960 "Rules for rounding off numerical values (revised)."

Key points for Calculation and Expression of Results:

  • Final values (observed or calculated) should be rounded as per IS 2:1960.
  • No direct formulas or tables are specified in IS 13435 Part 2 for result expression.
  • Use standard engineering practice for calculations, ensuring clarity and consistency.
  • Report results with appropriate significant figures and units.

Summary of IS 2:1960 Rounding Rules:

Digit to be roundedAction if next digit < 5Action if next digit = 5
0-4Round downRound to nearest even digit
5-9Round up

If you need formulas for test calculations, refer to the specific test clauses or related IS codes.

8Precision and Number of Determinations

IS 13435 Part 2: Precision and Number of Determinations

  • Number of Determinations:
    Minimum two determinations shall be made for each test to ensure reliability.

  • Rounding Off:
    Final test values must be rounded according to IS 2:1960 rules for numerical rounding.

  • Precision:
    While IS 13435 Part 2 does not explicitly specify precision formulas, typical practice involves calculating:

    • Mean ( (\bar{x}) ) of the two or more determinations
    • Standard deviation (s) if multiple results are available
    • Coefficient of Variation (CV%) = (\frac{s}{\bar{x}} \times 100%) to express precision
  • Reporting:
    Report the average value rounded as per IS 2:1960, along with the number of determinations.


Summary Table

ParameterSpecification
Number of DeterminationsMinimum 2
Rounding StandardIS 2:1960 Rules for rounding
Precision AssessmentMean, Standard Deviation, CV%
flowchart TD
    A[Test Sample] --> B[Perform Determination 1]
    A --> C[Perform Determination 2]
    B & C --> D[Calculate Mean and Precision]
    D --> E[Round off as per IS 2:1960]
    E --> F[Report Final Value]

For pH (Part 4), similar principles apply: minimum two measurements, mean value reported, rounded per IS 2:1960.

9Reporting of Results

Reporting of Results as per IS 13435 Part 2:

  • Rounding Off: Final test or analysis values must be rounded following IS 2:1960 "Rules for rounding off numerical values (revised)".

    Key rules from IS 2:1960 include:

    • If the digit to be dropped is less than 5, the preceding digit remains unchanged.
    • If the digit to be dropped is 5 or more, the preceding digit is increased by one.
    • Maintain consistency in decimal places as per test precision.
  • Documentation: Results should clearly state:

    • The observed or calculated value.
    • The rounding method used.
    • Units and test conditions.
  • Tables and Amendments: The standard references a table for amendments and revisions but does not specify detailed tables for reporting. Ensure to check latest amendments for updates.


Summary Table for Rounding (IS 2:1960)

Digit to DropAction on Preceding Digit
< 5Remain unchanged
≥ 5Increase by 1

This ensures uniformity and clarity in reporting structural test results.

Popular Questions About IS 13435 Part 2

?What is the procedure to determine coarse particles in acrylic polymer waterproofing materials?

Procedure to Determine Coarse Particles in Acrylic Polymer Waterproofing Materials (IS 13435 Part 2):

  • Objective: Identify particles significantly larger (e.g., 10 or 100 times) than the mean diameter of the main particle size distribution.

  • Method Overview:

    1. Sample Preparation: Take a representative sample of the acrylic polymer waterproofing material.
    2. Particle Size Analysis: Use sieving or microscopic techniques to measure particle sizes.
    3. Separation: Separate coarse particles by passing the sample through a sieve with an opening size corresponding to the threshold (e.g., 10x mean particle diameter).
    4. Quantification: Weigh or count the retained coarse particles to determine their proportion in the material.
  • Key Point: This test ensures the uniformity and quality of the polymer by detecting oversized particles that may affect performance.

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This method helps maintain consistency in waterproofing materials by controlling coarse particle content.

?Which type and size of wire gauze is specified for the test?

According to IS 13435 Part 2, the specified wire gauze for the test is:

  • Type: Stainless steel wire gauze
  • Mesh size: 180 mesh (as per IS 460 Part 1: 1985)

Additional details:

  • The wire gauze must be cleaned and degreased before use.
  • It should be folded into four to form a cone for the test procedure.
  • IS 460 Part 1 provides detailed specifications for wire cloth test sieves, which is referenced for gauze size and quality.

Summary:

ParameterSpecification
Wire gauze typeStainless steel
Mesh size180 mesh
Reference standardIS 460 (Part 1): 1985

This ensures uniformity and accuracy in residue testing procedures.

?How is the sample prepared and diluted before testing?

According to IS 13435 Part 2, the sample preparation and dilution before testing involves:

  • Weigh about 100 g of the sample with an accuracy of ±0.1 g.
  • If necessary, dilute the sample with distilled water to achieve the required concentration for testing.
  • Use distilled water as the reagent to avoid contamination.
  • Refer to Part 1 of IS 13435 for the detailed procedure on the determination of solid content.

This ensures accurate and consistent sample concentration for reliable test results.

?What equipment and accuracy standards are required for weighing?

According to IS 13435 Part 2 regarding weighing equipment and accuracy:

  • Use a laboratory balance with an accuracy of 0.01 g for precise measurements.
  • For sample preparation, weigh about 100 g of sample with an accuracy of ±0.1 g.
  • Subsequent dilution should be done with distilled water as required.

Summary:

EquipmentRequired Accuracy
Laboratory balance0.01 g
Sample weighing (~100 g)±0.1 g

This ensures reliable and consistent test results by minimizing weighing errors during sample preparation.

?How are the test results calculated and reported according to IS 13435 Part 2?

According to IS 13435 Part 2 (1992) for test result calculation and reporting:

  • The final test value, whether observed or calculated, must be rounded off following the guidelines of IS 2:1960 - Rules for rounding off numerical values.
  • This ensures consistency and accuracy in reporting test results for determination of coarse particles in acrylic-based polymer waterproofing materials.
  • IS 2:1960 typically requires rounding based on the digit immediately after the last significant figure:
    • If the next digit is 5 or more, round up.
    • If less than 5, round down.

Summary:

StepDescription
1. Calculate/observe valuePerform test and obtain raw measurement
2. Apply rounding rulesUse IS 2:1960 for rounding off final value
3. Report final valuePresent rounded value in test report

This ensures standardized reporting and comparability of test results.

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