IS 13630 PART 92006AI Search Enabled✦ AI Generated

Ceramic Tiles - Methods of the test, Sampling and Basis of Acceptance, Part 9: Determination of crazing resistance - Glazed tiles (see IS 13630: Parts 1 to 15)
2006 Edition

This standard outlines the procedure for assessing the crazing resistance of glazed ceramic tiles, excluding those designed with intentional crazing. It involves exposing tiles to high-pressure steam in an autoclave followed by staining to reveal fine surface cracks, serving as a quality assessment for manufacturers and testers.

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What This Standard Covers

This standard outlines the procedure for assessing the crazing resistance of glazed ceramic tiles, excluding those designed with intentional crazing. It involves exposing tiles to high-pressure steam in an autoclave followed by staining to reveal fine surface cracks, serving as a quality assessment for manufacturers and testers.

Who Uses This Standard

  • Manufacturers of ceramic tiles
  • Engineers specializing in quality assurance
  • Laboratories conducting material testing
  • Structural and civil engineers
  • Architects specifying tile materials
  • Construction site supervisors
  • Certification and compliance organizations

Key Topics Covered

Understanding crazing phenomena in glazed ceramic tiles
Criteria for selecting and preparing test samples
Utilization of steam autoclave for testing
Step-by-step crazing resistance test procedure
Application and removal of staining agents to detect crazes
Assessment standards for crazing post-test
Documentation and reporting of test outcomes
Sampling protocols for glazed tile batches
Acceptance guidelines for tile lots
Distinguishing intentional crazing from defects
Comparison with international ISO norms
Handling and cooling protocols for test specimens

Table of Contents

1Scope and Applicability

This section defines the extent and limitations of the standard, focusing on test methods for crazing resistance in glazed tiles, excluding those with intentional crazing features. It also specifies the rules for rounding numerical values as per IS 2:1960, ensuring consistency in test result reporting. The section references related Indian Standards for methodology alignment.

2Terminology and Definitions

Key terms are aligned with ISO 13006:1998 standards pertinent to ceramic tiles, including classifications and marking. The section emphasizes adherence to IS 2:1960 for rounding numerical data to maintain uniformity in reporting and interpretation of test results.

3Referenced Standards and Rounding Procedures

This part lists applicable Indian Standards referenced within the document and reiterates the importance of rounding off test values according to IS 2:1960 guidelines. It provides examples illustrating how to round values to the appropriate number of significant figures.

4Equipment and Instrumentation

Details the specifications and requirements for the autoclave apparatus used in testing, including pressure range (typically 1.2 to 1.5 MPa), temperature control (around 180°C ± 2°C), material construction, and safety features. It also reiterates the rounding rules for reporting test data.

5Test Sample Preparation and Handling

Describes the selection criteria for test specimens, ensuring they are free from pre-existing defects or crazing. Specifies the autoclave test procedure involving gradual pressurization to 750 ± 20 kPa over one hour, maintaining pressure for two hours, followed by controlled decompression and cooling stages both inside the autoclave and in ambient conditions.

6Testing Methodology

Though no dedicated procedure clause exists, this section consolidates instructions on preparing specimens, autoclave usage, and rounding off results per IS 2:1960. It highlights the importance of consistent specimen preparation and testing conditions for reliable assessment.

7Result Expression and Data Reporting

Specifies that final test results must be rounded according to IS 2:1960 rules to match the significant figures of the referenced values. It provides a summary of rounding rules and practical examples to ensure consistency across reports.

8Test Documentation and Reporting

Outlines the mandatory contents of the test report, including tile description, number of specimens tested, count of specimens exhibiting crazing, and descriptive documentation of crazing via text, sketches, or photos. It also cautions against confusing crazing with scratches or cracks, ensuring accurate reporting.

Popular Questions About IS 13630 PART 9

?How is the crazing resistance of glazed tiles tested according to IS 13630 Part 9?

The crazing resistance test involves selecting appropriate glazed tile specimens (excluding those with intentional crazing), exposing them to high-pressure steam in an autoclave at 750 ± 20 kPa and about 168 ± 1°C for two hours, followed by rapid decompression and controlled cooling. After the treatment, tiles are stained and inspected visually to detect fine surface cracks. The number of specimens tested and those showing crazing are recorded and reported.

?What are the guidelines for selecting and preparing test specimens for crazing resistance?

Specimens must be free from visible defects and pre-existing crazes before testing. Selection involves a visual inspection under normal conditions, allowing spectacles if routinely used. Multiple specimens from a batch are tested to ensure reliability. Post-test, specimens are examined carefully to distinguish crazing from scratches or cracks, and detailed documentation is maintained.

?What autoclave specifications and conditions are recommended for the crazing resistance test?

A steam autoclave with external steam supply is preferred, though a directly heated autoclave is acceptable. It should accommodate at least five tiles spaced to avoid contact. Testing involves gradually increasing pressure to 750 ± 20 kPa over one hour, maintaining it for two hours at approximately 168 ± 1°C, followed by rapid decompression to atmospheric pressure, then cooling specimens inside the autoclave for 30 minutes and subsequently at room temperature for another 30 minutes.

?How is crazing detected and assessed after steam autoclave treatment?

After autoclave exposure, tiles are stained to reveal fine cracks in the glaze surface. Visual inspection distinguishes crazing—network-like fine cracks limited to the glaze—from scratches or structural cracks. The number of specimens exhibiting crazing is recorded along with descriptive documentation such as text, drawings, or photographs.

?What criteria determine acceptance for crazing resistance in glazed tiles?

Acceptance criteria involve recording and reporting the presence and extent of crazing after testing, including detailed descriptions. The standard does not specify numeric thresholds but excludes tiles designed with inherent crazing features. Proper documentation of the number of specimens tested, those with crazing, and the nature of crazing ensures quality control and consistency.

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