IS 11251974AI Search Enabled✦ AI Generated

Method of test for determination of weathering of natural building stones

IS 1125:1974 specifies the standardized laboratory procedure to evaluate the weathering characteristics of natural building stones used in construction. It guides engineers and material testers in assessing the durability of stone samples through cyclic exposure to gypsum and water, measuring changes in absorption and volume to predict long-term performance under weathering conditions.

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What This Standard Covers

IS 1125:1974 specifies the standardized laboratory procedure to evaluate the weathering characteristics of natural building stones used in construction. It guides engineers and material testers in assessing the durability of stone samples through cyclic exposure to gypsum and water, measuring changes in absorption and volume to predict long-term performance under weathering conditions.

Who Uses This Standard

  • Civil Engineers
  • Materials Testing Laboratories
  • Geologists
  • Construction Quality Control Engineers
  • Architects
  • Quarry Managers
  • Research and Development Specialists in Building Materials

Key Topics Covered

Sample selection from quarries and natural rock
Preparation and dimensions of test specimens
Cyclic weathering test procedure using gypsum and water
Measurement of weight and volume changes
Calculation of absorption and volume increase percentages
Apparatus requirements and setup
Number of test cycles and duration
Cleaning and handling of specimens post-test
Reporting and documentation of test results
Interpretation of weathering resistance
Quality control for natural building stones
Standard rounding off rules for numerical data

Table of Contents

1Scope

IS 1125 - Scope & Key Specifications

  • Scope: Covers testing of natural stones for properties like water absorption and volume changes after cyclic tests.

  • Apparatus (Clause 4.1):

    • Enclosed balance, 1 kg capacity, sensitivity 0.01 g.
    • Suspension wire: brass, 0.81 mm dia.
    • Components: Beam (A), Loop (B), Suspension wire (C), Water level (D).
  • Test Specimen Info to Report (Clause 7.2):

    • Preparation method.
    • Size & shape.
    • Sample ID: quarry location, stone name/position, date, trade name/grade.
  • Key Formula (Clause 5.3):

[ \text{Water Absorption} = \frac{W_a - W_d}{W_d} \times 100% ]

Where:

  • (W_a) = final weight in air after 30 cycles + 24h immersion

  • (W_d) = dry weight before test

  • (W_s) = weight suspended in water after test (used for volume calculation)

  • Volume after test:

[ V_2 = \frac{W_a - W_s}{\rho_w} ]

(\rho_w) = density of water (usually 1 g/cm³)


Diagram of Apparatus (simplified):

graph LR
A[Beam of Balance] --> B[Loop for attachment]
B --> C[Suspension wire (0.81 mm brass)]
C --> Specimen[Specimen suspended in water]
Specimen --> D[Water level]

Note: Follow IS 2-1960 for rounding off values in reports.

2Selection of Sample

IS 1125: Selection of Sample for Testing Weathering of Natural Building Stones

Key Points from Clauses 2.1 to 2.3:

  • Representative Sample:
    The sample must represent the true average quality of the stone type or grade (Clause 2.1).

  • Source of Sample:
    Samples can be taken from:

    • Quarried stone
    • Natural rock (as per 2.2.1 and 2.2.2)
    • Must be adequate in size to prepare the required number of test specimens (Clause 2.2).
  • Multiple Samples for Variability:
    If quality varies perceptibly, select multiple samples to capture the range of properties (Clause 2.3).


Practical Guidelines:

ParameterSpecification
Sample SizeSufficient for all required test pieces
Number of SamplesAt least one; more if variability exists
Sampling LocationRandom but representative from quarry/rock

Summary Diagram:

flowchart TD
    A[Start: Identify Stone Grade] --> B{Is stone quality uniform?}
    B -- Yes --> C[Select representative sample]
    B -- No --> D[Select multiple samples]
    C --> E[Ensure adequate size for tests]
    D --> E
    E --> F[Prepare test specimens]

Note: Always follow IS 1125 for detailed sampling and testing procedures to ensure reliable weathering assessment.

3Preparation of Test Pieces

IS 1125: Preparation of Test Pieces - Key Points

  • Test Piece Dimensions (Clause 3.1):

    • Cylinders: Diameter = 50 mm, Height = 50 mm
    • Cubes: Edge length = 50 mm
  • Number of Test Pieces (Clause 3.3):

    • Minimum 3 test pieces per test to ensure reliability.
  • Reporting Requirements (Clause 7.2):

    • Description of preparation method.
    • Size and shape of test pieces.
    • Sample identification: quarry name/location, rock position, sampling date, trade name/grade.
  • Rounding Off Results (IS 2-1960):

    • Final test values should be rounded as per IS 2 guidelines.

