IS 107721983AI Search Enabled✦ AI Generated

quick setting lime pozzolana mixture

IS 10772:1983 specifies the requirements for quick setting lime pozzolana mixtures used as a cost-effective alternative to cement in various construction applications except reinforced concrete. It covers the composition, chemical and physical properties, manufacturing process, and quality control of mixtures made from hydrated lime, pozzolanic materials like fly ash or burnt clay, gypsum, and accelerators. This standard is essential for engineers and construction professionals seeking to utilize quick setting lime pozzolana mixtures for masonry, plastering, levelling courses, and other structural works.

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1983Edition
Building Limes and Gypsum ProductsCategory
Alternative search terms: IS 10772 PDF, IS 10772 pdf free download, IS 10772 free download pdf, IS10772 PDF, IS-10772 PDF, IS 10772 1983 PDF, IS 10772:1983 PDF, IS 10772-1983 PDF, IS 10772 (1983) PDF, IS 10772 1983 edition PDF, IS 10772 edition 1983 PDF

What This Standard Covers

IS 10772:1983 specifies the requirements for quick setting lime pozzolana mixtures used as a cost-effective alternative to cement in various construction applications except reinforced concrete. It covers the composition, chemical and physical properties, manufacturing process, and quality control of mixtures made from hydrated lime, pozzolanic materials like fly ash or burnt clay, gypsum, and accelerators. This standard is essential for engineers and construction professionals seeking to utilize quick setting lime pozzolana mixtures for masonry, plastering, levelling courses, and other structural works.

Who Uses This Standard

  • Civil Engineers
  • Construction Material Manufacturers
  • Quality Control Engineers
  • Masonry Contractors
  • Structural Engineers
  • Building Material Suppliers
  • Research and Development Professionals in Construction

Key Topics Covered

Scope and application of quick setting lime pozzolana mixtures
Classification of mixtures into Types 1, 2, and 3
Chemical requirements including lime content, carbon dioxide, magnesium oxide, and sulphate limits
Physical requirements such as fineness, setting time, compressive strength, water retention, and soundness
Manufacturing process involving intergrinding of hydrated lime, pozzolanas, gypsum, and accelerators
Use of various pozzolanic materials like fly ash, burnt clay, rice husk ash, and bagasse ash
Testing methods and reference standards for chemical and physical properties
Storage and handling guidelines for the mixtures
Sampling procedures and criteria for conformity
Packaging and delivery requirements
Exclusions such as non-use in reinforced concrete
Role of accelerators to reduce setting time and improve early strength

Table of Contents

1Scope

IS 10772 - Scope: Key Specifications & Tables

This standard covers quick setting lime pozzolana mixtures with types 1, 2, and 3 classified by lime reactivity (70, 50, 30 kgf/cm² respectively).

1. Physical Requirements (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Test Reference (IS 4031-1968)
Fineness (Residue on 150 micron sieve, %)≤ 5≤ 5≤ 5Clause S
Setting Time (Initial, hours, Min)0.50.50.5Clause 7
Setting Time (Final, hours, Max)242424Clause 7
Compressive Strength (N/mm²)Clause 9
- 7 days (min)2.51.00.4
- 28 days (min)6.02.51.0
- 90 days (min)8.04.01.5
Water Retention (%) (min)707070Clause 15
Soundness Expansion (mm, max)101010Clause 5

2. Chemical Requirements (Clause 5.1, Table 1)

CharacteristicRequirementTest Reference
Available Lime (%)≥ 25IS 1514-1959
Carbon Dioxide (%) (max)≤ 2IS 6932-1973
Magnesium Oxide (%) (max)≤ 6IS 1727-1967
Sulphate Content as SO3 (%)
2Definitions

IS 10772: Definitions & Key Specifications Summary

1. Definitions

  • As per Clause 2.1, definitions follow IS 6508:1972 (Glossary of terms relating to building lime).

