IS 73251974AI Search Enabled✦ AI Generated

Specification for apparatus for determining constituents of fresh concrete
1974 Edition

This standard outlines the specifications for equipment used to measure the amounts of cement, fine aggregate, and coarse aggregate in freshly mixed concrete with maximum aggregate size up to 40 mm. It provides detailed guidelines on the construction, materials, and dimensions of sieves, tanks, buckets, and balances to guarantee precise and repeatable assessment of concrete components. It is vital for laboratories and engineers engaged in concrete mix evaluation and quality assurance.

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1974Edition
Cement Concrete Aggregates and RCCCategory
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What This Standard Covers

This standard outlines the specifications for equipment used to measure the amounts of cement, fine aggregate, and coarse aggregate in freshly mixed concrete with maximum aggregate size up to 40 mm. It provides detailed guidelines on the construction, materials, and dimensions of sieves, tanks, buckets, and balances to guarantee precise and repeatable assessment of concrete components. It is vital for laboratories and engineers engaged in concrete mix evaluation and quality assurance.

Who Uses This Standard

  • Concrete Testing Laboratory Staff
  • Quality Assurance Engineers
  • Civil Engineering Professionals
  • Materials Testing Facilities
  • Construction Project Supervisors
  • Concrete Mix Design Specialists
  • R&D Engineers in Construction Materials

Key Topics Covered

Design criteria and specifications of testing apparatus
Construction materials for apparatus components
Dimensional standards and permissible tolerances
Bucket-shaped container specifications
Nested sieve sets for aggregate separation
Main and subsidiary water tanks design
Requirements for balances and counterweights
Specifications for funnels and stirring rods
Fundamental working principle for constituent determination
Marking protocols and apparatus identification
Sample washing and weighing procedures
Ensuring accuracy and consistency in measurements

Table of Contents

1Scope and Standard Specifications

Scope Overview: This section defines the requirements for apparatus used in determining the proportions of cement, fine aggregate, and coarse aggregate in fresh concrete, ensuring standardized testing methods.

Highlights:

  • Marking of Components (Clause 6.1): Each piece of equipment shall bear indelible markings of the manufacturer’s name or trademark and the manufacturing date, without affecting functionality.

  • Rounding Off Rules (Clause 0.3): Test outcomes must be rounded according to IS 2:1960, maintaining the specified number of significant figures.

  • Material Requirements (Clause 5.1): Materials used for apparatus parts are detailed in Table 1 to promote durability and precision.

Apparatus Components and Dimensions:

  • Standard Sieves: Diameter of 475 mm for coarse aggregate; 150-micron sieve for fines.
  • Supporting Mesh and Spider: Detailed design specifications with millimeter-level precision.
  • Funnels: Properly dimensioned to facilitate efficient sample transfer.

Summary Table:

ComponentSpecification
IS Sieve Diameter475 mm
Fine Spray for WashingAccording to IS requirements
Sieve Opening150 microns
MarkingManufacturer’s name and date (indelible)

flowchart LR
    A[Fresh Concrete Sample] --> B[Sieving Setup]
    B --> C{Sieves}
    C --> C1[475 mm Sieve]
    C --> C2[150 micron Sieve]
    B --> D[Supporting Mesh & Spider]
    B --> E[Funnel for Transfer]
    B --> F[Sample Bucket Base]
2Operational Principle

Working Principle Overview: This part describes how the apparatus separates and quantifies cement, fine aggregate, and coarse aggregate in fresh concrete with a maximum aggregate size of 40 mm.

Key Steps (Clause 2):

  • Separation by washing and sieving techniques.
  • Utilization of nested sieves (475 mm and 150-micron diameters) to differentiate coarse and fine aggregates.
  • Washing the concrete sample with a fine water spray to remove adhered cement paste.
  • Employing a bucket-shaped container submerged in a water tank to prevent loss during washing.

Essential Specifications:

PartMaterial and Dimensions
Water TankCorrosion-resistant metal (stainless steel or chrome/nickel plated steel), 2 mm thickness, 300 mm internal diameter and depth, overflow spout positioned 5 mm below rim, with tap and flexible piping to subsidiary tank, plus a baffle plate (1.6 mm thick, 70 x 100 mm) to reduce water turbulence.
SievesNested sieves: 475 mm diameter for coarse aggregate and 150-micron sieve for fines, conforming to IS standards.
MarkingIndelible manufacturer name/trademark and manufacture date on all components.

Apparatus Flow Representation:

flowchart LR
    A[Concrete Sample] --> B[Bucket Container]
    B --> C[Water Tank with Tap & Baffle]
    C --> D[Fine Spray Washing]
    D --> E[Nested Sieves]
    E --> F[Separated Cement, Fine and Coarse Aggregates]
3Apparatus Component Dimensions

Component Dimensions and Specifications:

Principal Measures (in millimeters):

ComponentSize and Notes
Main Water TankInternal diameter approx. 300 mm; depth approx. 300 mm
Overflow SpoutPositioned 5 mm below the top edge
Tap Location20 mm below the upper rim
Baffle PlateThickness 1.6 mm; size 70 mm (depth) x 100 mm (length); placed opposite tap, extending from top to 50 mm below tap center
Bucket ContainerSized to fit comfortably inside the main tank

Material Requirements (Clause 5.1):

  • Corrosion-resistant metals such as stainless steel or chromium/nickel plated steel sheet.
  • Tank thickness: 2.0 mm.
  • Baffle plate thickness: approximately 1.6 mm.