Summary Table for Test Pieces

ParameterCylinderCube
Diameter50 mm-
Height/Edge Length50 mm50 mm
Minimum Quantity3 pieces3 pieces

flowchart LR
    A[Sample Collection] --> B[Preparation of Test Pieces]
    B --> C{Shape}
    C -->|Cylinder| D[Diameter=50mm, Height=50mm]
    C -->|Cube| E[Edge=50mm]
    D & E --> F[Minimum 3 Pieces]
    F --> G[Testing]
    G --> H[Report Results]
    H --> I[Include preparation, size, ID]

This ensures standardized test piece preparation for consistent strength and durability testing of natural rock.

4Apparatus

IS 1125 - Apparatus for Weathering Test: Key Details

Apparatus Description (Clause 4.1 & 1.83)

  • Balance: Enclosed, 1 kg capacity, sensitivity 0.01 g.
  • Suspension wire: Brass, diameter 0.81 mm.
  • Basket: Made of 1.83 mm dia brass wire, all joints soldered.
  • Key Components:
    • A: Beam of balance
    • B: Loop for attachment
    • C: Suspension wire
    • D: Water level
    • E: Bail of basket
    • 7: Suspension basket
    • K: Water jar support
    • M: Bottom of basket
    • N: Balance pan suspension rod
    • P: Cut-away section of basket

Important Weights and Volumes (Clause 5.1)

SymbolDescription
W1Oven-dried weight before immersion
W2Weight suspended in water after 24-h immersion
W3Surface-dried weight after 24-h immersion
V1Volume after 24-h immersion
dDensity of water at test temperature
A2Final absorption (%) after 30 test cycles

Key Formula for Absorption (A2)

[ A_2 = \frac{W_3 - W_1}{W_1} \times 100 ]

Notes

  • Weights must be measured with the specified sensitive balance.
  • Volume (V_1) is typically calculated from the water displacement method.
  • Density (d) depends on temperature; refer to IS 2-1960 for rounding off rules.
flowchart LR
    W1[Oven-dried weight (W1)]
    W3[Surface-dried weight (W3)]
    W2[Weight in water (W2)]
    V1[Volume (V1)]
    d[Density of water (d)]
    A2[Absorption % (A2)]

    W1 --> A2
    W3 --> A2
    W2 --> V1
    V1 --> A2
    d --> A2

This apparatus and formula ensure precise measurement of specimen absorption and volume changes during weather

5Procedure

IS 1125: Procedure Summary for Testing

Apparatus (Clause 4.1)

  • Enclosed balance, 1 kg capacity, sensitive to 0.01 g.
  • Accessories for weighing specimen in water.
  • Components:
    • A: Beam of balance
    • B: Loop for attachment
    • C: Suspension wire (0.81 mm dia brass)
    • D: Water level

Testing Cycles (Clause 5.2)

  • Specimen placed in a 9 cm diameter, 1.5 cm deep dish.
  • Add 2 g powdered gypsum + 25 ml water.
  • Oven dry at 105 ± 2°C for at least 5 hours until dry.
  • Cool to 25 ± 5°C.
  • Repeat cycle 30 times, adding only 25 ml water after first cycle.

Key Measurements (Clause 5.3)

  • ( W_A ) = Final weight in air after 30 cycles + 24h immersion.
  • ( W_s ) = Final weight suspended in water after 30 cycles + 24h immersion.
  • ( V_2 ) = Final volume after 30 cycles.

Rounding Off (Clause 0.3)

  • Follow IS 2-1960 for rounding test results.

Formula for Specific Gravity or Volume Calculation:

[ \text{Volume } V_2 = \frac{W_A - W_s}{\rho_w} ]

where (\rho_w) = density of water (usually 1 g/cm³).


flowchart LR
    A[Start] --> B[Place specimen in dish]
    B --> C[Add 2g gypsum + 25 ml water]
    C --> D[Oven dry at 105±2°C for 5 hrs]
    D --> E[Cool to 25±5°C]
    E --> F{Repeat 30 cycles}
    F -->|Yes| C
    F -->|No| G[Weigh specimen in air (W_A)]
    G --> H[Weigh specimen suspended in water (W_s)]
    H --> I[Calculate volume (V_2)]
    I --> J[Report results]

This concise procedure ensures consistent testing and reporting under IS 1125.