2. Physical Requirements (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Test Method Reference
Fineness (% residue on 150µ IS sieve)≤ 5≤ 5≤ 5Clause S, IS 4031-1968
Setting Time (Initial, hours, Min)0.50.50.5Clause 7, IS 4031-1968
Setting Time (Final, hours, Max)242424Clause 7, IS 4031-1968
Compressive Strength (N/mm²)Clause 9, IS 4031-1968
- 7 days (min)2.51.00.4
- 28 days (min)6.02.51.0
- 90 days (min)8.04.01.5
Water Retention (%) (Min)707070Clause 15, IS 4031-1968
Soundness Expansion (mm) (Max)101010Clause 5, IS 4031-1968
  • Note: Types 1, 2, and 3 correspond to pozzolana with lime reactivity values of 70, 50, and 30 kgf/cm² respectively.

3. Chemical Requirements (Clause 5.1, Table 1)

| Characteristic | Requirement | Test Method Reference | |-----------------------------|-------------

3Manufacture

IS 10772: Manufacture - Key Specifications & Tables

1. Chemical Requirements (Table 1, Clause 5.1)

CharacteristicRequirementTest Method Reference
Available lime (%)Min 25IS:1514-1959*
Carbon dioxide (%)Max 2IS:6932-1973+
Magnesium oxide (%)Max 6IS:1727-1967$
Sulphate content (SO3%)Max 3IS:1727-1967
Free moisture (%)Max 2Appendix A, IS:4098-1983§
Loss on ignition (%)Max 20IS:6932-1973+

2. Physical Requirements (Table 2, Clause 6.1)

CharacteristicType 1Type 2Type 3Test Method Reference
Fineness (% residue on 150μ IS sieve)≤ 5≤ 5≤ 5Clause S, IS:4031-1968*
Setting time (Initial, hours, Min)0.50.50.5Clause 7, IS:4031-1968*
Setting time (Final, hours, Max)242424Clause 7, IS:4031-1968*
Compressive strength (N/mm², Min)Clause 9, IS:4031-1968*
- 7 days (avg. 3 cubes)2.51.00.4
- 28 days (avg. 3 cubes)6.02.51.0
- 90 days (avg. 3 cubes)8.04.01.5
4Classification

IS 10772: Classification of Pozzolana Based on Physical & Chemical Requirements

1. Classification Types (Clause 4.1)

  • Type 1, Type 2, Type 3 — classified by physical properties and lime reactivity:
    • Type 1: Lime reactivity ≥ 70 kgf/cm²
    • Type 2: Lime reactivity ≥ 50 kgf/cm²
    • Type 3: Lime reactivity ≥ 30 kgf/cm²

2. Physical Requirements (Table 2, Clause 6.1)

CharacteristicType 1Type 2Type 3Reference (IS 4031-1968)
Fineness (% residue on 150-micron sieve)≤ 5≤ 5≤ 5Clause S
Setting Time (Initial, Min)≥ 0.5≥ 0.5≥ 0.5Clause 7
Setting Time (Final, Max, hours)≤ 24≤ 24≤ 24Clause 7
Compressive Strength (N/mm²) at:Clause 9
- 7 days (min avg. 3 cubes)2.51.00.4
- 28 days6.02.51.0
- 90 days8.04.01.5
Water Retention (%)≥ 70≥ 70≥ 70Clause 15
Soundness (Expansion, mm, Max)≤ 10≤ 10≤ 10Clause 5

3. Chemical Requirements (Table 1, Clause 5.1)

CharacteristicRequirementReference Method
Available Lime (%)≥ 25IS 1514-195
5Chemical Requirements

IS 10772: Chemical Requirements Summary

Key Chemical Requirements (Clause 5.1, Table 1)

CharacteristicRequirementTest Method Reference
Available lime, % (Min)25IS 1514-1959*
Carbon dioxide, % (Max)2IS 6932-1973+
Magnesium oxide, % (Max)6IS 1727-1967$
Sulphate as SO₃, % (Max)3IS 1727-1967
Free moisture, % (Max)2Appendix A, IS 4098-1983§
Loss on ignition, % (Max)20IS 6932-1973+

Notes:

  • Available lime ensures sufficient hydraulic activity.
  • Limits on CO₂ and MgO control durability and prevent excessive expansion.
  • Sulphate content controls sulfate attack risk.
  • Free moisture and loss on ignition affect material stability and quality.