Marking Instructions (Clause 6.1):

  • Manufacturer’s name or trademark and date of manufacture must be clearly inscribed without impairing performance.

Diagram of Water Tank Setup:

flowchart TB
    A[Subsidiary Water Tank]
    B[Flexible Pipe and Tap (20 mm below top)]
    C[Main Water Tank (300 mm dia x 300 mm depth)]
    D[Overflow Spout (5 mm below rim)]
    E[Baffle Plate (70 x 100 mm, 1.6 mm thick)]
    F[Bucket Container]

    A --> B --> C
    C --> D
    C --> E
    C --> F
4Components and Accessories

Overview of Parts and Associated Components:

Marking Requirements (Clause 6.1):

  • Each apparatus part must bear:
    • The manufacturer’s name or registered trademark.
    • Date of manufacture.
  • Markings should not interfere with the apparatus function.

Materials for Various Components (Clause 5.1 and Table 1):

ItemMaterialSpecial FeaturesIS Reference
Bucket with HandleNon-corroding metal (stainless steel, chromium/nickel plated steel)Smooth finish internally and externally-
TankSame as bucketSmooth internal surface-
SpiderBrassAs per IS: 292-1961
Stand for BucketCast ironAs per IS: 210-1970

Additional Accessories:

  • Fine spray apparatus for washing samples.
  • Spider supporting mesh with specified dimensions.
  • Base support for sample buckets.
  • Funnel designed for material transfer.
  • Counterpoises for air and water weighing.
  • Flexible connections between tanks.

Material Flow Diagram:

graph LR
A[Bucket & Handle] -->|Material| B[Non-corrodible Metal]
C[Tank] -->|Material| B
D[Spider] -->|Material| E[Brass]
F[Stand] -->|Material| G[Cast Iron]
5Materials Utilized in Apparatus Fabrication

Materials Designated for Construction (Clause 5.1 & Table 1):

ComponentMaterialSpecial RequirementsIS Standard Reference
Bucket including handleCorrosion-resistant metal (stainless steel, chromium or nickel plated steel)Smooth finish both inside and outside-
TankSame as bucketSmooth internal surface-
SpiderBrassCompliance with IS: 292-1961
Stand for sample bucketCast ironCompliance with IS: 210-1970

Notes:

  • Use corrosion-resistant metals in all parts contacting cement to prevent deterioration.
  • Surfaces must be finished smoothly to avoid material sticking and to maintain measurement accuracy.
  • Brass and cast iron components are specified according to relevant Indian Standards.

Reference Standards:

  • IS 292-1961: Specifications for brass ingots and castings.
  • IS 210-1970: Specifications for grey iron castings.
flowchart LR
    A[Bucket & Handle] -->|Material| B[Stainless Steel / Chromium or Nickel Plated Steel]
    C[Tank] -->|Material| B
    D[Spider] -->|Material| E[Brass (IS 292-1961)]
    F[Stand for Sample Bucket] -->|Material| G[Cast Iron (IS 210-1970)]
6Identification and Marking Guidelines

Marking and Identification Protocol (Clause 6.1 & 6.1.1):

  • Mandatory Marking Elements:

    • Manufacturer’s name or registered trademark (or both).
    • Date of manufacture.
  • Markings must be permanent, clear, and must not hinder apparatus operation.

  • Optional Mark:

    • The ISI certification mark may be applied in accordance with Indian Standards Institution regulations, indicating conformity to quality and testing criteria.

Material Information (Table 1, Clause 5.1):

ComponentMaterialSpecial RequirementsIS Reference
Bucket including handleCorrosion-resistant metals (e.g., stainless steel, chromium/nickel plated steel)Smooth internal and external finish-
TankSame as bucketSmooth internal finish-
SpiderBrassPer IS: 292-1961
Stand for sample bucketCast ironPer IS: 210-1970

Marking Notes:

  • Markings should be placed to avoid any negative impact on the apparatus functionality.
  • Use of the ISI mark is regulated under the Indian Standards Institution Certification Marks Act.
  • For detailed apparatus layouts and dimensions, refer to IS 7325 figures (e.g., Fig. 4 for sieves, Fig. 5 for funnel).

flowchart TD
    A[Apparatus Component] --> B[Mark Manufacturer Name/Trademark]
    A --> C[Mark Date of Manufacture]
    A --> D{Optional: ISI Certification Mark}
    D --> E[Complies with ISI regulations]

Popular Questions About IS 7325

?What materials are specified for fabricating the apparatus components?

