IS 10013 Part 1 (1981) specifies the requirements for Acid-Copper-Chrome (ACC) preservative, a water-soluble fixed type wood preservative used for treating timber and lignocellulosic materials. This standard defines the composition, quality parameters, sampling, and marking requirements to ensure effective preservation and enhanced durability of timber, especially for species of lesser natural durability. It is essential for manufacturers, quality controllers, and engineers involved in timber treatment and wood preservation.
Overview
IS 10013 Part 1 (1981) specifies the requirements for Acid-Copper-Chrome (ACC) preservative, a water-soluble fixed type wood preservative used for treating timber and lignocellulosic materials. This standard defines the composition, quality parameters, sampling, and marking requirements to ensure effective preservation and enhanced durability of timber, especially for species of lesser natural durability. It is essential for manufacturers, quality controllers, and engineers involved in timber treatment and wood preservation.
Audience
Contents
Structure
Scope (from IS 10013 Part 1 - 1981):
| Active Ingredients (Nominal % by weight) | Chemical | Content |
|---|---|---|
| Chromic acetate / boric acid | Cr (C2H3O2)3.H2O | 5% |
| Copper sulphate | CuSO4.5H2O | 50% |
| Sodium dichromate or Potassium dichromate | Na2Cr2O7.2H2O or K2Cr2O7 | 45% |
| Quantity | Unit | Symbol |
|---|---|---|
| Length | metre | m |
| Mass | kilogram | kg |
| Time | second | s |
| Force | newton | N |
| Pressure/Stress | pascal | Pa |
| Energy | joule | J |
flowchart TD
A[Timber] --> B[Preservative Treatment]
B --> C[Acid-Copper-Chrome (ACC) Preservative]
C --> D[Improved Durability]
D --> E[Extended Service Life]
Summary: IS 10013 Part 1 defines the formulation and quality requirements of ACC preservative for wood, ensuring enhanced timber durability through standardized chemical composition and treatment processes.
IS 10013 (Part 1) – Composition & Properties of Acid-Copper-Chrome Preservative
| Ingredient | Chemical Formula | Percentage (%) |
|---|---|---|
| Chromic acetate/boric acid | Cr(C2H3O2)3·H2O | 5 |
| Copper sulphate | CuSO4·5H2O | 50 |
| Sodium dichromate OR | Na2Cr2O7·2H2O | 45 |
| Potassium dichromate | K2Cr2O7 | 45 |
flowchart LR
A[Chromic acetate/Boric acid 5%] --> C[Preservative Mix]
B[Copper sulphate 50%] --> C
D[Sodium or Potassium dichromate 45%] --> C
C --> E[Acid-Copper-Chrome Preservative]
This formulation ensures fungicidal and insecticidal protection for treated timber as per IS 10013 (Part 1).
IS 10013 Part 1 - Sampling Key Points
Sampling Procedure (Clause 3.1):
Chemical Analysis (Clause 4.1):
Marking (Clause 5.1.1):
| Aspect | Standard/Clause | Description |
|---|---|---|
| Sampling Method | IS 4905-1968 | Random sampling from drums |
| Chemical Analysis | IS 2753 (Part 1)-1964 | Estimation of preservatives (Cu, As, Cr, Zn, B, creosote, fuel oil) |
| Compliance | IS 10013 Clauses 2.1, 2.1.1 | Chemical proportions must meet specified limits |
| Marking | Clause 5.1.1 | ISI Mark for certified products |
flowchart TD
A[Supply Batch] --> B[Random Sampling (IS 4905)]
B --> C[Sample Collection from Drums]
C --> D[Chemical Analysis (IS 2753)]
D --> E{Compliance Check}
E -->|Yes| F[Mark with ISI Certification]
E -->|No| G[Reject / Reprocess]
This process ensures quality and consistency in preservative solutions per IS 10013 Part 1.
IS 10013 (Part 1) - Chemical Analysis of Preservative Solution
| Ingredient | Compound Formula | Minimum % by Weight |
|---|---|---|
| Chromic acetate/boric acid | Cr(C₂H₃O₂)₃·H₂O | 5 |
| Copper sulphate | CuSO₄·5H₂O | 50 |
| Sodium dichromate | Na₂Cr₂O₇·2H₂O | 45 (alternative) |
| Potassium dichromate | K₂Cr₂O₇ | 45 (alternative) |
flowchart TD
A[Sampling of Preservative Solution] --> B[Prepare Sample as per IS 2753]
B --> C[Estimate Copper Content]
B --> D[Estimate Chromium Content]
B --> E[Estimate Arsenic, Zinc, Boron]
B --> F[Estimate Creosote & Fuel Oil]
C --> G[Compare with Minimum %]
D --> G
E --> G
F --> G
G --> H{Complies with IS 10013?}
H -->|Yes| I[Accept Batch]
H -->|No| J[Reject or Reprocess]
Note: Always round off numerical values as per IS 10013 rules before reporting results.
Each container must be legibly marked with the following:
| Marking Item | Description |
|---|---|
| Manufacturer's Name/Trade-mark | Identifies the producer or brand |
| Date of Manufacture | Production date for traceability |
| Percentage of Dry Active Ingredients | Ensures minimum preservative content as per IS |
If you need details on minimum percentages of preservatives or rounding rules, please specify.
Frequently Asked
According to IS 10013 Part 1, the Acid-Copper-Chrome (ACC) preservative active ingredients and their nominal proportions by weight are:
| Ingredient | Chemical Formula | Proportion (%) |
|---|---|---|
| Chromic acetate / Boric acid (Cr (C2H3O2)3·H2O) | Chromic acetate or boric acid | 5 |
| Copper sulphate | CuSO4·5H2O | 50 |
| Sodium dichromate or Potassium dichromate | Na2Cr2O7·2H2O or K2Cr2O7 | 45 |
This formulation ensures effective timber preservation by combining copper's fungicidal properties with chromium's fixation and boric acid's insecticidal effect.
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According to IS 10013 Part 1, the purity requirements for chemicals in preservative formulations are:
Analysis methods are detailed in TS: 2753 (Part I)-1964 (Clause 1.3).
| Parameter | Requirement |
|---|---|
| Chemical purity | ≥ 95% |
| Active ingredient in dry solid | ≥ 95% |
| Solution concentration | 15% (1 kg preservative in solution) |
This ensures effective preservation and compliance with IS standards.
Sampling and Preparation for Chemical Analysis as per IS 10013 Part 1
For Solution or Paste (Clause 3.2):
For Dry Powder Form (Clause 3.3):
Chemical Analysis (Clause 4.1):
Summary Table:
| Form | Sampling Method | Sample Size |
|---|---|---|
| Solution/Paste | Mix thoroughly, take sample | ≥ 1 kg per drum |
| Dry Powder | Representative sample | ≥ 1% of total contents |
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This ensures representative sampling for accurate chemical composition verification.
According to IS 10013 Part 1, the pH range for the preservative solution ready for use must be:
This pH is measured using a glass electrode at 15-25°C (Clause 2.3).
Maintaining this pH ensures the preservative's chemical stability and effectiveness in protecting timber or other materials against decay.
According to IS 10013 Part 1, the mandatory labeling on preservative containers includes:
Additional points:
This ensures clarity on preservative quality and composition for safe and effective use.
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