References:

  • IS 1514: Methods for quick and hydrated lime.
  • IS 6932: Tests for building limes.
  • IS 1727: Chemical analysis methods.
  • IS 4098: Lime-pozzolana mixtures.

If needed, I can also provide physical requirements or testing procedures.

6Physical Requirements

IS 10772: Physical Requirements for Pozzolanic Materials (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Test Reference (IS 4031-1968)
Fineness (% residue on 150-micron sieve, max)5%5%5%Clause S
Setting Time (hours)Clause 7
- Initial (min)0.50.50.5
- Final (max)242424
Compressive Strength (N/mm², min)Clause 9
- 7 days (avg. of 3 cubes)2.51.00.4
- 28 days (avg. of 3 cubes)6.02.51.0
- 90 days (avg. of 3 cubes)8.04.01.5
Water Retention (%) (min)707070Clause 15
Soundness (Expansion, mm, max)101010Clause 5

Notes:

  • Types 1, 2, and 3 correspond to lime reactivity values of 70, 50, and 30 kgf/cm² respectively.
  • All physical tests refer to IS 4031-1968 methods.

Summary Diagram of Physical Requirement Checks

flowchart TD
    A[Start: Sample Pozzolana] --> B[Fineness Test (≤5% residue)]
    B --> C[Setting Time Test]
    C --> D{Initial ≥0.5 hr?}
    D -->|Yes| E{Final ≤24 hr?}
    D -->|No|
7Storage

IS 10772: Storage & Specifications Summary

Storage (Clause 7.1)

  • Store the mixture in a weather-tight building.
  • Ensure easy access for inspection and identification.
  • Protect from dampness to minimize deterioration.

Key Physical Requirements (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Test Reference
Fineness (% residue on 150-micron sieve)≤ 5≤ 5≤ 5IS 4031-1968 Clause S
Initial setting time (hours, min)0.50.50.5IS 4031-1968 Clause 7
Final setting time (hours, max)242424IS 4031-1968 Clause 7
Compressive strength (N/mm², min)IS 4031-1968 Clause 9
- 7 days2.51.00.4
- 28 days6.02.51.0
- 90 days8.04.01.5
Water retention (%)≥ 70≥ 70≥ 70IS 4031-1968 Clause 15
Soundness expansion (mm, max)101010IS 4031-1968 Clause 5

Note: Types 1, 2, 3 correspond to lime reactivity values of 70, 50, and 30 kgf/cm² respectively.


Chemical Requirements (Clause 5.1, Table 1)

CharacteristicRequirementTest Reference
Available lime (%)≥ 25IS 1514-1959
Carbon dioxide (%)
8Packaging and Delivery

IS 10772: Packaging and Delivery - Key Specifications

Packaging (Clause 8.1 & 8.3)

  • Bag Types: Jute, multi-ply paper, HDPE, or cloth bags.
  • Marking: Manufacturer's name/trade-mark, type, and net mass.
  • Bag Condition: Must be in good condition at delivery.
  • Net Mass per Bag: 50 kg ± 2.5%.

Physical Requirements (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Test Reference (IS 4031-1968)
Fineness (Residue on 150-micron) % Max555Clause S
Setting Time Initial (hours) Min0.50.50.5Clause 7
Setting Time Final (hours) Max242424Clause 7
Compressive Strength (N/mm²) MinClause 9
- 7 days average2.51.00.4
- 28 days average6.02.51.0
- 90 days average8.04.01.5
Water Retention % Min707070Clause 15
Soundness Expansion (mm) Max101010Clause 5

Notes:

  • Types 1, 2, and 3 correspond to lime reactivity values of 70, 50, and 30 kgf/cm² respectively.
  • Sampling (Clause 9.2): Test individual samples for MgO, CO₂, and water retention; composite samples for other tests.