As per IS 7325 Clause 5.1 and Table 1, the apparatus components are to be made from the following materials:

  • Main structural and body parts: mild steel or stainless steel to ensure corrosion resistance and longevity.
  • Sieves: stainless steel wire mesh to prevent rust and maintain mesh integrity.
  • Supporting mesh and spider: mild steel or stainless steel for durability and corrosion resistance.
  • Buckets and water tanks: constructed from non-corrosive materials like stainless steel or suitable plastics.
  • Flexible connectors: rubber or synthetic materials resistant to water and chemicals.
  • Counterpoises: cast iron or steel for stable and accurate weighing.

These material choices guarantee durability, precision, and compliance with functional requirements.


Materials Summary Table:

ComponentMaterial
Sieves (wire mesh)Stainless steel
Supporting Mesh & SpiderMild steel / Stainless steel
Sample Bucket & TanksStainless steel / Plastic
Flexible ConnectionsRubber / Synthetic
CounterpoisesCast iron / Steel

This selection supports corrosion resistance, dimensional stability, and precise measurement.

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?What are the required sizes and tolerances for the sieves and buckets?

According to IS 7325:

  • Sieves (Clause 4.1.5):

    • Diameter: 450 mm.
    • Two nested sieves:
      • IS sieve with 4.75 mm openings, depth 100 mm.
      • IS sieve with 150 microns opening, depth 300 mm.
    • Supported by a rigid, corrosion-resistant spider, typically brass, as shown in Fig. 4.
    • Conformance to IS:460-1962.
  • Buckets (Clause 4.1.2):

    • Made from corrosion-resistant metals such as stainless steel or chromium/nickel plated steel.
    • Thickness: 2.0 mm.
    • Internal diameter: 200 ± 5 mm at the top.
    • Depth: 180 ± 5 mm.
    • Smooth, sloping sides with a rounded bottom to prevent air pockets (refer to Fig. 2).
    • Weight uniformity tolerance: ±0.25 g in air, with an indicated correction for submerged weight loss.
  • Funnel (Clause 4.1.6):

    • Top diameter approximately 500 mm.
    • Bottom diameter approximately 150 mm.
    • Depth about 250 mm.
    • Thickness: 1.6 mm, made from corrosion-resistant metal.

These precise dimensions ensure consistent sample processing and reliable test results.

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?How does the apparatus accurately separate cement and aggregates?

The IS 7325 apparatus ensures precise separation of cement and aggregates by:

  • Weighing the fresh concrete sample both in air and submerged in water to determine its weight and volume characteristics.
  • Washing the sample thoroughly through two nested sieves:
    • The first sieve collects coarse aggregates (maximum nominal size up to 40 mm).
    • The second sieve captures fine aggregates, allowing cement paste and fines to be washed away.
  • The washing process removes cement paste, leaving clean aggregates behind.
  • The cleaned aggregates are then weighed while submerged in water to determine their weight accurately.
  • Using the known specific gravities of cement and aggregates, the proportions of each constituent are calculated.

This method leverages size and density differences along with careful washing and sieving to achieve accurate and reproducible constituent separation.

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?What is the procedure for weighing concrete samples in air and water?

The procedure according to IS 7325 for weighing concrete samples is as follows:

  1. Apparatus Preparation:

    • Use a semi-automatic balance with a 5 kg capacity and accuracy of 0.5 g.
    • The balance setup includes:
      • A counterpoise for weighing in air.
      • A separate counterpoise for weighing in water.
      • A main water tank and a subsidiary water tank connected with flexible piping (see IS 7325 Fig. 1).
  2. Weighing Steps:

    • Weigh the empty bucket in air using the air counterpoise.
    • Add the concrete sample into the bucket and weigh the combined sample in air.
    • Immerse the bucket containing the sample into the water tank and weigh it while submerged, using the water counterpoise.
  3. Post-Weighing Actions:

    • Wash the sample through the nested sieves to separate coarse and fine aggregates and remove cement.
    • Weigh the separated aggregates in water to determine their individual weights.
    • Calculate the proportions of the concrete constituents using their specific gravities.

Important Points:

  • Balance accuracy: ±0.5 g.
  • Maximum sample weight: 5 kg.
  • Use appropriate counterpoises for accurate air and water weighing.
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?How must the apparatus be marked to ensure identification and traceability?

According to IS 7325 Clause 6.1, each apparatus part must be clearly and permanently marked with:

  • The manufacturer’s name or registered trademark (or both).
  • The date of manufacture.

These markings must be legible and should not interfere with the apparatus’s operation.

Additionally, per Clause 6.1.1, the equipment may optionally include the ISI Certification Mark, indicating compliance with relevant Indian Standards under ISI supervision.

Summary of Marking Requirements:

Marking ElementRequirement
Manufacturer name/trademarkMandatory
Date of manufactureMandatory
ISI Certification MarkOptional (subject to licensing)

This marking system ensures product traceability and quality assurance throughout its lifecycle.

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