6Calculation

IS 1125: Key Formulas & Specifications for Calculation

The code focuses on determining water absorption and volume changes of specimens after immersion and cyclic testing.

Key Parameters:

SymbolDescription
W1Oven-dried weight before immersion
W3Surface-dried weight after 24h immersion
W2Weight suspended in water after 24h immersion
V1Volume after 24h immersion
WASurface-dried weight after 30 cycles + 24h immersion
WsWeight suspended in water after 30 cycles + 24h immersion
V2Volume after 30 cycles
dDensity of water at test temperature
A2Final absorption (%) after 30 cycles

Important Formulas:

  • Volume of specimen:

[ V = \frac{W_3 - W_2}{d} ]

  • Water absorption (%) after 30 cycles:

[ A_2 = \frac{W_A - W_1}{W_1} \times 100 ]

  • Density of specimen:

[ \rho = \frac{W_1}{V} ]

Apparatus:

  • Enclosed balance (capacity 1 kg, sensitivity 0.01 g)
  • Suspension wire (0.81 mm brass)
  • Water container with level control

Reporting:

  • Follow rounding rules per IS 2-1960.
  • Report weights, volumes, absorption percentages clearly.

flowchart LR
    W1[Oven-dried weight (W1)]
    W3[Surface-dried weight (W3)]
    W2[Weight suspended in water (W2)]
    d[Density of water (d)]
    V1[Volume after 24h immersion (V1)]
    A2[Water absorption (%)]

    W3 -->|Subtract| W2
    W2 -->|Divide by| d
    d --> V1
    W1 -->|Calculate absorption with WA| A2

This concise summary aids in calculating specimen volume, density, and water absorption per IS 1125.

7Report of Test Results

IS 1125: Report of Test Results - Key Points

Important Definitions (Clause 5.3)

  • WA = Final weight in air of surface-dried specimen after 30 cycles + 24h immersion.
  • V2 = Final volume of specimen after 30 cycles.
  • Ws = Final weight of specimen suspended in water after 30 cycles + 24h immersion.

Reporting Requirements (Clause 7)

  • 7.1: Report the average of three test results as:

    • % Increase in absorption
    • % Increase in volume
  • 7.2: Include additional info:

    • Preparation method of test pieces
    • Size & shape of test pieces
    • Sample identification: quarry name/location, rock position, sampling date, trade name/grade
  • Rounding: Final values rounded per IS 2-1960.


Typical Calculation Formulas

[ \text{Percentage Increase in Absorption} = \frac{W_A - W_0}{W_0} \times 100 ]

[ \text{Percentage Increase in Volume} = \frac{V_2 - V_0}{V_0} \times 100 ]

Where:

  • (W_0), (V_0) = Initial weight and volume before test cycles.

Summary Diagram

flowchart TD
    A[Initial Specimen] --> B{Test Cycles (30 cycles + 24h immersion)}
    B --> C[Measure WA (weight in air)]
    B --> D[Measure Ws (weight in water)]
    B --> E[Measure V2 (volume)]
    C --> F[Calculate % Increase in Absorption]
    E --> G[Calculate % Increase in Volume]
    F & G --> H[Report Average of 3 Specimens + Sample Details]

Ensure all values are averaged over three specimens and reported with proper sample identification and preparation details.

Popular Questions About IS 1125

?What are the required dimensions and shapes for test specimens?

According to IS 1125:

  • Specimen Shape & Size (Clause 3.1):

    • Cylinders: 50 mm diameter × 50 mm height, OR
    • Cubes: 50 mm × 50 mm × 50 mm
  • Surface Finish (Clause 3.2):

    • Smooth finish
    • Edges rounded with a radius ≈ 3 mm by grinding
  • Number of Specimens (Clause 3.3):

    • Minimum of 3 specimens per test
  • Reporting Requirements (Clause 7.2):

    • Preparation method
    • Size and shape of specimens
    • Sample identification details (quarry, location, date, trade name/grade)

Summary Table:

ParameterRequirement
ShapeCylinder or Cube
Cylinder Size50 mm diameter × 50 mm height
Cube Size50 mm cube
Edge Radius~3 mm (rounded by grinding)
Number of SpecimensAt least 3
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This ensures consistency and reliability in rock testing as per IS 1125.