Summary Diagram: Packaging & Delivery Flow

flowchart TD
    A[Manufacture Lime Pozzolana Mixture]
    B[Pack
9Sampling and Criteria for Conformity

IS 10772: Sampling and Criteria for Conformity

Key Specifications:

  • Bag net mass: 50 kg ± 2.5% (Clause 8.3)
  • Sampling & Inspection: As per IS 3535-1966 (Clause 9.1), except 5.8.1.
  • Sample Types (Clause 9.2):
    • Individual samples: Tested for MgO, CO₂, and water retention.
    • Composite samples: Tested for all other requirements.

Sampling & Testing Summary

ParameterSample TypeTest Method Reference
Magnesium Oxide (MgO)Individual sampleIS 3535 / Clause 6.1 & Table 2
Carbon Dioxide (CO₂)Individual sampleIS 3535 / Clause 6.1 & Table 2
Water RetentionIndividual sampleIS 3535 / Clause 6.1 & Table 2
Other PropertiesComposite sampleIS 3535 / Clause 6.1 & Table 2

Criteria for Conformity:

  • Tests must conform to requirements in columns 3 to 5 of Table 2 (Clause 6.1).
  • Process and lot inspection follow IS 3535 procedures.

Sampling Procedure (per IS 3535):

  • Samples taken randomly from bags in the lot.
  • Composite samples made by mixing individual samples.
  • Testing ensures uniformity and compliance.

Tolerance Formula for Bag Weight:

[ \text{Permissible weight range} = 50 \text{ kg} \pm (2.5% \times 50) = 50 \pm 1.25 \text{ kg} ]


flowchart TD
    A[Lot of Bags] --> B{Sampling}
    B --> C[Individual Samples]
    B --> D[Composite Sample]
    C --> E[Test MgO, CO₂, Water Retention]
    D --> F[Test Other Properties]
    E & F --> G{Conformity Check}
    G -->|Pass| H[Accept Lot]
    G -->|Fail| I[Reject Lot]

Summary: IS 10772 mandates specific sampling methods aligned with IS 3535,

10Inspection and Testing

IS 10772: Inspection and Testing Key Points

1. Inspection Requirements (Clause 9.1)

  • Process and lot inspection as per IS 3535-1966, except clause 5.8.1.
  • Sampling and testing follow Methods of sampling hydraulic cements.

2. Physical Requirements (Clause 6.1, Table 2)

CharacteristicType 1Type 2Type 3Reference Method (IS 4031-1968)
Fineness (% residue on 150 µm)≤ 5≤ 5≤ 5Clause S
Initial Setting Time (hours, min)0.50.50.5Clause 7
Final Setting Time (hours, max)242424Clause 7
Compressive Strength (N/mm²)Clause 9
- 7 days (min)2.51.00.4
- 28 days (min)6.02.51.0
- 90 days (min)8.04.01.5
Water Retention (%) (min)707070Clause 15
Soundness Expansion (mm, max)101010Clause 5

Note: Type 1, 2, 3 correspond to lime reactivity values of 70, 50, and 30 kgf/cm² respectively.

3. Chemical Requirements (Clause 5.1, Table 1)

CharacteristicRequirementTest Method
Available Lime (%)≥ 25IS 1514-1959
Carbon Dioxide (%)≤ 2IS 6932-1973

Popular Questions About IS 10772

?What types of pozzolanic materials are permitted in the quick setting lime pozzolana mixture?