?How is the cyclic weathering test conducted using gypsum and water?

Cyclic Weathering Test Procedure (IS 1125, Clauses 5.1 to 5.3):

  1. Specimen Preparation:

    • Place each specimen in a flat dish (glass/porcelain/glazed stoneware).
    • Dish size: 9 cm diameter × 1.5 cm depth.
    • Add 2 g powdered gypsum + 25 ml water.
  2. First Cycle:

    • Put dishes with specimens in a well-ventilated oven at 105 ± 2°C.
    • Maintain for ≥ 5 hours or until water evaporates and gypsum dries.
    • Remove and cool to 25 ± 5°C.
  3. Subsequent Cycles (2 to 30):

    • Repeat the above cycle 29 times.
    • Add only 25 ml water (no gypsum added after first cycle).
  4. Post-Cycle Treatment:

    • Brush specimens with stiff-fibre brush to remove gypsum particles.
    • Immerse specimens in water for 24 hours.
    • Surface dry and weigh in air (W4) and in water (Ws) as per Clause 5.1.

Summary Table of Key Parameters:

ParameterValue
Dish size9 cm diameter × 1.5 cm depth
Powdered gypsum2 g (only first cycle)
Water per cycle25 ml
Oven temperature105 ± 2°C
Oven duration≥ 5 hours
Number of cycles30
Cooling temperature25 ± 5°C
Post-test soaking24 hours in water

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?What changes in stone properties are measured to assess weathering?

To assess weathering of natural building stones as per IS 1125, the following changes in stone properties are measured:

  • Loss in weight: Indicates material degradation due to weathering.
  • Change in compressive strength: Reduction reflects weakening of stone structure.
  • Alteration in water absorption: Increase shows enhanced porosity from weathering.
  • Surface texture and color changes: Visual signs of weathering effects.
  • Resistance to wetting-drying cycles and sulphate attack: Evaluated by repeated exposure tests.

These changes are determined by subjecting stone samples to accelerated weathering tests simulating:

  • Corrosive groundwater,
  • Wetting and drying cycles,
  • Sulphate attack,
  • Temperature variations.

Sample preparation involves selecting unweathered stones from different strata with distinct color, texture, or structure variations.


Summary Table of Key Weathering Parameters:

Property MeasuredSignificance
Weight loss (%)Material degradation
Compressive strength changeStructural weakening
Water absorption change (%)Porosity increase
Visual texture/color changeSurface deterioration
Resistance to cyclesDurability under environmental stress

This method ensures comprehensive evaluation of stone durability for construction use.

?How many cycles are performed in the weathering test and what is their duration?

According to IS 1125 Clause 5.2 and 5.3, the weathering test involves:

  • Number of cycles: 30 cycles.
  • Duration per cycle: Each cycle consists of:
    • Adding 2 g powdered gypsum + 25 ml water to the specimen in a dish.
    • Heating in a ventilated oven at 105 ± 2°C for at least 5 hours or until dry.
    • Cooling to 25 ± 5°C.
  • For the first cycle, gypsum is added; for subsequent 29 cycles, only 25 ml water is added.
  • After 30 cycles, specimens are brushed, immersed in water for 24 hours, surface dried, and weighed.

Summary:

ParameterValue
Number of cycles30
Temperature105 ± 2°C
Heating duration≥ 5 hours per cycle
Cooling temperature25 ± 5°C
Water added per cycle25 ml (2 g gypsum only 1st cycle)

This simulates accelerated weathering to assess stone durability.

?What information must be included in the test report for stone weathering?

IS 1125 does not explicitly list the details to be included in the test report for stone weathering within the provided context. However, based on standard engineering practice and typical IS code requirements for material testing reports, the test report for stone weathering should include:

  • Identification of the stone sample: source, type, and physical description.
  • Date and place of testing.
  • Test method reference: IS 1125 (First Revision).
  • Test conditions: details of exposure cycles (wetting/drying, temperature variations, sulphate concentration).
  • Duration of the test.
  • Initial and final physical properties: weight, dimensions, and appearance.
  • Results: quantitative data on weight loss, surface degradation, or strength reduction.
  • Observations: any visible changes, cracks, or scaling.
  • Conclusion: assessment of the stone’s resistance to weathering.
  • Signature and details of the testing authority.

This ensures traceability and clarity for evaluating stone durability.

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