According to IS 10772, the permitted pozzolanic materials for quick setting lime pozzolana mixture include:

  • Burnt clay (per IS: 1344-1981)
  • Fly ash (per IS: 3812-1981)
  • Rice husk ash
  • Bagasse ash
  • Calcined clay (per IS: 1344-1981)
  • Other suitable pozzolanas manufactured from locally available materials

These are interground with hydrated Class C lime (per IS: 712-1984), Type IV gypsum (per IS: 1290-1973), and/or suitable hardening accelerators to meet the specification requirements.

Summary:

Material TypeReference IS Code
Hydrated Class C LimeIS 712-1984
Burnt Clay (Pozzolana)IS 1344-1981
Fly AshIS 3812-1981
Rice Husk AshLocally sourced
Bagasse AshLocally sourced
Type IV GypsumIS 1290-1973

This combination ensures rapid setting and strength development in the lime-pozzolana mixture.

?What are the chemical limits for lime, carbon dioxide, and sulphate content in the mixture?

According to IS 10772 Clause 5.1, Table 1, the chemical limits for lime-pozzolana mixtures are:

Chemical ComponentLimit (%)Test Method Reference
Available Lime (min)25IS: 1514-1959
Carbon Dioxide (max)2IS: 6932-1973
Magnesium Oxide (max)6IS: 1727-1967
Sulphate as SO₃ (max)3IS: 1727-1967
Free Moisture (max)2Appendix A, IS: 4098-1983
Loss on Ignition (max)20IS: 6932-1973

Additional notes:

  • Gypsum content in the mixture should not exceed 6% by mass of lime and pozzolana.
  • Accelerators like metallic sulphates, chlorides, alum, etc., should not exceed 1% by mass.

This ensures the mixture's chemical stability and performance as a building lime-pozzolana blend.

?How is the setting time controlled and what are the minimum and maximum limits?

Setting Time Control in IS 10772 (Quick Setting Lime Pozzolana Mixture):

  • Control Method: Setting time is controlled by the proportions of hydrated lime, pozzolana, gypsum (max 6% by mass of lime + pozzolana), and accelerators (max 1% by mass).
  • Test Method: Setting time is measured as per IS 4031 (Part 5): 1988.
Setting Time TypeMinimum (hours)Maximum (hours)
Initial Setting Time0.5-
Final Setting Time-24
  • Notes:
    • Initial setting time must be at least 0.5 hours.
    • Final setting time must not exceed 24 hours.
    • Gypsum and accelerators regulate the setting rate.
    • Lime reactivity (IS 1727) and physical tests (IS 4031 parts) ensure compliance.
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This ensures rapid but controlled setting for durability and workability.

?What compressive strength values are required at 7, 28, and 90 days for different mixture types?

According to IS 10772 - Quick Setting Lime Pozzolana Mixture, the minimum compressive strength requirements for mortar cubes are:

Age (days)Type 1 (N/mm²)Type 2 (N/mm²)Type 3 (N/mm²)
72.51.00.4
286.02.51.0
908.04.01.5

Notes:

  • These values are averages of at least 3 mortar cubes tested as per IS 4031 (Part 7):1988.
  • Type 1, 2, and 3 correspond to pozzolana with lime reactivity values of 70, 50, and 30 kgf/cm² respectively.
  • Compressive strength reflects the hydraulic activity and quality of the lime-pozzolana mixture.

This ensures durability and performance for different mixture grades in construction applications.

?How should the mixture be stored to maintain quality before use?

To maintain the quality of the quick setting lime pozzolana mixture before use, IS 10772 specifies:

  • Storage Location: Store the mixture in a weather-tight building to protect it from moisture and dampness.
  • Accessibility: Ensure easy access for inspection and identification.
  • Packaging: Use bags made of jute, multiply paper, HDPE, or cloth, clearly marked with the manufacturer's name/trademark and net mass.
  • Bag Condition: Bags must be in good condition at delivery to prevent contamination or loss of material.

This prevents deterioration and maintains the mixture's properties until use.

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Key: Protect from moisture + proper packaging = maintained quality.

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